#------------------------------------------------------------------------------ #$Date: 2018-09-06 11:24:34 +0300 (Thu, 06 Sep 2018) $ #$Revision: 1277 $ #$URL: svn://172.16.1.111/rod/cif/3/50/02/3500216.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500216 loop_ _publ_author_name 'Kumar, A.' 'Cassetta, M.' 'El Mendili, Y.' 'Zanatta, M.' 'Daldosso, N.' 'Mariotto, G.' _publ_section_title ; Raman spectrum of commercial Al2O3 ; _journal_name_full 'Personal communication to ROD' _journal_year 2018 _chemical_compound_source 'commercial powder Alfa Aesar 99%' _chemical_formula_structural 'O3 Al2' _chemical_formula_sum 'Al2 O3' _chemical_name_mineral Corundum _chemical_name_systematic 'Aluminium oxide' _space_group_IT_number 167 _symmetry_cell_setting trigonal _symmetry_space_group_name_Hall '-R 3 2"c' _symmetry_space_group_name_H-M 'R -3 c :H' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_formula_units_Z 6 _cell_length_a 4.7606(5) _cell_length_b 4.7606(5) _cell_length_c 12.994(1) _cod_original_formula_sum 'O3 Al2' _raman_determination_method experimental _[local]_chemical_compound_color Brown _[local]_chemical_compound_state Solid _raman_measurement_device.location 'University of Verona' _raman_measurement_device.company Horiba _raman_measurement_device.model LabRamHR800 _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.50 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 633 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 1 _raman_measurement_device.power_on_sample 0.6 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1.5 _raman_measurement_device.diffraction_grating 600 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 50 _raman_measurement.datetime_initiated 2018-01-22 _rod_data_source.file alphaAl2O3.rod.txt _rod_data_source.block 0000001 _rod_database.code 3500216 loop_ _raman_complementary.id _raman_complementary.method 1 EDX loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 silicon_wafer loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 1000017 COD http://www.crystallography.net/cod/1000017.html ; no XRD analysis data. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 150.04601 34993.398 151.323 22122.801 152.59801 14905.2 153.87399 10743.4 155.151 8082.7998 156.425 6259.7998 157.701 5018.7998 158.97701 4191.3999 160.25101 3466.3999 161.526 3017.8 162.80099 2643.6001 164.075 2286.8 165.349 2023.4 166.62399 1856 167.896 1680.6 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247.698 843.59998 248.959 845.20001 250.218 894.79999 251.47701 869.59998 252.73599 912.20001 253.995 918.79999 255.25301 962 256.51199 937 257.76999 980.79999 259.02802 1036.8 260.28699 1034.6 261.54501 1077.4 262.802 1158.2 264.05899 1190 265.31601 1275.8 266.573 1346 267.82901 1458.4 269.086 1579.8 270.34201 1731.6 271.59799 1968.8 272.853 2238.6001 274.10901 2631.3999 275.36401 3131 276.61899 3938.3999 277.87399 5181.2002 279.129 7176.6001 