#------------------------------------------------------------------------------ #$Date: 2018-09-06 12:05:33 +0300 (Thu, 06 Sep 2018) $ #$Revision: 1285 $ #$URL: svn://172.16.1.111/rod/cif/3/50/02/3500222.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500222 loop_ _publ_author_name 'Kumar, A.' 'Cassetta, M.' 'El Mendili, Y.' 'Zanatta, M.' 'Daldosso, N.' 'Mariotto, G.' _publ_section_title ; Raman spectrum of commercial B2O3 ; _journal_name_full 'Personal communication to ROD' _journal_year 2018 _chemical_compound_source 'Commercial powder Alfa Aesar 99.98%' _chemical_formula_structural 'B2 O3' _chemical_formula_sum 'B2 O3' _chemical_name_mineral 'Boron trioxide' _chemical_name_systematic 'Boron trioxide' _space_group_crystal_system trigonal _space_group_IT_number 152 _space_group_name_Hall 'P 31 2"' _space_group_name_H-M_alt 'P 31 2 1' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_formula_units_Z 3 _cell_length_a 4.3358 _cell_length_b 4.3358 _cell_length_c 8.3397 _cell_volume 135.775 _raman_determination_method experimental _[local]_chemical_compound_color white _[local]_chemical_compound_state Solid _raman_measurement_device.location 'University of Verona' _raman_measurement_device.company Horiba _raman_measurement_device.model LabRamHR800 _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.50 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 633 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 1 _raman_measurement_device.power_on_sample 6 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1.5 _raman_measurement_device.diffraction_grating 600 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 50 _raman_measurement.datetime_initiated 2018-01-23 _rod_data_source.file B2O3.txt _rod_data_source.block 0000001 _rod_database.code 3500222 loop_ _raman_complementary.id _raman_complementary.method 1 EDX loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 silicon_wafer loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 1510796 COD http://www.crystallography.net/cod/1510796.html ; no XRD analysis data. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 150.04601 586.40002 151.323 550.20001 152.59801 551.40002 153.87399 556.79999 155.151 536.79999 156.425 544.40002 157.701 532.79999 158.97701 529.79999 160.25101 516.79999 161.526 525.59998 162.80099 544.20001 164.075 545.59998 165.349 523.40002 166.62399 538.40002 167.896 548.59998 169.17101 540.40002 170.44299 544.59998 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495.79999 1033.58 516.40002 1034.71 499 1035.84 496.20001 1036.97 500.39999 1038.1 501.79999 1039.22 498.79999 1040.35 508.79999 1041.48 497.79999 1042.6 515.40002 1043.73 513.59998 1044.86 493 1045.99 508.20001 1047.11 499.39999 1048.24 504.20001 1049.36 502.39999 1050.49 508.20001 1051.62 510.20001 1052.74 500 1053.87 506 1054.99 492.20001 1056.12 501.20001 1057.24 507.20001 1058.37 506.20001 1059.49 512.59998 1060.61 510 1061.74 515 1062.86 504 1063.99 514.59998 1065.11 499.79999 1066.23 502.20001 1067.36 506.20001 1068.48 508.20001 1069.6 495.20001 1070.72 509 1071.85 501.79999 1072.97 492 1074.09 518.20001 1075.21 498.60001 1076.33 500.39999 1077.45 495.79999 1078.58 491.79999 1079.7 506.39999 1080.8199 503.60001 1081.9399 498.20001 1083.0601 509.39999 1084.1801 526.79999 