#------------------------------------------------------------------------------
#$Date: 2019-06-12 16:33:18 +0300 (Wed, 12 Jun 2019) $
#$Revision: 1352 $
#$URL: svn://172.16.1.111/rod/cif/3/50/02/3500284.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500284
loop_
_publ_author_name
'Kumar, A.'
'Zanatta, M.'
'Bersani, D'
'Daldosso, N.'
'Mariotto, G.'
_publ_section_title
;
 Raman spectrum of FeHO2
;
_journal_name_full               'Personal communication to ROD'
_journal_year                    2019
_chemical_compound_source
'natural'_chemical_formula_structural     'Fe O (O H)'
_chemical_formula_sum            'Fe H O2'
_chemical_name_mineral           Lepidocrocite
_chemical_name_systematic        'Iron(III) oxide hydroxide'
_space_group_IT_number           63
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      63
_symmetry_space_group_name_Hall  '-A 2 2a'
_symmetry_space_group_name_H-M   'A m a m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   3.87
_cell_length_b                   12.51
_cell_length_c                   3.06
_cell_volume                     148.1
_raman_determination_method      experimental
_[local]_chemical_compound_color white
_[local]_chemical_compound_state Solid
_raman_measurement_device.location 'University of Verona'
_raman_measurement_device.company
'Thermo Scientific_raman_measurement_device.model DXR2'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.50
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 633
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 1
_raman_measurement_device.power_on_sample 1
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1.5
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 30
_raman_measurement.datetime_initiated 2019-03-07
_rod_data_source.file            FeOOH.txt
_rod_data_source.block
/var/www/html/rod/tmp/uploads/1560346320.661-06A4055A28351D0A.rod
_rod_database.code               3500284
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 silicon_wafer
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 1011026 COD http://www.crystallography.net/cod/1011026.html
;
no XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.raw_intensity
_raman_spectrum.intensity
50.67041 45.78841 44.096783
51.634651 44.99511 43.225357
52.598881 44.256569 42.408897
53.56311 43.627361 41.701996
54.527351 43.088669 41.085819
55.491581 42.623341 40.543228
56.455818 42.163109 40.005947
57.420052 41.682701 39.448708
58.384281 41.154121 38.843506
59.348518 40.62608 38.239059
60.312752 40.111851 37.64864
61.276989 39.607361 37.06818
62.241219 39.107792 36.492847
63.205448 38.6134 35.922905
64.169693 38.10387 35.338039
65.133919 37.484879 34.643925
66.098152 36.944611 34.028748
67.062393 36.51643 33.525867
68.026619 36.251301 33.186253
68.990852 36.122841 32.983517
69.955093 35.97583 32.762444
70.919319 35.808769 32.521534
71.883553 35.593712 32.232834
72.847794 35.380428 31.946117
73.812019 35.175621 31.668087
74.776253 35.029209 31.448664
75.740494 34.8974 31.244051
76.70472 34.66251 30.936567
77.668953 34.299461 30.501133
78.633186 33.54287 29.672365
79.59742 32.982208 29.039734
80.561653 32.626511 28.612276
81.525887 32.626751 28.540962
82.490128 32.798229 28.641092
83.454361 32.882 28.653725
84.418587 32.863609 28.564398
85.382828 32.64357 28.273632
86.347061 32.488831 28.048372
87.311287 32.395302 27.884525
88.275528 32.44463 27.863741
89.239761 32.51125 27.860455
90.203987 32.492779 27.772284
