#------------------------------------------------------------------------------ #$Date: 2018-09-06 14:52:22 +0300 (Thu, 06 Sep 2018) $ #$Revision: 1313 $ #$URL: svn://172.16.1.111/rod/cif/3/50/02/3500250.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500250 loop_ _publ_author_name 'Kumar, A.' 'Cassetta, M.' 'El Mendili, Y.' 'Zanatta, M.' 'Daldosso, N.' 'Mariotto, G.' _publ_section_title ; Raman spectrum of commercial Nb2O5 ; _journal_name_full 'Personal communication to ROD' _journal_year 2018 _chemical_compound_source 'commercial powder Alfa Aesar 99.5%' _chemical_formula_structural 'Nb2 O5' _chemical_formula_sum 'Nb2 O5' _chemical_name_mineral Niobite _space_group_IT_number 12 _symmetry_space_group_name_Hall '-C 2y' _symmetry_space_group_name_H-M 'C 1 2/m 1' _cell_angle_alpha 90 _cell_angle_beta 120.8 _cell_angle_gamma 90 _cell_formula_units_Z 16 _cell_length_a 28.51 _cell_length_b 3.83 _cell_length_c 17.48 _raman_determination_method experimental _[local]_chemical_compound_color white _[local]_chemical_compound_state Solid _raman_measurement_device.location 'University of Verona' _raman_measurement_device.company Horiba _raman_measurement_device.model LabRamHR800 _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.50 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 633 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 1 _raman_measurement_device.power_on_sample 6 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1.5 _raman_measurement_device.diffraction_grating 600 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 50 _raman_measurement.datetime_initiated 2018-01-22 _rod_data_source.file Nb2O5.txt _rod_data_source.block 0000001 _rod_database.code 3500250 loop_ _raman_complementary.id _raman_complementary.method 1 EDX loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 silicon_wafer loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 1534156 COD http://www.crystallography.net/cod/1534156.html ; no XRD analysis data. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 150.04601 17530.6 151.323 17242.199 152.59801 17049.6 153.87399 17419.801 155.151 18718.801 156.425 19822 157.701 19935 158.97701 19328.4 160.25101 18894.801 161.526 18688.6 162.80099 18934.4 164.075 19179 165.349 19544.199 166.62399 19649.801 167.896 19878.801 169.17101 20197.4 170.44299 20432 171.716 20724.199 172.98801 20901.801 174.26199 21278.199 175.535 21622.6 176.806 21999.6 178.078 22202.199 179.349 22386.6 180.621 22585.801 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324.15302 12549.4 325.39999 12052.8 326.647 11483.4 327.89301 10997.2 329.13901 10721.2 330.384 10460.4 331.63 10214.2 332.87601 10139.2 334.121 10077.4 335.366 10151.8 336.612 10097.4 337.85599 10155.8 339.10101 10033 340.34399 9870.4004 341.58899 9921.4004 342.83301 9839.5996 344.07599 9987.4004 345.32001 10009.6 346.56201 10162.6 347.806 10037.4 349.048 9851 350.29099 