#------------------------------------------------------------------------------ #$Date: 2018-09-06 14:57:44 +0300 (Thu, 06 Sep 2018) $ #$Revision: 1318 $ #$URL: svn://172.16.1.111/rod/cif/3/50/02/3500255.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500255 loop_ _publ_author_name 'Kumar, A.' 'Cassetta, M.' 'El Mendili, Y.' 'Zanatta, M.' 'Daldosso, N.' 'Mariotto, G.' _publ_section_title ; Raman spectrum of commercial Sb2O3 ; _journal_name_full 'Personal communication to ROD' _journal_year 2018 _chemical_compound_source 'commercial Merk 99%' _chemical_formula_structural 'Sb2 O3' _chemical_formula_sum 'O3 Sb2' _chemical_name_mineral Valentinite _chemical_name_systematic Valentinite _space_group_IT_number 56 _symmetry_space_group_name_Hall '-P 2ab 2ac' _symmetry_space_group_name_H-M 'P c c n' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 12.46 _cell_length_b 4.92 _cell_length_c 5.42 _cod_original_formula_sum 'Sb2 O3' _raman_determination_method experimental _[local]_chemical_compound_color white _[local]_chemical_compound_state Solid _raman_measurement_device.location 'University of Verona' _raman_measurement_device.company Horiba _raman_measurement_device.model 'LabRamHR800_raman_measurement_device.optics_type microscope' _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.50 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 633 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 1 _raman_measurement_device.power_on_sample 6 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1.5 _raman_measurement_device.diffraction_grating 600 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 50 _raman_measurement.datetime_initiated 2018-01-22 _rod_data_source.file Sb2O3.txt _rod_data_source.block 0000001 _rod_database.code 3500255 loop_ _raman_complementary.id _raman_complementary.method 1 EDX loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 silicon_wafer loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 1534337 COD http://www.crystallography.net/cod/1534337.html ; no XRD analysis data. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 150.04601 11431.4 151.323 9242 152.59801 7649.7998 153.87399 6379.6001 155.151 5627.7998 156.425 4941.2002 157.701 4394.7998 158.97701 3956.8 160.25101 3780.6001 161.526 3812.3999 162.80099 3367 164.075 3236.3999 165.349 3064.3999 166.62399 2993.8 167.896 2970.6001 169.17101 2990.6001 170.44299 2996.6001 171.716 3010.6001 172.98801 3099.6001 174.26199 3201 175.535 3404.2 176.806 3588.2 178.078 4018.8 179.349 4469.2002 180.621 5021.6001 181.892 5847 183.164 6938 184.43401 8168 185.705 9599 186.97501 10941.8 188.246 12297.6 189.515 13392.4 190.785 12911 192.054 10884.6 193.32401 8621.2002 194.593 6948 195.862 6036.7998 197.13 5367.3999 198.39799 4913 199.66701 4588.6001 200.93401 4453.2002 202.203 4452.7998 203.47 4547 204.737 4704.6001 206.005 5019 207.271 5344.7998 208.539 5998.3999 209.80499 6931.3999 211.07001 8194.2002 212.33701 10135 213.603 12776 214.868 15648.4 216.134 17742.6 217.399 18350.199 218.66299 17751.199 219.929 16627 221.19299 15514.8 222.457 14758 223.72099 14414.4 224.98599 14007.4 226.24899 13650.8 227.51199 12888.8 228.776 11982.2 230.039 10976.8 231.30099 9937 232.564 9059.2002 233.827 8233.7998 235.089 7441.3999 236.351 7038.3999 237.612 6524.3999 238.873 