280.383 10529.8 281.638 15754.2 282.89001 22277 284.14401 26890.4 285.39801 26959 286.651 23218.4 287.905 17777 289.15799 12658.6 290.41 8924 291.66299 6431.6001 292.91599 5038.3999 294.168 4197.2002 295.418 3821.2 296.67001 3728.6001 297.922 3853.8 299.173 4266.6001 300.42499 4916.6001 301.67599 5886 302.92499 6919 304.17599 7593.2002 305.42599 7460 306.677 6812.6001 307.927 5943.6001 309.17499 5090.2002 310.42499 4344.6001 311.67401 3771.3999 312.923 3212.6001 314.17099 2780 315.42001 2484.3999 316.668 2213.2 317.91699 1992.8 319.16299 1830.8 320.41101 1675.6 321.659 1570.2 322.905 1510.6 324.15302 1449.6 325.39999 1387.6 326.647 1293 327.89301 1282.2 329.13901 1197.2 330.384 1200.2 331.63 1155.2 332.87601 1133.8 334.121 1102.6 335.366 1096 336.612 1081.2 337.85599 1052 339.10101 1029.6 340.34399 1000.8 341.58899 1015 342.83301 995.79999 344.07599 952.79999 345.32001 950.20001 346.56201 939 347.806 949 349.048 951.79999 350.29099 976.40002 351.53201 959.40002 352.77499 973 354.01599 1006.2 355.259 1008 356.5 983.40002 357.742 966.59998 358.98199 935.40002 360.224 916.40002 361.46399 895.20001 362.70499 908.79999 363.944 894 365.185 898.79999 366.42401 921.40002 367.66299 925.20001 368.90399 917 370.142 948.40002 371.38199 943.79999 372.62 942.79999 373.858 981.20001 375.09698 968.40002 376.33499 1009.0667 377.57401 1050 378.811 1050.8 380.048 1061.2 381.28601 1080.6 382.52301 1112.6 383.759 1118.4 384.99701 1158.2 386.233 1181.8 387.46799 1239 388.70401 1318.4 389.94101 1343.2 391.17599 1423 392.41101 1515.6 393.647 1653 394.88199 1811.8 396.116 2035.8 397.35101 2349.6001 398.58499 2838.2 399.82001 3433 401.05301 4267.6001 402.28699 5372.2002 403.51999 6475.3999 404.755 7176.6001 405.987 7051.6001 407.22 6345.7998 408.452 5226.3999 409.685 4142.7998 410.91699 3327.2 412.14899 2729.3999 413.38199 2324.3999 414.61301 2000.6 415.84399 1749 417.07501 1595.8 418.306 1480.8 419.53699 1386.4 420.767 1286.6 421.99799 1259 423.228 1201.6 424.45901 1206.6 425.689 1139.8 426.918 1134 428.147 1123.4 429.37601 1131.6 430.60501 1090.4 431.83401 1129.6 433.06299 1125.2 434.29099 1099.8 435.51901 1123.6 436.74701 1137.2 437.97501 1142.6 439.202 1159.2 440.42899 1165.4 441.65601 1186.4 442.883 1185.2 444.10999 1213.2 445.33499 1252.4 446.56201 1254.4 447.78799 1292.2 449.01401 1330.4 450.23901 1380.6 451.465 1435.4 452.69 1486.8 453.91501 1555.2 455.14001 1618.4 456.36499 1670.2 457.58801 1750 458.81299 1858.8 460.03699 1919 461.26099 2075.3999 462.48499 2226 463.70801 2351.6001 464.92999 2585.8 466.15302 2804.3999 467.37601 3099.8 468.599 3438.6001 469.82001 3787.6001 471.043 4232.3999 472.26501 4683.3999 473.487 5180 474.70901 5669 475.92899 6191.7998 477.151 6646 478.37201 7252.2002 479.59201 7689 480.81201 7977.3999 482.03299 8172 483.254 8070.3999 484.47198 7851.3999 485.69299 7427.7998 486.91199 7008.6001 488.13101 6390.2002 489.35001 5849.2002 490.56799 5319.3999 491.78699 