91.168228 32.37513 27.585136
92.132462 32.122009 27.26272
93.096687 31.863041 26.934664
94.060928 31.595501 26.598236
95.025162 31.31381 26.24786
95.989403 31.01808 25.883648
96.953629 30.70072 25.498009
97.917862 30.30271 25.031921
98.882103 29.787069 24.448404
99.846329 29.450411 24.044071
100.8106 29.35553 23.881714
101.7748 29.764009 24.222921
102.739 30.11186 24.503704
103.7033 30.244591 24.569555
104.6675 30.011459 24.269753
105.6317 29.44253 23.634354
106.596 29.05467 23.180214
107.5602 28.88286 22.942329
108.5244 29.185221 23.178816
109.4887 29.425091 23.353003
110.4529 29.55069 23.413122
111.4171 29.47242 23.269569
112.3814 29.26808 23.000137
113.3456 29.15196 22.819132
114.3098 29.14323 22.745708
115.2741 29.38352 22.921497
116.2383 29.565821 23.039497
117.2025 29.68445 23.094023
118.1668 29.723789 23.069447
119.131 29.697689 22.979631
120.0952 29.62266 22.841082
121.0595 29.478029 22.63312
122.0237 29.177019 22.26898
122.9879 28.98455 22.013575
123.9522 28.893801 21.860073
124.9164 28.987181 21.890902
125.8806 29.13699 21.978352
126.8449 29.26358 22.042768
127.8091 29.309731 22.026943
128.7733 29.21196 21.867392
129.73759 29.26103 21.854864
130.7018 29.474751 22.007183
131.666 29.982611 22.453835
132.63029 30.53476 22.944958
133.5945 31.0674 23.416767
134.5587 31.41925 23.707977
135.52299 31.616619 23.844893
136.4872 32.19545 24.363461
137.4514 33.16898 25.276918
138.4157 34.750671 26.798721
139.3799 36.53299 28.521343
140.3441 38.536579 30.465424
141.3084 41.52911 33.398628
142.2726 44.842701 36.653088
143.2368 46.99688 38.748318
144.2011 47.886398 39.579075
145.1653 46.57967 38.213768
146.1295 45.016659 36.592369
147.0938 43.201111 34.718616
148.058 40.66943 32.128918
149.0222 38.04781 29.449467
149.9865 35.86385 27.207851
150.9507 34.186989 25.47353
151.9149 33.145962 24.375223
152.8792 32.293941 23.466101
153.8434 31.626089 22.741339
154.8076 31.25606 22.314579
155.7719 30.970341 21.972309
156.7361 30.70121 21.646814
157.7003 30.408001 21.297422
158.6646 30.088921 20.922338
159.6288 29.88604 20.663639
160.593 29.807961 20.529922
161.5573 30.06811 20.73461
162.5215 30.269421 20.880644
163.4857 30.382299 20.938427
164.45 30.3894 20.890608
165.4142 30.315241 20.761711
166.3784 30.208719 20.600634
167.3427 30.068159 20.405687
168.3069 29.79875 20.082079
169.2711 29.58626 19.815569
170.2354 29.40958 19.585039
171.1996 29.31348 19.435272
172.1638 29.23781 19.306116
173.1281 29.142719 19.157707
174.0923 29.035021 18.996874
175.0565 28.920259 18.829153
176.0208 28.80969 18.665796
176.985 28.70731 18.510811
177.9492 28.544769 18.295839
178.9135 28.41917 18.117977
179.8777 28.349119 17.995842
180.8419 28.361 17.955818
181.8062 28.44593 17.98901
182.7704 28.52117 18.01269
183.7346 28.58847 18.028605
184.6989 28.70768 18.096596
185.6631 28.77981 18.117687
186.6273 28.80641 18.093418
187.5916 28.72333 17.959641
188.5558 28.59676 17.782545
189.5201 28.516251 17.651682
190.4843 28.469259 17.55451
191.4485 28.409731 17.444973
192.4128 28.469851 17.45525
193.377 28.645241 17.580969
194.3412 29.056749 17.942982
195.3055 29.51613 18.353029
196.2697 29.939939 18.727678
197.2339 30.249161 18.987909
198.1982 30.42292 19.112843
199.1624 30.728279 19.369551
200.1266 31.183741 19.776527
201.0909 31.74297 20.287434
202.0551 32.491951 20.988266
203.0193 33.444038 21.89237
203.9836 34.143059 22.543573
204.9478 34.967861 23.320726
205.912 36.701801 25.007183
206.8763 39.111649 27.369709