6187.3999 240.136 5966.2002 241.397 5815.7998 242.657 5772.2002 243.918 5699.7998 245.17799 5764 246.438 5929.3999 247.698 6020.6001 248.959 6300.6001 250.218 6699.6001 251.47701 7672 252.73599 9903.4004 253.995 13357.8 255.25301 15280.4 256.51199 15036.4 257.76999 13477.8 259.02802 12114.8 260.28699 11192 261.54501 10693 262.802 10124 264.05899 9701.2002 265.31601 9509.4004 266.573 9521.7998 267.82901 9605.4004 269.086 9678.7998 270.34201 10099.8 271.59799 10428.8 272.853 10935.8 274.10901 11619 275.36401 12286.2 276.61899 13146.2 277.87399 14270.8 279.129 15790.6 280.383 17649.4 281.638 19614.6 282.89001 21461.801 284.14401 22917.199 285.39801 23641.4 286.651 24123.4 287.905 24871.199 289.15799 25736.801 290.41 27225.199 291.66299 28580.199 292.91599 29826.6 294.168 30764.4 295.418 31475.801 296.67001 31830 297.922 31402 299.173 30383.199 300.42499 29035 301.67599 27413.6 302.92499 25679.199 304.17599 23679.4 305.42599 21942.199 306.677 20014.801 307.927 18434.199 309.17499 16877 310.42499 15601.4 311.67401 14211.2 312.923 13026.8 314.17099 11992.2 315.42001 10988.6 316.668 10104.8 317.91699 9370.5996 319.16299 8756.2002 320.41101 8097.2002 321.659 7672 322.905 7174.3999 324.15302 6711.2002 325.39999 6369.3999 326.647 6015.2002 327.89301 5658 329.13901 5316.2002 330.384 5102.7998 331.63 4840 332.87601 4547.7998 334.121 4392.6001 335.366 4206 336.612 4035 337.85599 3860.6001 339.10101 3723.8 340.34399 3659.3999 341.58899 3538.3999 342.83301 3433.2 344.07599 3400.2 345.32001 3323.8 346.56201 3256.8 347.806 3211.2 349.048 3191.3999 350.29099 3071 351.53201 3067.8 352.77499 3027.8 354.01599 3028.3999 355.259 2987.6001 356.5 2977 357.742 2939.3999 358.98199 2897 360.224 2806.2 361.46399 2765.2 362.70499 2679.8 363.944 2667.6001 365.185 2625.6001 366.42401 2609.3999 367.66299 2576.8 368.90399 2595.2 370.142 2616.3999 371.38199 2698.6001 372.62 2813.8 373.858 2951 375.09698 2924 376.33499 2805.6001 377.57401 2575.8 378.811 2425 380.048 2365.3999 381.28601 2305 382.52301 2298.2 383.759 2228.8 384.99701 2195.3999 386.233 2177.2 387.46799 2133.8 388.70401 2136.3999 389.94101 2082 391.17599 2111.8 392.41101 2101.6001 393.647 2132.2 394.88199 2039.6 396.116 2058.2 397.35101 2037.8 398.58499 2054.3999 399.82001 2065.8 401.05301 2030.8 402.28699 2054.6001 403.51999 2051.8 404.755 2042.2 405.987 2062.8 407.22 2068.8 408.452 2078 409.685 2101.8 410.91699 2116.3999 412.14899 2128.2 413.38199 2141 414.61301 2182.2 415.84399 2202.8 417.07501 2261.3999 418.306 2314.8 419.53699 2382.8 420.767 2489 421.99799 2544 423.228 2610.6001 424.45901 2760.2 425.689 2804.2 426.918 2958.3999 428.147 3118.3999 429.37601 3257.8 430.60501 3493.3999 431.83401 3650.2 433.06299 3937 434.29099 4168.2002 435.51901 4467 436.74701 4815.6001 437.97501 5012 439.202 5383.3999 440.42899 5620 441.65601 5918.3999 442.883 6110.6001 444.10999 6223.3999 445.33499 6277.3999 446.56201 6243.3999 447.78799 6172.7998 449.01401 6422.3999 450.23901 6308.3999 451.465 6270.6001 452.69 6009.6001 453.91501 5505.6001 455.14001 4886 456.36499 4451.7998 457.58801 4071.3999 458.81299 3849.2 460.03699 3729.8 461.26099 3605.2 462.48499 3492.3999 463.70801 3407.2 464.92999 3333.6001 466.15302 3387 467.37601 3355.2 468.599 3429 469.82001 3464.8 471.043 3517.8 472.26501 3592.8 473.487 3697 474.70901 3865 