4843.3999 493.00601 4506.7998 494.22299 4082.6001 495.44199 3849.2 496.66 3602.3999 497.87701 3495.8 499.095 3308 500.311 3187.2 501.52899 3093.2 502.745 3073.2 503.96201 3013.2 505.17899 3007.3999 506.39401 3028 507.61099 3014.2 508.82599 3031.2 510.04199 3082.6001 511.25699 3204.2 512.47302 3314.3999 513.68701 3465.6001 514.90198 3689.2 516.11603 3864.8 517.33099 4185.3999 518.54498 4517.6001 519.75897 4861.7998 520.97198 5375.6001 522.185 5800.6001 523.39899 6364.6001 524.612 6813.7998 525.82501 7290 527.03802 7535.7998 528.24902 7595.6001 529.46301 7482.3999 530.67401 7225 531.88702 6727.6001 533.09802 6239 534.30902 5609 535.521 5052 536.73199 4599.6001 537.94202 4168.6001 539.15399 3767.3999 540.36298 3446 541.573 3189 542.784 2997.6001 543.99402 2729.2 545.203 2626.8 546.41199 2435.3999 547.62201 2337.8 548.83099 2238 550.039 2180 551.24701 2108.6001 552.45697 2055.2 553.66498 1984 554.87201 1906.2 556.08002 1869.2 557.289 1822.2 558.49597 1760.2 559.703 1707.8 560.909 1697.2 562.11603 1660.4 563.32202 1606.8 564.53003 1598.4 565.73602 1556.6 566.94202 1556.8 568.14697 1507.6 569.35303 1506.6 570.55798 1465 571.763 1462.4 572.96802 1454.8 574.17401 1436.6 575.37799 1398.4 576.58197 1435 577.78601 1369.6 578.98999 1377.8 580.19397 1348.6 581.39697 1360.6 582.60101 1331.6 583.80402 1313.2 585.00702 1343.6 586.20898 1323.4 587.41199 1300 588.61401 1292.8 589.81598 1284.2 591.01801 1293.2 592.21997 1280.8 593.422 1273.2 594.62299 1290.6 595.82397 1287.6 597.02502 1330.2 598.22601 1314.2 599.427 1335.4 600.62598 1320.6 601.82599 1326.2 603.026 1345.6 604.22601 1349 605.42603 1376.2 606.625 1350.2 607.82397 1339.2 609.02301 1353.2 610.22101 1340.8 611.41998 1340.6 612.61798 1325.6 613.81702 1359.6 615.01501 1337 616.21301 1333.8 617.409 1295.4 618.60699 1300.8 619.80402 1347.2 621.00098 1313.8 622.19702 1352 623.39398 1327.2 624.591 1336.4 625.78699 1332.4 626.98199 1329.8 628.17798 1365.6 629.37402 1372.2 630.57001 1413 631.76398 1404.6 632.95898 1443.4 634.15399 1472.2 635.34802 1464.2 636.54199 1531.8 637.737 1527.4 638.92999 1585.2 640.12402 1601.8 641.31799 1661.8 642.51099 1687.8 643.70398 1765 644.896 1824.6 646.09003 1903.8 647.28302 1944.8 648.474 1982.2 649.66699 2010.4 650.85797 2033.4 652.04999 2119.2 653.24103 2175 654.43298 2188.8 655.62299 2194.8 656.815 2209 658.00598 2222 659.19598 2193.8 660.38702 2221 661.57703 2223.2 662.76599 2228.2 663.95599 2221.2 665.14502 2257 666.33502 2245 667.52399 2300.3999 668.71399 2337.2 669.90198 2393.3999 671.091 2450.6001 672.27899 2488.8 673.466 2596.6001 674.65503 2716 675.84198 2848.6001 677.03101 3015.6001 678.21802 3094.8 679.40399 3324.8 680.59198 3505.2 681.77802 3760.6001 682.96399 4034.2 684.15198 4345.3999 685.33698 4737.6001 686.52301 5177.2002 687.71002 5698.2002 688.89502 6227.7998 690.08002 6980 691.26599 7735.2002 692.45001 8495.4004 693.63501 9451.7998 694.81897 10591.6 696.00403 11686.2 697.18799 