207.8405 40.694599 28.90551
208.8047 45.26339 33.427315
209.769 52.55975 40.676846
210.7332 62.47979 50.550232
211.6974 75.176071 63.200024
212.6617 90.775833 78.753456
213.6259 113.3261 101.25756
214.5901 145.23579 133.12123
215.5544 169.41541 157.255
216.5186 184.2187 172.01263
217.4828 185.5316 173.28003
218.4471 181.5041 169.20717
219.4113 173.1823 160.84018
220.3755 156.1837 143.79655
221.3398 133.89481 121.46279
222.304 114.6458 102.16908
223.2682 99.133507 86.612244
224.2325 89.049507 76.483856
225.1967 80.997108 68.38723
226.1609 74.567749 61.913811
227.1252 70.488724 57.790878
228.0894 67.743187 55.001595
229.0536 65.707672 52.922493
230.0179 64.358261 51.529652
230.9821 63.706261 50.834377
231.9463 63.661629 50.746635
232.9106 64.264603 51.306652
233.8748 65.19384 52.193092
234.839 66.97403 53.930637
235.8033 69.682587 56.596706
236.7675 72.805519 59.677311
237.7317 76.770882 63.600502
238.696 82.448433 69.236031
239.6602 89.044838 75.790573
240.6244 92.46933 79.173363
241.5887 103.1558 89.818275
242.5529 121.1329 107.75397
243.51711 134.33659 120.91643
244.4814 159.7722 146.31096
245.4456 205.7823 192.28011
246.40981 286.16299 272.62003
247.3741 402.36661 388.78299
248.3383 512.01721 498.39313
249.30251 610.70673 597.0423
250.2668 753.04712 739.34253
251.231 842.44049 828.69586
252.19521 870.64471 856.86029
253.1595 781.94189 768.11774
254.1237 631.54358 617.67981
255.08791 494.32391 480.42072
256.05219 379.83801 365.89554
257.01639 291.46619 277.48459
257.98071 220.09351 206.07294
258.94489 164.98039 150.92102
259.90909 134.9516 120.85356
260.87341 114.3399 100.20332
261.83759 97.904984 83.730042
262.80179 86.168442 71.955269
263.76611 78.663239 64.41198
264.73029 72.448402 58.159222
265.69449 67.218307 52.891338
266.65881 63.727348 49.36274
267.62299 60.649639 46.24754
268.58719 57.843071 43.403629
269.55151 55.229019 40.752373
270.51569 52.880619 38.36692
271.47989 50.852409 36.3018
272.44421 49.20607 34.618694
273.40839 47.994888 33.370895
274.37259 46.93119 32.270721
275.33691 45.993359 31.296553
276.30109 45.211361 30.478371
277.26529 44.525909 29.756874
278.22961 43.92458 29.11964
279.19379 43.439411 28.598717
280.15799 43.049511 28.173199
281.12231 42.714828 27.803041
282.08649 42.410221 27.463102
283.05069 42.060711 27.078402
284.01501 41.853729 26.836369
284.97919 41.802261 26.749994
285.94339 42.016991 26.929956
286.90771 42.319351 27.197687
287.87189 42.642849 27.4867
288.83609 42.892941 27.702446
289.80042 43.097969 27.873262
290.76459 43.464352 28.205578
291.72879 44.02203 28.729326
292.69312 44.77417 29.447674
293.65729 45.75597 30.395821
294.62149 46.96328 31.569614
295.58578 48.23053 32.80349
296.54999 49.763031 34.30275
297.51419 51.708679 36.215298
298.47849 53.891659 38.365307
299.44269 56.224319 40.665134
300.40689 59.40522 43.813343
301.37119 63.606758 47.982323
302.33539 68.214302 52.557446
303.29959 74.304619 58.615475
304.26389 82.053932 66.332634
305.22809 94.44294 78.689621
306.19229 108.4945 92.709305
307.15659 120.2992 104.48225
308.12079 129.4276 113.57903
309.08499 136.509 120.62896
310.04929 139.4888 123.57741
311.01349 137.39191 121.4493
311.97769 125.3075 109.33382
312.94199 111.7363 95.731659
313.90619 99.311203 83.275749
314.87039 88.530067 72.463921
315.83469 79.387703 63.291004
316.79889 71.765747 55.638626
317.76309 65.818703 49.661289
318.72739 62.12677 45.93919
319.69159 59.333969 43.116356
320.65579 57.09491 40.847393