475.92899 4057.8 477.151 4288.7998 478.37201 4544.2002 479.59201 4839.6001 480.81201 5312.7998 482.03299 5786.7998 483.254 6416 484.47198 7197 485.69299 8090.6001 486.91199 8832.5996 488.13101 9560.2002 489.35001 10149.4 490.56799 10412 491.78699 10716.6 493.00601 11170.6 494.22299 11654 495.44199 12445.6 496.66 13286.6 497.87701 14177.8 499.095 15071.6 500.311 15708.2 501.52899 16258.6 502.745 16222.4 503.96201 16000.8 505.17899 15286 506.39401 14484.8 507.61099 13434.4 508.82599 12425.6 510.04199 11349 511.25699 10434 512.47302 9584.2002 513.68701 8934 514.90198 8277.2002 516.11603 7631.3999 517.33099 7139.7998 518.54498 6757.6001 519.75897 6308.7998 520.97198 6026.6001 522.185 5746 523.39899 5462.2002 524.612 5224.6001 525.82501 4939.7998 527.03802 4789.2002 528.24902 4598.6001 529.46301 4388.2002 530.67401 4247.7998 531.88702 4045.2 533.09802 3878.3999 534.30902 3705.8 535.521 3570 536.73199 3435 537.94202 3331 539.15399 3174 540.36298 3069.2 541.573 3020.3999 542.784 2952.3999 543.99402 2837.8 545.203 2813 546.41199 2770.2 547.62201 2714.6001 548.83099 2706.2 550.039 2659 551.24701 2621.8 552.45697 2629.8 553.66498 2580 554.87201 2556.8 556.08002 2578.8 557.289 2574.2 558.49597 2566.6001 559.703 2555.8 560.909 2599 562.11603 2557.3999 563.32202 2583.3999 564.53003 2560 565.73602 2604.6001 566.94202 2615.8 568.14697 2673 569.35303 2705.3999 570.55798 2743.3999 571.763 2826.3999 572.96802 2842.8 574.17401 2938.2 575.37799 2972.3999 576.58197 3038.2 577.78601 3166.3999 578.98999 3280 580.19397 3408.2 581.39697 3587.8 582.60101 3703.2 583.80402 3918.3999 585.00702 4089.6001 586.20898 4341.2002 587.41199 4663.3999 588.61401 4890 589.81598 5178.2002 591.01801 5560.3999 592.21997 5889.2002 593.422 6094.3999 594.62299 6235 595.82397 6361 597.02502 6286 598.22601 6223.7998 599.427 5982.6001 600.62598 5739.3999 601.82599 5443.3999 603.026 5058.2002 604.22601 4798.2002 605.42603 4529.6001 606.625 4289.6001 607.82397 4117.7998 609.02301 3888 610.22101 3756 611.41998 3552 612.61798 3375.6001 613.81702 3189 615.01501 3023.8 616.21301 2889.3999 617.409 2755.2 618.60699 2601 619.80402 2464.3999 621.00098 2340.2 622.19702 2229 623.39398 2136 624.591 2057.2 625.78699 1961.6 626.98199 1950.4 628.17798 1917.2 629.37402 1876 630.57001 1784.8 631.76398 1799.8 632.95898 1747.4 634.15399 1693.6 635.34802 1687.8 636.54199 1642.2 637.737 1623.2 638.92999 1624 640.12402 1602.2 641.31799 1614.2 642.51099 1600.2 643.70398 1622.6 644.896 1607.65 646.09003 1607.65 647.28302 1638 648.474 1581.8 649.66699 1620.8 650.85797 1603.2 652.04999 1594.8 653.24103 1594.8 654.43298 1595.2 655.62299 1612.6 656.815 1604.6 658.00598 1646 659.19598 1657 660.38702 1675.6 661.57703 1670.4 662.76599 1708.8 663.95599 1725 665.14502 1782 666.33502 1832 667.52399 1886.4 668.71399 1921.2 669.90198 1997 671.091 2073.8 672.27899 2204.2 673.466 2296 674.65503 2430 675.84198 2576.8 677.03101 2727.8 678.21802 2898.6001 679.40399 2969.3999 680.59198 3168.6001 681.77802 3234.8 682.96399 3263 684.15198 3211 685.33698 3211.6001 686.52301 3088.8 687.71002 2942 688.89502 2827.3999 690.08002 2655.6001 691.26599 2556.3999 692.45001 2360.8 693.63501 2305.8 694.81897 2206.8 696.00403 2103 697.18799 1988.2 698.37201 1954.4 699.55499 1897.8 700.73901 1873.2 701.92297 1790 703.10602 1804.6 704.289 