12670.6 698.37201 13717.6 699.55499 14528.8 700.73901 15140 701.92297 15198.8 703.10602 15223.6 704.289 14486.8 705.47101 13646.2 706.65399 12646.4 707.83698 11501.4 709.01898 10289.8 710.20099 9179.4004 711.383 8243.2002 712.56403 7224 713.745 6484.3999 714.927 5825.6001 716.10901 5207.2002 717.289 4773 718.46997 4367.3999 719.65002 4011.8 720.83002 3625.3999 722.01001 3338.3999 723.19 3133 724.37 2940.6001 725.54901 2750.2 726.72803 2563.6001 727.90698 2413.8 729.086 2303 730.26501 2155 731.44299 2093 732.62201 2002.8 733.79999 1897 734.97803 1855.4 736.15503 1780.4 737.33301 1739.6 738.51001 1648.4 739.68799 1577 740.86499 1545.4 742.04102 1499.6 743.21802 1452.4 744.39502 1375.8 745.56897 1357.6 746.745 1331.4 747.92102 1281.4 749.09698 1274.4 750.27301 1251.4 751.448 1209 752.62299 1158 753.797 1144.2 754.97198 1135.4 756.146 1106 757.32098 1072.8 758.495 1055.6 759.66803 1029.6 760.841 1018.8 762.01501 1019 763.18903 990.40002 764.362 975.40002 765.534 1008.4 766.70697 1038.8 767.88 979.96667 769.05103 960.79999 770.22302 949.40002 771.39502 947 772.56799 946.79999 773.73798 935.20001 774.90997 940 776.08099 964.40002 777.25098 948.20001 778.422 961.79999 779.59302 955.59998 780.763 977.79999 781.93298 949 783.10199 989.20001 784.27301 984.20001 785.44299 988.79999 786.61102 1027.8 787.78101 1041 788.94897 1015.4 790.11798 1038 791.28699 1036.2 792.45502 1055.4 793.62402 1078.2 794.79102 1095.6 795.95898 1097.8 797.12598 1103 798.29401 1102.8 799.461 1091.8 800.62799 1091.8 801.79498 1083.4 802.96198 1073.8 804.12799 1078.8 805.29498 1066.4 806.46002 1064.2 807.62701 1048.6 808.79199 1059.8 809.95599 1006 811.12299 1012.8 812.28699 957 813.453 957.79999 814.617 952.79999 815.78101 922.59998 816.94598 908.59998 818.10999 902.20001 819.27301 868.20001 820.43799 875.40002 821.60101 853.79999 822.763 830.79999 823.92798 839.59998 825.09003 818.59998 826.25201 825 827.41602 802.79999 828.578 804 829.73999 792.20001 830.901 801.20001 832.06403 781.20001 833.22498 790.79999 834.38599 800.79999 835.547 762.59998 836.70898 785.40002 837.87 769.59998 839.03003 775.59998 840.19 767.20001 841.34998 784.59998 842.51202 780 843.67102 774.59998 844.83099 774.79999 845.98999 764.79999 847.14899 764.79999 848.30798 766.79999 849.46802 770 850.62701 770.59998 851.78497 763.59998 852.94299 750.59998 854.10101 748.40002 855.25897 748.79999 856.41699 748.20001 857.57397 742.79999 858.73102 749 859.888 736.40002 861.04498 750 862.20203 739.40002 863.35901 726 864.51501 724.40002 865.67102 712.79999 866.82703 727.79999 867.98297 715.59998 869.13898 701.59998 870.29401 689 871.45001 703.79999 872.60498 694.20001 873.76001 687.40002 874.91498 689 876.06897 697.20001 877.224 684.40002 878.37799 680.59998 879.53198 659.59998 880.68597 687.59998 881.84003 656.59998 882.992 687.20001 884.14502 653 885.29797 672.59998 886.45099 660.79999 887.604 675 888.75702 669.40002 889.90802 658 