9519.2002 351.53201 9175.7998 352.77499 8849.7998 354.01599 8608.7998 355.259 8340 356.5 8257.7998 357.742 8133.7998 358.98199 8101.7998 360.224 8034.7998 361.46399 8009.2002 362.70499 7988.3999 363.944 7856.6001 365.185 7806 366.42401 7691.7998 367.66299 7574.2002 368.90399 7482.7998 370.142 7364.2002 371.38199 7295.2002 372.62 7217.7998 373.858 7081.6001 375.09698 7048 376.33499 6977.7998 377.57401 6905.7998 378.811 6909 380.048 6821.6001 381.28601 6814.2002 382.52301 6838.7998 383.759 6868.3999 384.99701 6836.6001 386.233 6957.3999 387.46799 6948.6001 388.70401 6993.3999 389.94101 7054 391.17599 7142.2002 392.41101 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39950.199 660.38702 40171 661.57703 40309.602 662.76599 40160.602 663.95599 39548.398 665.14502 38923.199 666.33502 38491 667.52399 37812 668.71399 37414.801 669.90198 37151.199 671.091 37085.199 672.27899 37188 673.466 37677 674.65503 37895.602 675.84198 38242.398 677.03101 37886.801 678.21802 37069.602 679.40399 36140.801 680.59198 34923.199 681.77802 34125.602 682.96399 33270.398 684.15198 32636.6 685.33698 31966.4 686.52301 31220.4 687.71002 30476.6 688.89502 29860.6 690.08002 28902.199 691.26599 27681.4 692.45001 26749.4 693.63501 25667 694.81897 24448.801 696.00403 23448 697.18799 22417 698.37201 21424.199 699.55499 20594.6 700.73901 19576.801 701.92297 18913.801 703.10602 18194 704.289 17508 705.47101 16964.199 706.65399 16418.199 707.83698 15866.2 709.01898 15454.2 710.20099 15030.6 711.383 14670.2 712.56403 14385.6 713.745 14032.8 714.927 13704 716.10901 13321.2 717.289 12976.6 718.46997 12668.8 719.65002 12367.2 720.83002 12025.2 722.01001 11631.4 723.19 11225.4 724.37 10917.2 725.54901 10633 726.72803 10359.4 727.90698 10043.8 729.086 9739 730.26501 9494.4004 731.44299 9186.7998 732.62201 8884 733.79999 8672.5996 734.97803 8459.5996 736.15503 8253.7998 737.33301 8140 738.51001 7921.6001 739.68799 7780.3999 740.86499 7714.3999 742.04102 7498.3999 743.21802 7539.7998 744.39502 7344 745.56897 7352.3999 746.745 7242 747.92102 7177.2002 749.09698 7155.2002 750.27301 7107.6001 751.448 7135.6001 752.62299 7087.6001 753.797 7075.3999 754.97198 7122.3999 756.146 7074.6001 757.32098 7110.6001 758.495 7040.3999 759.66803 6913.6001 760.841 6781.2002 762.01501 6781 763.18903 6580 764.362 6404.6001 765.534 6239 766.70697 6095.3999 767.88 5892.6001 769.05103 5724.3999 770.22302 5615.7998 771.39502 5448.7998 772.56799 5372.3999 773.73798 5241.7998 774.90997 5151 776.08099 5104.3999 777.25098 5005.6001 778.422 4952.7998 779.59302 4876 780.763 4741.6001 781.93298 4719.7998 783.10199 4613.3999 784.27301 4545.6001 785.44299 4479.3999 786.61102 4462.7998 787.78101 4402.6001 788.94897 4305.2002 790.11798 4311.2002 791.28699 4199 792.45502 4200.2002 793.62402 4211.6001 794.79102 4147.3999 795.95898 4111 797.12598 4088.2 798.29401 4040.3999 799.461 4007.2 800.62799 4023.2 801.79498 3973.8 802.96198 