1773.2 705.47101 1765.2 706.65399 1751.2 707.83698 1762.6 709.01898 1752 710.20099 1751.4 711.383 1754.6 712.56403 1734.6 713.745 1791.4 714.927 1757.8 716.10901 1739.8 717.289 1672.8 718.46997 1623.8 719.65002 1585.8 720.83002 1511.6 722.01001 1533.8 723.19 1438.6 724.37 1449 725.54901 1437.2 726.72803 1397.4 727.90698 1378 729.086 1355.8 730.26501 1341.6 731.44299 1318.2 732.62201 1294.8 733.79999 1320.4 734.97803 1294.6 736.15503 1297 737.33301 1262.8 738.51001 1285.6 739.68799 1246.2 740.86499 1242.2 742.04102 1243.4 743.21802 1239.4 744.39502 1225.8 745.56897 1212.4 746.745 1204.2 747.92102 1179 749.09698 1172.2 750.27301 1217.2 751.448 1212.4 752.62299 1190 753.797 1187 754.97198 1175.8 756.146 1172.2 757.32098 1159 758.495 1185 759.66803 1154.6 760.841 1183.4 762.01501 1139.2 763.18903 1130.4 764.362 1147.6 765.534 1154.8 766.70697 1111.8 767.88 1128.2 769.05103 1126.4 770.22302 1107.8 771.39502 1128.8 772.56799 1127.2 773.73798 1120.2 774.90997 1119 776.08099 1117.2 777.25098 1113.2 778.422 1116.8 779.59302 1103 780.763 1102.2 781.93298 1094.2 783.10199 1102 784.27301 1095.2 785.44299 1093.6 786.61102 1076.8 787.78101 1086.6 788.94897 1078 790.11798 1103.8 791.28699 1117 792.45502 1091.8 793.62402 1102.2 794.79102 1089.2 795.95898 1086.4 797.12598 1075.4 798.29401 1071.8 799.461 1094.4 800.62799 1075 801.79498 1057.4 802.96198 1074.8 804.12799 1085.6 805.29498 1074.8 806.46002 1087.4 807.62701 1071.8 808.79199 1050.2 809.95599 1069.8 811.12299 1051.2 812.28699 1058.4 813.453 1097.4 814.617 1064.6 815.78101 1060.6 816.94598 1057.8 818.10999 1084.2 819.27301 1082.4 820.43799 1081 821.60101 1067.6 822.763 1073.4 823.92798 1095.8 825.09003 1054.8 826.25201 1051.4 827.41602 1088.8 828.578 1055.4 829.73999 1070.4 830.901 1059.4 832.06403 1069.8 833.22498 1068.2 834.38599 1077.8 835.547 1047.4 836.70898 1055 837.87 1065.4 839.03003 1056 840.19 1050.8 841.34998 1062.6 842.51202 1049.6 843.67102 1044 844.83099 1035 845.98999 1054.8 847.14899 1053 848.30798 1028.2 849.46802 1044.8 850.62701 1046 851.78497 1044.4 852.94299 1041.4 854.10101 1028.8 855.25897 1042.4 856.41699 1030 857.57397 1027 858.73102 1009.8 859.888 1007.6 861.04498 1018.4 862.20203 1045.2 863.35901 1035.2 864.51501 1031 865.67102 1027 866.82703 1033.4 867.98297 1021.4 869.13898 1043.4 870.29401 1023.4 871.45001 1028.4 872.60498 1017.6 873.76001 1033.4 874.91498 1027.6 876.06897 1011.4 877.224 1018.6 878.37799 1020.8 879.53198 1028 880.68597 1022.8 881.84003 1014.8 882.992 1030.4 884.14502 1015.8 885.29797 993 886.45099 998.20001 887.604 1003.2 888.75702 1007 889.90802 995.79999 891.06 1041.6 892.21198 1021.4 893.36401 1016 894.51599 1015.8 895.66602 997 896.81799 1029.6 897.96899 1004.6 899.12 994 900.26898 1006.2 901.41998 1009.8 902.57098 1031.4 903.72101 1007 904.87 993.40002 906.02002 1010 907.16998 1015.6 908.31799 1035.6 909.46698 982.79999 910.617 1007 911.76398 1010.8 912.91302 1004.2 914.06201 988.40002 915.20898 1042.6 916.35797 1015.6 917.50403 994.40002 918.65198 1028.2 919.79999 985.59998 920.94702 1000.4 922.09399 978.59998 923.23999 986.40002 924.38702 995 925.53302 1016 926.67999 1023 927.82501 1009.4 928.97101 1016.2 930.11603 1020.4 931.26202 1006 932.40698 1013 933.55298 1031.8 934.69702 992 935.84198 1000.6 936.98602 1013.6 938.13098 1012.4 939.27502 