891.06 651.79999 892.21198 663 893.36401 671.79999 894.51599 667.20001 895.66602 657 896.81799 672.40002 897.96899 652.59998 899.12 646.59998 900.26898 656.40002 901.41998 667.79999 902.57098 664.79999 903.72101 653.79999 904.87 660.79999 906.02002 695.20001 907.16998 658 908.31799 670.79999 909.46698 676.79999 910.617 654.20001 911.76398 661.20001 912.91302 656.59998 914.06201 672.40002 915.20898 686.20001 916.35797 688 917.50403 707.40002 918.65198 705.59998 919.79999 694.20001 920.94702 717.79999 922.09399 711.79999 923.23999 718.20001 924.38702 733.40002 925.53302 716.79999 926.67999 726.59998 927.82501 738.20001 928.97101 762.79999 930.11603 766 931.26202 739.20001 932.40698 760.59998 933.55298 775.79999 934.69702 772.59998 935.84198 777.59998 936.98602 801.59998 938.13098 809 939.27502 810.59998 940.41901 828.40002 941.56201 835.20001 942.70502 844.79999 943.84998 863.40002 944.992 854.40002 946.13599 886.79999 947.27802 903.20001 948.41998 911.79999 949.56403 911.79999 950.70502 918.20001 951.84698 909.59998 952.98999 927 954.13098 907.59998 955.27197 913.20001 956.414 948.40002 957.55499 954.20001 958.69501 959 959.83698 973.20001 960.97699 981.20001 962.117 994.40002 963.25702 977 964.39801 939.20001 965.53699 953.79999 966.677 953 967.81598 937.20001 968.95502 934.79999 970.09497 895 971.23401 894.20001 972.37201 887.79999 973.51001 871.59998 974.64801 879.20001 975.78601 884 976.92499 874.79999 978.06299 917.79999 979.20001 926.79999 980.33698 920 981.474 960.20001 982.61102 980.79999 983.74799 1010.8 984.88397 1115.6 986.021 1250.2 987.15698 1426.6 988.29303 1789.4 989.42902 2414 990.565 3883.8 991.70099 7398.3999 992.836 15151.6 993.97101 23402 995.10602 23294.801 996.24103 15996.6 997.37598 9123.5996 998.50897 5371.6001 999.64301 3685 1000.78 2798.8 1001.91 2327.8 1003.04 2104.6001 1004.18 1879.2 1005.31 1702 1006.44 1615 1007.58 1528.6 1008.71 1511.6 1009.84 1426 1010.98 1400.4 1012.11 1389.6 1013.24 1377.8 1014.37 1358 1015.5 1360.6 1016.63 1349 1017.77 1352 1018.9 1329.8 1020.03 1326.6 1021.16 1343.4 1022.29 1335.8 1023.42 1362.4 1024.55 1331 1025.6801 1373.4 1026.8101 1360.6 1027.9399 1351.2 1029.0699 1339.2 1030.2 1317.2 1031.33 1333.8 1032.45 1303 1033.58 1293 1034.71 1305.2 1035.84 1283.2 1036.97 1270.4 1038.1 1271.6 1039.22 1262.4 1040.35 1216.2 1041.48 1193.6 1042.6 1193.8 1043.73 1152 1044.86 1132.6 1045.99 1104 1047.11 1092.8 1048.24 1058.2 1049.36 1048.6 1050.49 1031.2 1051.62 1016.2 1052.74 989.59998 1053.87 971.20001 1054.99 944.40002 1056.12 941.59998 1057.24 913.20001 1058.37 908.59998 1059.49 881 1060.61 872.40002 1061.74 861.40002 1062.86 818.40002 1063.99 821.20001 1065.11 818.79999 1066.23 814.59998 1067.36 798.40002 1068.48 774.40002 1069.6 760.40002 1070.72 744 1071.85 735.59998 1072.97 735.20001 1074.09 733 1075.21 716.59998 1076.33 696.40002 1077.45 689.40002 1078.58 685.20001 1079.7 686.40002 1080.8199 661 1081.9399 659 1083.0601 