#------------------------------------------------------------------------------ #$Date: 2019-06-11 16:15:37 +0300 (Tue, 11 Jun 2019) $ #$Revision: 1338 $ #$URL: svn://172.16.1.111/rod/cif/3/50/02/3500270.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500270 loop_ _publ_author_name 'Kumar, Arun' 'Zanatta, M.' 'Nazzareni, S' 'Daldosso, N.' 'Mariotto, G.' _publ_section_title ; Raman spectrum of Mg(OH)2 ; _journal_name_full 'Personal communication to ROD' _journal_year 2019 _chemical_compound_source 'natural'_chemical_formula_structural 'Mg (O H)2' _chemical_formula_sum 'H2 Mg O2' _chemical_name_mineral Brucite _chemical_name_systematic 'Magnesium hydroxide' _space_group_IT_number 164 _symmetry_cell_setting trigonal _symmetry_Int_Tables_number 164 _symmetry_space_group_name_Hall '-P 3 2"' _symmetry_space_group_name_H-M 'P -3 m 1' _audit_creation_date 1999-03-08 _audit_creation_method 'generated by RETRIEVE 2.0' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_formula_units_Z 1 _cell_length_a 3.142(1) _cell_length_b 3.142(1) _cell_length_c 4.766(2) _cell_volume 40.7 _raman_determination_method experimental _[local]_chemical_compound_color white _[local]_chemical_compound_state Solid _raman_measurement_device.location 'University of Verona' _raman_measurement_device.company 'Thermo Scientific_raman_measurement_device.model DXR2' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.50 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 633 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 1 _raman_measurement_device.power_on_sample 8 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1.5 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 30 _raman_measurement.datetime_initiated 2019-05-13 _rod_data_source.file MgOH2.txt _rod_data_source.block /var/www/html/rod/tmp/uploads/1560258707.6008-06A4055A28351D0A.rod _rod_database.code 3500270 loop_ _raman_complementary.id _raman_complementary.method 1 EDX loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 silicon_wafer loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 1000054 COD http://www.crystallography.net/cod/1000054.html ; no XRD analysis data. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.raw_intensity _raman_spectrum.intensity 50.491089 12.06803 3.9834073 51.455318 11.57179 3.4838996 52.419559 11.07708 2.9859114 53.38379 10.40745 2.31299 54.34802 9.70036 1.6026 55.31226 9.43454 1.33347 56.27649 9.68088 1.57648 57.24072 11.15551 3.04778 58.20496 12.24914 4.13807 59.16919 12.91946 4.80503 60.13342 13.01627 4.89848 61.09766 12.71234 4.59117 62.06189 12.3419 4.21734 63.02612 11.8652 3.73725 63.99036 11.03793 2.90657 64.95459 10.46998 2.3352 65.91882 10.17018 2.03198 66.88306 10.2823 2.14066 67.84729 10.60826 2.46317 68.81152 10.89624 2.7477 69.77576 11.13728 2.98527 70.73999 11.29935 3.14387 71.70422 11.47038 3.31141 72.66846 11.67359 3.51113 73.63269 12.06943 3.90347 74.59692 12.4094 4.23993 75.56116 12.46774 4.29475 76.52539 12.11604 3.93952 77.48962 11.0599 2.87985 78.45386 10.355 2.1714 79.41809 10.0063 1.81915 80.38232 10.29189 2.10118 81.34656 10.70718 