3923.8 804.12799 3964.8 805.29498 3923.6001 806.46002 3930.8 807.62701 3959.3999 808.79199 3915 809.95599 3886.6001 811.12299 3949.8 812.28699 3903.8 813.453 3945.3999 814.617 3947.2 815.78101 3977.3999 816.94598 4012.8 818.10999 4005.3999 819.27301 4053.8 820.43799 4087.3999 821.60101 4175 822.763 4195.3999 823.92798 4272.7998 825.09003 4379.6001 826.25201 4447 827.41602 4502.2002 828.578 4536.2002 829.73999 4627 830.901 4729 832.06403 4798.3999 833.22498 4925.7998 834.38599 4889.6001 835.547 4962.2002 836.70898 4985.2002 837.87 4976 839.03003 5032.6001 840.19 5103.3999 841.34998 5199 842.51202 5262.3999 843.67102 5316.3999 844.83099 5454.2002 845.98999 5520.3999 847.14899 5548.3999 848.30798 5642.3999 849.46802 5622.6001 850.62701 5646.6001 851.78497 5534 852.94299 5379.3999 854.10101 5222.3999 855.25897 5042.2002 856.41699 4828.7998 857.57397 4628 858.73102 4548.7998 859.888 4286.7998 861.04498 4139.3999 862.20203 4067.2 863.35901 3942.3999 864.51501 3803.6001 865.67102 3786.8 866.82703 3685.3999 867.98297 3650 869.13898 3600.6001 870.29401 3633.2 871.45001 3602.2 872.60498 3596.8 873.76001 3649 874.91498 3616.2 876.06897 3697.3999 877.224 3721.6001 878.37799 3827 879.53198 3886 880.68597 4028.8 881.84003 4175.3999 882.992 4324.3999 884.14502 4522 885.29797 4737.3999 886.45099 5018 887.604 5293.7998 888.75702 5609.7998 889.90802 5955.7998 891.06 6236.3999 892.21198 6533.3999 893.36401 6774.3999 894.51599 6910.3999 895.66602 6933 896.81799 6968.3999 897.96899 6884.6001 899.12 6914.6001 900.26898 6895.7998 901.41998 6978.2002 902.57098 6969.7998 903.72101 6990 904.87 6913.7998 906.02002 6892.2002 907.16998 6726.3999 908.31799 6670.7998 909.46698 6469.7998 910.617 6267 911.76398 6029 912.91302 5753.2002 914.06201 5557 915.20898 5313 916.35797 5153 917.50403 4931.3999 918.65198 4790 919.79999 4666 920.94702 4564.2002 922.09399 4472.3999 923.23999 4368.6001 924.38702 4271.3999 925.53302 4206.7998 926.67999 4179.7998 927.82501 4067 928.97101 4002.2 930.11603 3890.8 931.26202 3793.3999 932.40698 3742 933.55298 3692.6001 934.69702 3619 935.84198 3610 936.98602 3573.3999 938.13098 3562.2 939.27502 3483.8 940.41901 3496.8 941.56201 3533.6001 942.70502 3499 943.84998 3553 944.992 3487.6001 946.13599 3541.6001 947.27802 3557.3999 948.41998 3634.3999 949.56403 3669.8 950.70502 3667 951.84698 3791 952.98999 3777.2 954.13098 3840.6001 955.27197 3949.8 956.414 4033.6001 957.55499 4042.3999 958.69501 4170.7998 959.83698 4254 960.97699 4361.2002 962.117 4499.7998 963.25702 4594.6001 964.39801 4816.6001 965.53699 4985.6001 966.677 5181.2002 967.81598 5413.2002 968.95502 5674.2002 970.09497 5952.2002 971.23401 6226 972.37201 6635.3999 973.51001 7092.3999 974.64801 7493 975.78601 8128 976.92499 8719.2002 978.06299 9598.2002 979.20001 10534.4 980.33698 11703.6 981.474 13206.2 982.61102 14964.8 983.74799 17138.199 984.88397 19921.801 986.021 23401.6 987.15698 27367.199 