1085.3 508.39999 1086.42 514 1087.54 501.79999 1088.66 505.20001 1089.78 521.40002 1090.9 516.59998 1092.02 503.60001 1093.14 525.40002 1094.25 518 1095.37 511.79999 1096.49 501.79999 1097.61 517.59998 1098.73 512.59998 1099.85 517.20001 1100.96 521 1102.08 504.79999 1103.2 513.79999 1104.3101 508.79999 1105.4301 493.60001 1106.55 508.39999 1107.67 521 1108.78 516.79999 1109.9 502.20001 1111.01 512.20001 1112.13 493.79999 1113.24 512.79999 1114.36 522 1115.48 501.60001 1116.59 496.79999 1117.71 514.59998 1118.8199 525.20001 1119.9301 513.59998 1121.05 525 1122.16 525 1123.28 513 1124.39 536.59998 1125.51 531 1126.62 522.79999 1127.73 508.60001 1128.84 511.39999 1129.96 520.59998 1131.0699 520 1132.1801 509.39999 1133.29 507.20001 1134.41 508.79999 1135.52 510.20001 1136.63 527.40002 1137.74 521.59998 1138.85 520.20001 1139.97 530.59998 1141.08 510.20001 1142.1899 525.40002 1143.3 533.79999 1144.41 524.40002 1145.52 520.79999 1146.63 534.79999 1147.74 524 1148.85 530 1149.96 521.59998 1151.0699 541.20001 1152.1801 552.40002 1153.29 528.20001 1154.39 541.79999 1155.5 548 1156.61 570.40002 1157.72 564.40002 1158.83 584.79999 1159.9399 595.20001 1161.04 606 1162.15 622.20001 1163.26 651.40002 1164.37 675.79999 1165.47 702.59998 1166.58 749.20001 1167.6899 739 1168.79 739 1169.9 730.79999 1171.01 708.79999 1172.11 664.59998 1173.22 649 1174.3199 619.79999 1175.4301 582.79999 1176.54 568.40002 1177.64 558.59998 1178.75 557.59998 1179.85 536.40002 1180.95 542.40002 1182.0601 544.40002 1183.16 540.59998 1184.27 548 1185.37 540.20001 1186.48 531.20001 1187.58 546.40002 1188.6801 536.40002 1189.78 538.79999 1190.89 534 1191.99 545.59998 1193.09 511.20001 1194.2 542 1195.3 520.20001 1196.4 525.20001 1197.5 530.40002 1198.6 531.20001 1199.71 527.79999 1200.8101 530 1201.91 532.40002 1203.01 516.79999 1204.11 520 1205.21 545.79999 1206.3101 504.60001 1207.41 524.20001 1208.51 523.40002 1209.61 519.79999 1210.71 519.40002 1211.8101 529.20001 1212.91 533.20001 1214.01 528.79999 1215.11 540.79999 1216.21 534 1217.3101 535.40002 1218.4 527.59998 1219.5 532.40002 1220.6 532.59998 1221.7 533.40002 1222.8 532 1223.89 534.79999 1224.99 531.20001 1226.09 543 1227.1899 523.40002 1228.28 528 1229.38 525.79999 1230.48 523.59998 1231.5699 521.20001 1232.67 523.79999 1233.76 529.20001 1234.86 529.79999 1235.96 522 1237.05 535.79999 1238.15 536.79999 1239.24 532.59998 1240.34 520 1241.4301 524.20001 1242.53 548.79999 1243.62 538.79999 1244.71 528.20001 1245.8101 521 1246.9 527 1248 523.20001 1249.09 540.79999 1250.1801 523.59998 1251.28 532 1252.37 545.79999 1253.46 553.79999 1254.5601 531 1255.65 540.40002 1256.74 527.79999 1257.83 543.79999 1258.92 539.59998 1260.02 536 1261.11 544 1262.2 534.20001 1263.29 535.79999 1264.38 546.40002 1265.47 536.79999 1266.5601 528 1267.65 534.20001 1268.74 546.59998 1269.83 548 1270.92 532.20001 1272.01 547 1273.1 547 1274.1899 539.40002 1275.28 562.59998 1276.37 535.79999 1277.46 556 1278.55 539.79999 1279.64 550.79999 1280.73 538.40002 1281.8199 526.59998 1282.9 563 1283.99 553.20001 1285.08 553.59998 1286.17 555 1287.25 537.20001 1288.34 553.59998 1289.4301 540.59998 1290.51 547.79999 1291.6 552.20001 1292.6899 560 1293.77 552.20001 1294.86 553.20001 1295.95 544.59998 1297.03 541.40002 1298.12 551 1299.2 539.59998