2.5129 82.31079 10.99198 2.79412 83.27502 11.13071 2.92926 84.23926 11.10804 2.903 85.20349 11.01952 2.81088 86.16772 10.83424 2.62199 87.13196 10.32568 2.10981 88.09619 9.93022 1.71073 89.06042 9.79572 1.5726 90.02466 10.09802 1.87126 90.98889 10.85244 2.62204 91.95313 11.36837 3.13432 92.91736 11.59853 3.36082 93.88159 11.33041 3.08903 94.84583 11.02728 2.78223 95.81006 10.75032 2.50159 96.77429 10.48468 2.23227 97.73853 10.23755 1.98144 98.70276 10.04885 1.78905 99.66699 9.91594 1.65244 100.6312 9.80708 1.53987 101.5955 9.79802 1.52709 102.5597 9.90139 1.62674 103.5239 10.27631 1.99793 104.4882 10.76509 2.48297 105.4524 11.07312 2.78726 106.4166 11.17608 2.88648 107.3809 10.90414 2.61079 108.3451 10.6274 2.3303 109.3093 10.34467 2.04381 110.2736 9.96224 1.65761 111.2378 9.60376 1.29536 112.202 9.38506 1.07288 113.1663 9.36335 1.0474 114.1305 9.69417 1.37443 115.0947 9.89111 1.56758 116.059 9.95475 1.62742 117.0232 9.66075 1.32962 117.9874 9.36309 1.02816 118.9517 9.22877 0.89003 119.9159 9.35993 1.01738 120.8801 9.83358 1.48722 121.8444 10.17743 1.82725 122.8086 10.36661 2.01261 123.7728 10.28619 1.92836 124.7371 10.16228 1.80062 125.7013 10.03899 1.6735 126.6655 9.91743 1.5481 127.6298 9.80047 1.4273 128.59399 9.69102 1.314 129.5582 9.59171 1.21084 130.52251 9.4765 1.09178 131.48669 9.38615 0.99757 132.4509 9.31739 0.92496 133.41521 9.22879 0.8325 134.37939 9.15592 0.75576 135.3436 9.16887 0.76485 136.30791 9.30269 0.8948 137.27209 9.81072 1.39896 138.2363 10.12689 1.71126 139.20061 10.26607 1.84656 140.16479 10.00434 1.58095 141.129 9.62376 1.1965 142.09331 9.34572 0.91457 143.0575 9.2182 0.78317 144.0217 9.32514 0.88622 144.98599 9.38089 0.93808 145.9502 9.38154 0.93484 146.9144 9.17251 0.72192 147.87869 8.99974 0.54525 148.8429 8.94205 0.48367 149.8071 9.10483 0.64256 150.77139 9.49927 1.03309 151.7356 9.77731 1.30723 152.6998 9.92379 1.44982 153.66409 9.79593 1.31806 154.6283 9.64699 1.1652 155.5925 9.4971 1.01141 156.55679 9.31319 0.8236 157.521 9.12137 0.62787 158.4852 8.98868 0.49127 159.44949 8.92735 0.42604 160.4137 9.01886 0.51364 161.3779 9.09518 0.58605 162.34219 9.15113 0.63809 163.3064 9.16049 0.64355 164.2706 9.15517 0.63431 165.23489 9.16255 0.63779 166.1991 9.18299 0.65431 167.1633 9.21335 0.68076 168.12759 9.2642 0.7277 169.0918 9.33603 0.79562 170.056 9.53351 0.9892 171.02029 9.69187 1.14364 171.9845 9.7589 1.20676 172.9487 9.64327 1.08722 173.91299 9.35085 0.79089 174.8772 9.14559 0.58173 175.8414 9.04737 0.47959 176.80569 9.22272 0.65104 177.7699 9.37855 0.80296 178.7341 9.49398 0.91449 179.69839 9.55387 0.97047 180.6626 9.57 0.9827 181.6268 9.56306 0.97185 182.59109 9.52092 0.92581 183.5553 9.36664 0.76763 184.5195 9.29059 0.68769 185.4838 9.29439 0.68759 186.448 9.49211 0.88141 187.4122 9.72566 1.11107 188.3765 9.90146 1.28297 189.3407 9.98223 1.35985 190.3049 9.94906 1.32278 191.2692 9.91401 1.28385 192.2334 9.88923 1.25518 193.1976 9.91904 1.28111 194.1619 9.93183 1.29001 195.1261 9.91444 1.26874 196.0903 9.80408 1.1545 197.0546 9.63728 0.98382 198.0188 9.53896 0.88163 198.983 9.53698 0.87577 199.9473 