988.29303 32406.801 989.42902 37530.801 990.565 42271.398 991.70099 45587 992.836 46895.602 993.97101 45873 995.10602 42921.801 996.24103 39145.199 997.37598 34984.602 998.50897 31257.4 999.64301 27857 1000.78 24978.4 1001.91 22536.801 1003.04 20469.4 1004.18 18624.801 1005.31 16968 1006.44 15481.6 1007.58 13905.8 1008.71 12572.6 1009.84 11287.2 1010.98 9979 1012.11 8974.2002 1013.24 8100.2002 1014.37 7232.3999 1015.5 6528.7998 1016.63 5958.3999 1017.77 5451.7998 1018.9 4983 1020.03 4632.6001 1021.16 4361.3999 1022.29 4068.3999 1023.42 3857.2 1024.55 3598.2 1025.6801 3375 1026.8101 3209.2 1027.9399 3109.6001 1029.0699 2924.6001 1030.2 2787.3999 1031.33 2655.8 1032.45 2576.8 1033.58 2491 1034.71 2395.6001 1035.84 2325.8 1036.97 2250 1038.1 2169.3999 1039.22 2119 1040.35 2072.6001 1041.48 2014 1042.6 1976.6 1043.73 1946.8 1044.86 1896.6 1045.99 1851.6 1047.11 1803.6 1048.24 1763.8 1049.36 1768 1050.49 1699.4 1051.62 1676.4 1052.74 1656.4 1053.87 1639.4 1054.99 1636.2 1056.12 1597.4 1057.24 1596.2 1058.37 1585.6 1059.49 1584 1060.61 1548.4 1061.74 1531 1062.86 1521.2 1063.99 1514.4 1065.11 1497.6 1066.23 1480.8 1067.36 1471.8 1068.48 1445.2 1069.6 1448.4 1070.72 1434.2 1071.85 1426.4 1072.97 1438 1074.09 1420.4 1075.21 1387.4 1076.33 1402.8 1077.45 1374 1078.58 1375.8 1079.7 1359.6 1080.8199 1379.2 1081.9399 1330.8 1083.0601 1342.6 1084.1801 1339.2 1085.3 1329.6 1086.42 1331.2 1087.54 1315 1088.66 1300 1089.78 1329.2 1090.9 1263.2 1092.02 1292.2 1093.14 1292.6 1094.25 1281.6 1095.37 1249.4 1096.49 1294.6 1097.61 1244.6 1098.73 1284.6 1099.85 1246.6 1100.96 1242.4 1102.08 1243.8 1103.2 1230.8 1104.3101 1232 1105.4301 1392 1106.55 1230 1107.67 1219.4 1108.78 1205.8 1109.9 1247.2 1111.01 1224 1112.13 1203 1113.24 1193.6 1114.36 1191.8 1115.48 1197 1116.59 1186.4 1117.71 1200.2 1118.8199 1189.8 1119.9301 1177 1121.05 1196.8 1122.16 1176.4 1123.28 1150.8 1124.39 1175.4 1125.51 1182.4 1126.62 1145.2 1127.73 1149.4 1128.84 1147.6 1129.96 1133.6 1131.0699 1142.2 1132.1801 1133 1133.29 1138.8 1134.41 1136.2 1135.52 1128.2 1136.63 1122.8 1137.74 1103.4 1138.85 1138.8 1139.97 1095.8 1141.08 1127.6 1142.1899 1132 1143.3 1098.8 1144.41 1117 1145.52 1103.8 1146.63 1128.4 1147.74 1086.8 1148.85 1108 1149.96 1110 1151.0699 1085.8 1152.1801 1096.6 1153.29 1091.2 1154.39 1069.6 1155.5 1081.6 1156.61 1054 1157.72 1075 1158.83 1089 1159.9399 1065.4 1161.04 1095.8 1162.15 1063.6 1163.26 1077.4 1164.37 1054.2 1165.47 1069.6 1166.58 1083 1167.6899 1055.8 1168.79 1036 1169.9 1054.2 1171.01 1051.2 1172.11 1063.6 1173.22 1053.6 1174.3199 1055.4 1175.4301 1051.6 1176.54 1037.8 1177.64 1052.6 1178.75 1030.4 1179.85 1037.6 1180.95 1045 1182.0601 1022.6 1183.16 1025 1184.27 1010.8 1185.37 1007.4 1186.48 1049.2 1187.58 1010.6 1188.6801 1001.4 1189.78 1004.2 1190.89 1020.2 1191.99 1024.6 1193.09 995.20001 1194.2 1019.6 1195.3 1018.4 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