#------------------------------------------------------------------------------ #$Date: 2018-09-06 13:06:21 +0300 (Thu, 06 Sep 2018) $ #$Revision: 1302 $ #$URL: svn://172.16.1.111/rod/cif/3/50/02/3500239.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500239 loop_ _publ_author_name 'Kumar, A.' 'Cassetta, M.' 'El Mendili, Y.' 'Zanatta, M.' 'Daldosso, N.' 'Mariotto, G.' _publ_section_title ; Raman spectrum of commercial H3BO3 ; _journal_name_full 'Personal communication to ROD' _journal_year 2018 _chemical_compound_source 'commercial Prolabo 99%' _chemical_formula_structural 'B H3 O3' _chemical_formula_sum 'B H3 O3' _chemical_name_mineral 'Boric acid' _chemical_name_systematic 'orthoboric acid' _space_group_IT_number 145 _symmetry_cell_setting trigonal _symmetry_space_group_name_Hall 'P 32' _symmetry_space_group_name_H-M 'P 32' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_formula_units_Z 6 _cell_length_a 7.0453(4) _cell_length_b 7.0453(4) _cell_length_c 9.5608(7) _raman_determination_method experimental _[local]_chemical_compound_color white _[local]_chemical_compound_state Solid _raman_measurement_device.location 'University of Verona' _raman_measurement_device.company Horiba _raman_measurement_device.model 'LabRamHR800_raman_measurement_device.optics_type microscope' _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.50 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 633 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 1 _raman_measurement_device.power_on_sample 6 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1.5 _raman_measurement_device.diffraction_grating 600 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 50 _raman_measurement.datetime_initiated 2018-01-22 _rod_data_source.file H3BO3.txt _rod_data_source.block 0000001 _rod_database.code 3500239 loop_ _raman_complementary.id _raman_complementary.method 1 EDX loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 silicon_wafer loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 2013259 COD http://www.crystallography.net/cod/2013259.html ; no XRD analysis data. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 150.04601 523 151.323 467.79999 152.59801 474.60004 153.87399 451.20001 155.151 445.60004 156.425 446.19998 157.701 432.79999 158.97701 436.20001 160.25101 425.39999 161.526 421.00003 162.80099 410.59998 164.075 404.19998 165.349 410.60001 166.62399 409.00003 167.896 409 169.17101 403.20001 170.44299 404.60001 171.716 409.79999 172.98801 414.00003 174.26199 407 175.535 412.39999 176.806 423.60004 178.078 434 179.349 443.99997 180.621 462.20001 181.892 470.60001 183.164 478.79999 184.43401 504 185.705 532.20001 186.97501 517.79999 188.246 476.20001 189.515 471.20004 190.785 437.39999 192.054 434 193.32401 439.19998 194.593 435.39996 195.862 433.00003 197.13 444.00003 198.39799 443 199.66701 472.39999 200.93401 495.59998 202.203 530.59998 203.47 558 204.737 630.59998 206.005 706.59998 207.271 790.59991 208.539 846.20001 209.80499 882.40002 211.07001 831.00006 212.33701 798 213.603 711.19995 214.868 643.20001 216.134 573 217.399 521.79999 218.66299 501.00003 219.929 488.60001 221.19299 460.79996 222.457 446.79999 223.72099 454 224.98599 446.60001 226.24899 436.79999 227.51199 420.60001 228.776 427.60004 230.039 410 231.30099 437 232.564 405.79996 233.827 396.20001 235.089 397.00003 236.351 391 237.612 394.20001 238.873 394.20001 240.136 386 241.397 387.80002 242.657 374 243.918 378 245.17799 372.39999 246.438 372.60001 247.698 380 248.959 371.79999 250.218 389.60001 251.47701 365.19998 252.73599 