9.79555 1.13048 200.9115 9.98072 1.31178 201.8757 10.07011 1.3973 202.84 9.92898 1.25231 203.8042 9.72134 1.04081 204.7684 9.58773 0.90334 205.7327 9.58438 0.89614 206.6969 9.7622 1.0701 207.6611 9.92151 1.22557 208.6254 10.0287 1.32891 209.5896 10.04717 1.34353 210.5538 10.04629 1.33881 211.5181 10.04764 1.33632 212.4823 10.05181 1.33666 213.4465 10.06042 1.34144 214.4108 10.08104 1.35823 215.375 10.11464 1.388 216.3392 10.18059 1.45013 217.3035 10.23863 1.50435 218.2677 10.28455 1.54646 219.2319 10.28825 1.54635 220.1962 10.28612 1.54041 221.1604 10.31423 1.56471 222.1246 10.3972 1.64388 223.0889 10.56237 1.80526 224.0531 10.71459 1.95368 225.0173 10.83298 2.06829 225.9816 10.87849 2.11001 226.9458 10.91398 2.14172 227.91 10.9592 2.18316 228.8743 11.00501 2.2252 229.8385 11.05626 2.27268 230.8027 11.14021 2.35287 231.767 11.26759 2.47649 232.7312 11.51873 2.72387 233.6954 11.74368 2.94507 234.6597 11.924 3.12164 235.6239 12.03226 3.22616 236.5881 12.10212 3.29229 237.5524 12.16491 3.35134 238.5166 12.19573 3.37843 239.4808 12.15671 3.33569 240.4451 12.19221 3.36747 241.4093 12.34056 3.51211 242.3735 12.75426 3.9221 243.3378 13.17678 4.34092 244.302 13.53655 4.69699 245.2662 13.71751 4.87425 246.2305 13.78021 4.93326 247.1947 13.92555 5.07492 248.15891 14.21267 5.35836 249.1232 14.76255 5.90457 250.0874 15.33456 6.47291 251.05161 15.88074 7.01543 252.0159 16.35279 7.48382 252.9801 16.80932 7.9367 253.94431 17.29245 8.41618 254.9086 17.7809 8.90099 255.8728 18.26093 9.37739 256.83701 18.83912 9.95195 257.8013 19.55147 10.66068 258.7655 20.3827 11.48829 259.72971 21.35629 12.45827 260.694 22.47754 13.57591 261.6582 23.67551 14.77028 262.62241 25.011 16.10217 263.5867 26.59863 17.68622 264.5509 28.3797 19.46371 265.51511 30.09487 21.1753 266.4794 32.42624 23.5031 267.4436 35.55953 26.63283 268.40781 39.0179 30.08764 269.3721 43.38157 34.44775 270.3363 48.91928 39.98192 271.30051 55.7325 46.7916 272.2648 63.77096 54.82653 273.229 73.03469 64.08674 274.19321 83.75228 74.80081 275.1575 99.74895 90.79397 276.1217 114.2668 105.30831 277.08591 125.8521 116.89011 278.0502 135.7028 126.73733 279.0144 142.33031 133.36134 279.97861 144.3046 135.33215 280.9429 139.4722 130.49628 281.9071 126.4264 117.44702 282.87131 111.7376 102.75477 283.8356 97.71378 88.72749 284.7998 83.39442 74.40469 285.76401 70.27183 61.27866 286.7283 58.87514 49.87854 287.6925 49.70429 40.70426 288.65671 42.43713 33.43369 289.621 36.4109 27.40405 290.58521 31.56321 22.55296 291.54941 28.28115 19.26751 292.5137 25.64507 16.62804 293.47791 23.31257 14.29216 294.44211 21.25309 12.22931 295.4064 19.48533 10.45818 296.37061 18.02 8.9895 297.33481 16.96927 7.93542 298.2991 16.29762 7.26043 299.26331 15.74677 6.70624 300.22751 15.21314 6.16928 301.1918 14.67363 5.62646 302.15601 14.16928 5.1188 303.12021 13.71032 4.65653 304.0845 13.32158 4.2645 305.04871 12.9798 3.91943 306.01291 12.66241 3.59876 306.9772 12.36099 3.29407 307.94141 12.0745 3.00431 308.90561 11.8059 2.73246 309.8699 11.55588 2.47919 310.83411 11.31994 2.24001 311.79831 11.10604 2.02288 312.7626 10.91929 1.8329 313.72681 