#------------------------------------------------------------------------------ #$Date: 2018-04-12 12:44:02 +0300 (Thu, 12 Apr 2018) $ #$Revision: 433 $ #$URL: svn://172.16.1.111/rod/cif/3/50/02/3500214.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500214 loop_ _publ_author_name 'El Mendili, Y' _publ_section_title ; Raman spectrum of commercial Tschermigite ; _journal_name_full 'Personal communication to ROD' _journal_year 2018 _chemical_compound_source 'commercial powder SRL, 99.5% 7784-26-1' _chemical_formula_structural 'Al H28 N O20 S2' _chemical_formula_sum 'Al H28 N O20 S2' _chemical_name_mineral Tschermigite _space_group_IT_number 205 _symmetry_space_group_name_Hall '-P 2ac 2ab 3' _symmetry_space_group_name_H-M 'P a -3' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 12.248 _cell_length_b 12.248 _cell_length_c 12.248 _raman_determination_method experimental _[local]_chemical_compound_color white _[local]_chemical_compound_state Solid _raman_measurement_device.location ENSICAEN _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model DXR _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 20 _raman_measurement_device.microscope_numerical_aperture 0.25 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 780 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 1 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1.3 _raman_measurement_device.diffraction_grating 900 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.datetime_initiated 2018-03-20 _raman_measurement.integration_time 600 _rod_data_source.file Tschermigite.rod _rod_data_source.block 3500020 _rod_database.code 3500214 loop_ _raman_complementary.id _raman_complementary.method 1 EDX loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9008299 COD http://www.crystallography.net/cod/9008299.html ; no XRD analysis data. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 4.917182e+001 0.000000e+000 5.013597e+001 1.140974e-001 5.110012e+001 1.110633e-001 5.206428e+001 1.082730e-001 5.302843e+001 1.058765e-001 5.399258e+001 1.042133e-001 5.495674e+001 1.042873e-001 5.592089e+001 1.065675e-001 5.688504e+001 1.084835e-001 5.784920e+001 1.091396e-001 5.881335e+001 1.086510e-001 5.977750e+001 1.062657e-001 6.074165e+001 1.008461e-001 6.170581e+001 9.360708e-002 6.266996e+001 8.748841e-002 6.363412e+001 8.337556e-002 6.459827e+001 8.084772e-002 6.556242e+001 7.920804e-002 6.652657e+001 7.851426e-002 6.749073e+001 7.832830e-002 6.845488e+001 7.844628e-002 6.941904e+001 7.899105e-002 7.038319e+001 7.968573e-002 7.134734e+001 8.041252e-002 7.231149e+001 8.127169e-002 7.327565e+001 8.153850e-002 7.423980e+001 8.078517e-002 7.520395e+001 7.909670e-002 7.616811e+001 7.720000e-002 7.713226e+001 7.540316e-002 7.809641e+001 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