987.20001 940.41901 1004.4 941.56201 1016.8 942.70502 1013 943.84998 996.79999 944.992 1000.2 946.13599 1039 947.27802 1003.6 948.41998 1025.4 949.56403 1015.6 950.70502 1013.4 951.84698 1008.6 952.98999 1012.6 954.13098 1010.6 955.27197 1025.6 956.414 999.59998 957.55499 1003.8 958.69501 1017 959.83698 1004.4 960.97699 1011.2 962.117 1008 963.25702 1010.2 964.39801 1012.8 965.53699 1003.8 966.677 1019 967.81598 988.40002 968.95502 1091.8 970.09497 1193.2 971.23401 1027.2 972.37201 1009.6 973.51001 1012.8 974.64801 1004.4 975.78601 1019.6 976.92499 1016.2 978.06299 1015.6 979.20001 1030.4 980.33698 995.59998 981.474 1035.4 982.61102 1011 983.74799 1015.2 984.88397 1027.6 986.021 1009.2 987.15698 1031 988.29303 1020.4 989.42902 1036.2 990.565 1005 991.70099 1029.2 992.836 1024 993.97101 1016.8 995.10602 1019.8 996.24103 1016.8 997.37598 1003.8 998.50897 1035.2 999.64301 1024.4 1000.78 1026.8 1001.91 1022.8 1003.04 1025.6 1004.18 1030.6 1005.31 1018.8 1006.44 1029.6 1007.58 1007.2 1008.71 1016.8 1009.84 1030.6 1010.98 1030.6 1012.11 1014.2 1013.24 1017 1014.37 1030.2 1015.5 1035.4 1016.63 1015.2 1017.77 1016.8 1018.9 1034.8 1020.03 1034.4 1021.16 1064.2 1022.29 1009.4 1023.42 1024.6 1024.55 1022.6 1025.6801 1036.8 1026.8101 1026.6 1027.9399 1046.8 1029.0699 1038.2 1030.2 1007.8 1031.33 1028 1032.45 1023.4 1033.58 1054.6 1034.71 1031.6 1035.84 1029.8 1036.97 1019.8 1038.1 1044 1039.22 1011.2 1040.35 1018.8 1041.48 1047 1042.6 1035.6 1043.73 1040.8 1044.86 1027.8 1045.99 1040 1047.11 1048.2 1048.24 1014.8 1049.36 1018 1050.49 1033.2 1051.62 1044.4 1052.74 1023.8 1053.87 1045 1054.99 1026.2 1056.12 1042 1057.24 1022.2 1058.37 1030.2 1059.49 1017 1060.61 1019.4 1061.74 1008.4 1062.86 1039.6 1063.99 1039.8 1065.11 1026.4 1066.23 1034.6 1067.36 1034 1068.48 1026.2 1069.6 1038.4 1070.72 1027.8 1071.85 1042.6 1072.97 1035.8 1074.09 1007.6 1075.21 1026 1076.33 1022.2 1077.45 1018 1078.58 1025.4 1079.7 1001.4 1080.8199 1035.8 1081.9399 1040.6 1083.0601 1028.2 1084.1801 1032.4 1085.3 1044.6 1086.42 1032.4 1087.54 1048.4 1088.66 1052.8 1089.78 1049.2 1090.9 1020.2 1092.02 1074 1093.14 1046.4 1094.25 1038.4 1095.37 1047.4 1096.49 1045 1097.61 1012 1098.73 1070 1099.85 1034.6 1100.96 1030.8 1102.08 1038.4 1103.2 1020.4 1104.3101 1043.6 1105.4301 1033.2 1106.55 1028.6 1107.67 1042.6 1108.78 1030.8 1109.9 1049 1111.01 1050.8 1112.13 1054.4 1113.24 1055.4 1114.36 1034.4 1115.48 1054.6 1116.59 1017.2 1117.71 1046.4 1118.8199 1066.8 1119.9301 1041 1121.05 1045.2 1122.16 1024 1123.28 1034.8 1124.39 1026.4 1125.51 1049.8 1126.62 1042 1127.73 1033.6 1128.84 1020 1129.96 1032.8 1131.0699 1048 1132.1801 1030 1133.29 1035.6 1134.41 1040.6 1135.52 1037.6 1136.63 1048.4 1137.74 1039.2 1138.85 1023 1139.97 1005 1141.08 1025.4 1142.1899 1029.2 1143.3 1024.4 1144.41 1040.8 1145.52 1008 1146.63 1032.8 1147.74 1024.6 1148.85 1004.2 1149.96 1045 1151.0699 1032.4 1152.1801 1040 1153.29 1028 1154.39 1031.8 1155.5 1028.8 1156.61 1024.4 1157.72 1021 1158.83 1046.8 1159.9399 1026 1161.04 1028.8 1162.15 1032.8 1163.26 1044 1164.37 1057.2 1165.47 1031.2 1166.58 1036.8 1167.6899 1024.6 1168.79 1043.4 1169.9 1062.6 1171.01 1051.4 1172.11 1021.8 1173.22 1048.2 1174.3199 1065.4 1175.4301 1040 1176.54 1050.4 1177.64 1022.4 1178.75 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