10.75826 1.66866 314.69101 10.62541 1.5326 315.6553 10.52248 1.42647 316.61951 10.45749 1.35829 317.58371 10.43774 1.33536 318.548 10.43319 1.32764 319.51221 10.42846 1.31974 320.47641 10.41781 1.30593 321.4407 10.41128 1.29626 322.40491 10.41422 1.29606 323.36911 10.4492 1.3279 324.3334 10.50092 1.3765 325.29761 10.53514 1.40761 326.26181 10.52836 1.39772 327.2261 10.46348 1.32974 328.19031 10.3776 1.24077 329.15451 10.29314 1.15324 330.1188 10.20789 1.06491 331.08301 10.1288 0.98276 332.04721 10.06117 0.91208 333.01151 9.98897 0.83683 333.97571 9.91908 0.7639 334.93991 9.88085 0.72265 335.90421 9.9036 0.74239 336.86841 10.04551 0.88129 337.83261 10.19246 1.02524 338.79691 10.2741 1.10389 339.76111 10.24323 1.07003 340.72531 10.16279 0.98662 341.68961 10.08162 0.90249 342.65381 10.01598 0.83389 343.61801 9.96431 0.77928 344.58231 9.92383 0.73586 345.54651 9.89542 0.70452 346.51071 9.89277 0.69896 347.47501 9.89652 0.6998 348.43921 9.89395 0.69433 349.40341 9.88015 0.67764 350.36771 9.8624 0.65701 351.33191 9.847 0.63874 352.29611 9.821 0.60988 353.26041 9.78299 0.56902 354.22461 9.7631 0.54629 355.18881 9.78586 0.56621 356.15311 9.89061 0.66814 357.11731 10.01935 0.79407 358.08151 10.12823 0.90015 359.04581 10.22359 0.99271 360.01001 10.29994 1.06628 360.97421 10.34949 1.11305 361.93851 10.35466 1.11546 362.90271 10.31313 1.07117 363.86691 10.25693 1.01223 364.83121 10.20845 0.96101 365.79541 10.14771 0.89754 366.75961 10.10849 0.85561 367.72391 10.11458 0.85899 368.68811 10.21898 0.9607 369.65231 10.37179 1.11082 370.61661 10.50618 1.24253 371.58081 10.57791 1.3116 372.54501 10.58405 1.31508 373.50931 10.55928 1.28766 374.47351 10.53218 1.25793 375.43771 10.49324 1.21636 376.40201 10.45813 1.17863 377.36621 10.43975 1.15765 378.33041 10.46482 1.18012 379.29471 10.50811 1.22083 380.25891 10.53266 1.2428 381.22311 10.485 1.19258 382.18741 10.35781 1.06283 383.15161 10.23693 0.93941 384.11581 10.20922 0.90916 385.08011 10.34091 1.03833 386.04431 10.5499 1.2448 387.00851 10.73662 1.42902 387.97281 10.92196 1.61186 388.93701 11.08631 1.77373 389.90121 11.1988 1.88375 390.86551 11.20798 1.89047 391.82971 11.10755 1.78758 392.79391 10.98028 1.65787 393.75821 10.91001 1.58517 394.72241 10.91122 1.58396 395.68661 10.97421 1.64454 396.65091 11.07197 1.7399 397.61511 11.23114 1.89668 398.57932 11.42926 2.09243 399.54361 11.62568 2.28648 400.50781 11.78381 2.44225 401.47198 11.9001 2.55619 402.43631 12.01305 2.66681 403.40051 12.17244 2.82387 404.36469 12.42409 3.07321 405.32901 12.71721 3.36402 406.29321 12.95882 3.60334 407.25739 13.06725 3.70949 408.22171 13.10758 3.74755 409.18591 13.19736 3.83507 410.15009 13.44403 4.07949 411.11441 13.8463 4.47952 412.07861 14.28189 4.91288 413.04279 14.59742 5.22619 414.00711 14.70179 5.32836 414.97131 14.71188 5.33625 415.93549 14.88845 5.51064 416.89981 15.26857 5.88858 417.86401 15.80824 6.42609 418.82819 16.42143 7.03713 419.79251 17.05192 7.66548 420.75671 17.70428 8.31571 421.72089 18.43957 9.04888 422.68521 19.31288 9.92008 423.64941 20.30863 10.91373 424.61359 21.44705 12.05007 425.57791 22.79154 