371.39999 253.995 372.79999 255.25301 375.20001 256.51199 374 257.76999 378 259.02802 365.60001 260.28699 379.20001 261.54501 369 262.802 365 264.05899 368 265.31601 381 266.573 362.99997 267.82901 358.79999 269.086 369.60001 270.34201 355.79996 271.59799 360.20001 272.853 358.60001 274.10901 357.20001 275.36401 358 276.61899 354.79999 277.87399 361.79999 279.129 357.39999 280.383 357.79999 281.638 356.00003 282.89001 366.60001 284.14401 357.60004 285.39801 347.19998 286.651 356.60001 287.905 347.19998 289.15799 342 290.41 354 291.66299 362.20001 292.91599 344.60001 294.168 340.39999 295.418 356.20001 296.67001 354.20004 297.922 343.20001 299.173 356 300.42499 335.59998 301.67599 366 302.92499 344 304.17599 356 305.42599 341 306.677 341.20004 307.927 349.20001 309.17499 351.39996 310.42499 351.39999 311.67401 344 312.923 348 314.17099 336.59998 315.42001 353.40002 316.668 346.39999 317.91699 361.79996 319.16299 331.20001 320.41101 346.20001 321.659 356 322.905 353.20001 324.15302 345 325.39999 355.20001 326.647 336.59998 327.89301 348.00003 329.13901 349.60001 330.384 357.20001 331.63 343.40002 332.87601 342 334.121 346 335.366 348.20001 336.612 359.39999 337.85599 335.20001 339.10101 344.39999 340.34399 343.40002 341.58899 349.60001 342.83301 338.59998 344.07599 340.60001 345.32001 342.60001 346.56201 363.60001 347.806 353.79996 349.048 371.20004 350.29099 360.79999 351.53201 343 352.77499 342.20004 354.01599 345.79999 355.259 339 356.5 350.20004 357.742 354.39999 358.98199 335.20001 360.224 335.99997 361.46399 349 362.70499 346.20001 363.944 339.59998 365.185 347.40002 366.42401 342 367.66299 352.20001 368.90399 346.19998 370.142 340 371.38199 352.39999 372.62 340.60001 373.858 337.39999 375.09698 367.60004 376.33499 369.39999 377.57401 355.20001 378.811 346.40002 380.048 359.20001 381.28601 340 382.52301 355.79999 383.759 352.79996 384.99701 340.20001 386.233 342.39999 387.46799 350.39999 388.70401 337.79996 389.94101 360.39999 391.17599 361.20001 392.41101 347.39999 393.647 347 394.88199 358.39999 396.116 348 397.35101 347.39999 398.58499 344 399.82001 351.60004 401.05301 356.20001 402.28699 341.19998 403.51999 361.79999 404.755 355 405.987 360.60001 407.22 365.80002 408.452 350.20001 409.685 358.39999 410.91699 350.40002 412.14899 356.79999 413.38199 341.39999 414.61301 350.79999 415.84399 359.39999 417.07501 348.79999 418.306 348.20001 419.53699 351.60004 420.767 362.39999 421.99799 343.20001 423.228 349.39999 424.45901 353.60001 425.689 353 426.918 349.20001 428.147 344.60004 429.37601 357 430.60501 339.59998 431.83401 355.20004 433.06299 350.79999 434.29099 366.79996 435.51901 355.79996 436.74701 368 437.97501 356 439.202 362 440.42899 347.60001 441.65601 351.79999 442.883 360.20001 444.10999 357 445.33499 366.80002 446.56201 366.60001 447.78799 357.39996 449.01401 354.80002 450.23901 362 451.465 362 452.69 353.79999 453.91501 351.39999 455.14001 369.60001 456.36499 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385.79996 711.383 367 712.56403 373.60001 713.745 375.39999 714.927 366 716.10901 387.79999 717.289 386.39999 718.46997 384.39999 719.65002 385.60001 720.83002 380.59998 722.01001 377 723.19 375.39999 724.37 393.79996 725.54901 377.79999 726.72803 373.79999 727.90698 400.60001 729.086 385.20001 730.26501 383.39999 731.44299 389.39999 732.62201 386.60001 733.79999 385.60001 734.97803 391.79999 736.15503 395.39999 737.33301 393.79996 738.51001 386.39999 739.68799 380.79999 740.86499 393 742.04102 384.39999 743.21802 378.20004 744.39502 387.06665 745.56897 384.1861 746.745 