663 1084.1801 647 1085.3 643.20001 1086.42 639.79999 1087.54 635.20001 1088.66 627 1089.78 628.40002 1090.9 626.20001 1092.02 628 1093.14 613.79999 1094.25 618.79999 1095.37 591.79999 1096.49 596.59998 1097.61 592.40002 1098.73 608.59998 1099.85 595.79999 1100.96 587.20001 1102.08 591.20001 1103.2 558.40002 1104.3101 561.59998 1105.4301 576.20001 1106.55 578.79999 1107.67 579.20001 1108.78 557.20001 1109.9 557.20001 1111.01 566.79999 1112.13 552.79999 1113.24 548 1114.36 546.59998 1115.48 543 1116.59 530.79999 1117.71 541.59998 1118.8199 529 1119.9301 510.20001 1121.05 515.40002 1122.16 521 1123.28 506 1124.39 516 1125.51 531.79999 1126.62 506.39999 1127.73 511 1128.84 493.20001 1129.96 501.60001 1131.0699 490.79999 1132.1801 489.60001 1133.29 499.39999 1134.41 488.39999 1135.52 490.60001 1136.63 493 1137.74 485.20001 1138.85 477.60001 1139.97 482.39999 1141.08 466.20001 1142.1899 463.39999 1143.3 460.20001 1144.41 470.79999 1145.52 490.20001 1146.63 447 1147.74 448.79999 1148.85 438 1149.96 450.39999 1151.0699 457.39999 1152.1801 448.60001 1153.29 451.39999 1154.39 428 1155.5 431.60001 1156.61 433.79999 1157.72 447.39999 1158.83 446.79999 1159.9399 419.20001 1161.04 427.60001 1162.15 443.60001 1163.26 428.60001 1164.37 414.20001 1165.47 429.79999 1166.58 431.20001 1167.6899 420.20001 1168.79 423.39999 1169.9 432 1171.01 417.20001 1172.11 411.79999 1173.22 411 1174.3199 410 1175.4301 403.60001 1176.54 411.20001 1177.64 407.20001 1178.75 411.79999 1179.85 414.79999 1180.95 402.60001 1182.0601 400 1183.16 382.39999 1184.27 398.60001 1185.37 405.39999 1186.48 410.39999 1187.58 382 1188.6801 376.20001 1189.78 386 1190.89 384.39999 1191.99 380.79999 1193.09 404.79999 1194.2 388.39999 1195.3 386.39999 1196.4 379.20001 1197.5 386 1198.6 376.39999 1199.71 383.79999 1200.8101 374.60001 1201.91 395.60001 1203.01 375.20001 1204.11 390.79999 1205.21 376.60001 1206.3101 379.79999 1207.41 389.39999 1208.51 383.60001 1209.61 375.39999 1210.71 380.39999 1211.8101 377.39999 1212.91 385.79999 1214.01 384.79999 1215.11 385.79999 1216.21 384 1217.3101 375 1218.4 385.20001 1219.5 383.39999 1220.6 386.20001 1221.7 391.20001 1222.8 388 1223.89 387.79999 1224.99 383.20001 1226.09 385.79999 1227.1899 372 1228.28 375.79999 1229.38 381 1230.48 371.79999 1231.5699 374 1232.67 368.60001 1233.76 375.20001 1234.86 377.79999 1235.96 377 1237.05 366.60001 1238.15 351.20001 1239.24 368.20001 1240.34 375.39999 1241.4301 378 1242.53 379 1243.62 372.79999 1244.71 390.39999 1245.8101 372.20001 1246.9 378 1248 369 1249.09 367.39999 1250.1801 349.20001 1251.28 377 1252.37 382.20001 1253.46 408.60001 1254.5601 374.39999 1255.65 366.39999 1256.74 364.60001 1257.83 378.39999 1258.92 363.79999 1260.02 368.39999 1261.11 384.39999 1262.2 363.20001 1263.29 373.79999 1264.38 381.60001 1265.47 367 1266.5601 372.79999 1267.65 372.20001 1268.74 377.39999 1269.83 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