13.39248 426.54211 24.19039 14.78927 427.50629 25.75107 16.34789 428.47061 27.71722 18.312 429.43481 29.87086 20.46361 430.39899 32.27223 22.86296 431.36331 35.44011 26.02883 432.32751 39.56252 30.14924 433.29169 44.29836 34.88309 434.25601 50.29293 40.87569 435.22021 58.98475 49.56555 436.18439 69.70196 60.2808 437.14871 82.88936 73.46626 438.11292 100.2844 90.85938 439.07709 125.8354 116.40846 440.04141 158.3347 148.90585 441.00562 190.4285 180.99776 441.96979 218.7309 209.29826 442.93411 244.6675 235.23299 443.89828 264.52939 255.09302 444.86249 270.34271 260.90448 445.82681 255.8759 246.43584 446.79099 223.30991 213.86801 447.75519 192.7704 183.32669 448.71951 163.3924 153.94688 449.68369 135.4446 125.99729 450.64789 110.755 101.30591 451.61221 90.86855 81.41769 452.57639 75.98888 66.53625 453.54059 64.87553 55.42115 454.50491 55.57764 46.12153 455.46909 48.42997 38.97213 456.43329 43.26328 33.80373 457.39761 38.83859 29.37733 458.36179 35.26952 25.80658 459.32599 32.5075 23.04287 460.29031 30.11765 20.65136 461.25449 27.97067 18.50272 462.21881 26.06709 16.59749 463.18301 24.41906 14.94783 464.14719 23.10348 13.63063 465.11151 22.20452 12.73005 466.07571 21.64299 12.16692 467.03989 20.99741 11.51976 468.00421 20.17535 10.69612 468.96841 19.19766 9.71686 469.93259 18.33703 8.85468 470.89691 17.63935 8.15546 471.86111 17.10424 7.61882 472.82529 16.671 7.18406 473.78961 16.30291 6.81446 474.75381 16.00677 6.51683 475.71799 15.77207 6.28064 476.68231 15.5781 6.0852 477.64651 15.47128 5.97692 478.61069 15.46641 5.9706 479.57501 15.34357 5.84632 480.53922 15.02881 5.53014 481.50339 14.49622 4.99613 482.46771 14.00698 4.50549 483.43188 13.68689 4.18401 484.39609 13.56888 4.06462 485.36041 13.55753 4.0519 486.32458 13.50676 3.99978 487.28879 13.40735 3.89902 488.25311 13.26055 3.75089 489.21729 13.12201 3.61103 490.18149 12.9915 3.47921 491.14581 12.8672 3.35361 492.10999 12.74448 3.22961 493.07419 12.61403 3.09788 494.03851 12.469 2.95159 495.00269 12.34458 2.82592 495.96689 12.27728 2.75738 496.93121 12.28689 2.76577 497.89539 12.34997 2.82763 498.85959 12.37524 2.8517 499.82391 12.35746 2.83273 500.78809 12.29349 2.76758 501.75229 12.20376 2.67668 502.71661 12.07702 2.54878 503.68079 11.89126 2.36188 504.64499 11.72255 2.19204 505.60931 11.59902 2.06738 506.57349 11.53403 2.00129 507.53769 11.50189 1.96805 508.50201 11.46567 1.93074 509.46619 11.42668 1.89068 510.43039 11.38592 1.84886 511.39471 11.35199 1.81388 512.35889 11.31538 1.77623 513.32312 11.25311 1.71293 514.28741 11.23104 1.68985 515.25159 11.25606 1.71386 516.21582 11.34369 1.8005 517.18011 11.46104 1.91687 518.14429 11.59947 2.05434 519.10852 11.78849 2.2424 520.07281 11.99549 2.44846 521.03699 12.11747 2.5695 522.00122 12.12286 2.57397 522.96552 11.96718 2.41738 523.92969 11.86171 2.31102 524.89392 11.8261 2.27452 525.85822 11.90614 2.35369 526.82239 11.97077 2.41746 527.78662 11.9955 2.44134 528.75092 11.96272 2.40772 529.71509 11.90286 2.34704 530.67932 11.84196 2.28532 531.64362 11.77104 2.2136 532.60779 11.69402 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