369.79999 747.92102 382.39999 749.09698 381.79999 750.27301 366.20001 751.448 393.60001 752.62299 391.20001 753.797 387.20001 754.97198 383.99997 756.146 371.60001 757.32098 390.20001 758.495 366.60001 759.66803 355.79999 760.841 362.39999 762.01501 375.19998 763.18903 369.60004 764.362 372.39999 765.534 373.60001 766.70697 380 767.88 382.39999 769.05103 381 770.22302 376.79999 771.39502 372.20001 772.56799 376 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836.70898 402.79999 837.87 387.60001 839.03003 392.60001 840.19 402.79999 841.34998 399.99997 842.51202 409.79999 843.67102 407 844.83099 410.20001 845.98999 414.40002 847.14899 412.60001 848.30798 423.99997 849.46802 409.60001 850.62701 417.99997 851.78497 428.20001 852.94299 422.80002 854.10101 442.39999 855.25897 438.20004 856.41699 442.79996 857.57397 471.79999 858.73102 471.20001 859.888 498.20001 861.04498 502.39996 862.20203 549.40009 863.35901 556.20001 864.51501 584.79999 865.67102 598 866.82703 615.59998 867.98297 680.19995 869.13898 682 870.29401 780.20001 871.45001 836.40002 872.60498 947.00006 873.76001 1108.4 874.91498 1357.4 876.06897 1671.8 877.224 2222.2 878.37799 2997.2002 879.53198 4121.7998 880.68597 5095.3999 881.84003 5559.6006 882.992 5121 884.14502 4027.3999 885.29797 2901 886.45099 2070.2 887.604 1554.2 888.75702 1199 889.90802 1017.9999 891.06 851 892.21198 745.20001 893.36401 679.79999 894.51599 614.00006 895.66602 573.40002 896.81799 545.20001 897.96899 530.40002 899.12 493 900.26898 471.60001 901.41998 463.39999 902.57098 474.20001 903.72101 443.79999 904.87 453.00003 906.02002 466 907.16998 431.19998 908.31799 411 909.46698 416.39996 910.617 405.79996 911.76398 392.79999 912.91302 411.20001 914.06201 384.80002 915.20898 402.39999 916.35797 404.39996 917.50403 389 918.65198 390.60001 919.79999 383.59998 920.94702 386.79999 922.09399 384.20001 923.23999 387.20001 924.38702 362 925.53302 387.60001 926.67999 396.19998 927.82501 375.60001 928.97101 381.99997 930.11603 379.60001 931.26202 370.79999 932.40698 376 933.55298 385.80002 934.69702 367.60001 935.84198 380.79996 936.98602 388.60004 938.13098 368.60001 939.27502 372.20001 940.41901 375.40002 941.56201 375.39999 942.70502 378.60001 943.84998 369 944.992 373.39999 946.13599 373.79999 947.27802 382.60001 948.41998 378.60001 949.56403 379.60001 950.70502 388.39999 951.84698 378.39999 952.98999 362.79999 954.13098 375.39999 955.27197 363.59998 956.414 371.60001 957.55499 344.79999 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378 1022.29 377.20001 1023.42 374 1024.55 379.60001 1025.6801 382.39999 1026.8101 373.99997 1027.9399 382.80002 1029.0699 378 1030.2 376.60001 1031.33 379.60001 1032.45 382.20001 1033.58 379.39999 1034.71 377.00003 1035.84 371.79996 1036.97 380.60001 1038.1 382 1039.22 366.60004 1040.35 376.99997 1041.48 387.60001 1042.6 369.60001 1043.73 364 1044.86 383.79999 1045.99 391.20001 1047.11 376.39999 1048.24 372.60001 1049.36 359.60001 1050.49 376 1051.62 390 1052.74 366.79999 1053.87 385.60001 1054.99 372.60001 1056.12 383 1057.24 374.60001 1058.37 383.19998 1059.49 377 1060.61 378.79999 1061.74 377.40002 1062.86 379.39999 1063.99 388.39999 1065.11 370.20004 1066.23 374.59998 1067.36 391.20001 1068.48 383.79999 1069.6 381 1070.72 364.99997 1071.85 377.00003 1072.97 364.80002 1074.09 384.79999 1075.21 367.20001 1076.33 383.20001 1077.45 388 1078.58 371.99997 1079.7 370.60004 1080.8199 381.79999 1081.9399 380.20001 1083.0601 377.79999 1084.1801 380 1085.3 384.60001 1086.42 392.79999 1087.54 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