321.62009 55.532841 39.255554
322.58429 54.43742 38.130489
323.54849 53.717072 37.380627
324.51279 53.443329 37.077499
325.47699 53.58395 37.188862
326.44119 53.939159 37.51495
327.40549 54.44574 37.992523
328.36969 55.02179 38.5397
329.33389 55.867489 39.356651
330.29819 57.000702 40.46125
331.26239 58.339569 41.771622
332.22659 59.990211 43.393906
333.19089 62.012482 45.387932
334.15509 64.421806 47.769146
335.11929 67.218384 50.537731
336.08359 70.374359 53.665844
337.04779 73.904533 57.168282
338.01199 78.049408 61.285542
338.97629 82.437477 65.646126
339.94049 86.970093 70.151382
340.90469 91.88813 75.042175
341.86899 96.901756 80.028687
342.83319 101.7364 84.836334
343.79739 106.8803 89.953362
344.76169 112.5036 95.549919
345.72589 116.8 99.819695
346.69009 119.2165 102.20969
347.65439 119.0941 102.06091
348.61859 117.3512 100.29175
349.58279 114.1827 97.097107
350.54709 108.3405 91.228889
351.51129 101.2085 84.070999
352.47549 94.242691 77.079414
353.43979 87.745758 70.556816
354.40399 81.648087 64.433609
355.36819 76.421097 59.181206
356.33249 72.251419 54.986229
357.29669 69.720787 52.430416
358.26089 67.941017 50.625591
359.22519 66.704514 49.364143
360.18939 65.753242 48.38805
361.15359 65.307953 47.91806
362.11789 65.650909 48.236423
363.08209 66.795593 49.35664
364.0463 68.680107 51.216801
365.01059 71.601784 54.114239
365.97479 75.72049 58.208824
366.939 80.11795 62.582279
367.90329 86.195381 68.635826
368.86749 94.431648 76.84832
369.8317 104.7815 87.174522
370.79599 117.3889 99.758377
371.76019 132.3949 114.74094
372.7244 151.44749 133.77023
373.68869 175.8824 158.18193
374.65289 199.77631 182.05276
375.6171 220.40891 202.66238
376.58139 242.5228 224.75342
377.54559 258.9324 241.14029
378.5098 266.99689 249.18213
379.47409 262.33389 244.49663
380.43829 248.7592 230.89952
381.4025 231.6739 213.79195
382.36679 211.7588 193.85464
383.33099 187.9615 170.03528
384.2952 164.71111 146.76292
385.25949 144.1942 126.22416
386.22369 127.3614 109.36963
387.1879 112.8505 94.83709
388.15219 100.2672 82.232269
389.11639 89.952766 71.896431
390.0806 81.519623 63.44199
391.04489 74.391777 56.292953
392.00909 68.554619 50.434715
392.9733 64.16391 46.023033
393.93759 60.451981 42.290237
394.90179 57.028229 38.84573
395.866 53.81625 35.613106
396.83029 50.963341 32.739655
397.79449 48.551708 30.30759
398.7587 46.902592 28.638149
399.72299 45.69788 27.413218
400.68719 44.530731 26.225956
401.6514 43.120312 24.795532
402.61569 41.419788 23.075106
403.5799 39.805592 21.441114
404.5441 38.500351 20.116184
405.50839 37.790562 19.38681
406.4726 37.273041 18.849812
407.4368 36.748539 18.305937
408.40109 36.132481 17.670605
409.3653 35.478619 16.997576
410.3295 34.852371 16.352268
411.29379 34.297451 15.778387
412.258 33.818901 15.280981
413.2222 33.372139 14.815468
414.18649 32.929409 14.354087
415.1507 32.42696 13.83309
416.1149 31.97027 13.357956
417.07919 31.608459 12.9778
418.0434 31.41 12.7611
419.0076 31.30295 12.63591
419.97189 31.21994 12.534861
420.9361 31.131519 12.428501
421.9003 31.039511 12.318654
422.86459 30.956671 12.218076
423.8288 30.881639 12.125408
424.793 30.785021 12.011253
425.75729 30.713579 11.922372
426.7215 30.7036 11.895054
427.6857 30.78709 11.961305
428.64999 30.92811 12.085182
429.6142 31.0938 12.233829
430.5784 31.33198 12.455067
431.54269 31.62203 12.72827
432.5069 31.8612 12.950691
433.4711 31.97436 13.047199
434.43539 31.92466 12.980945
435.3996 31.776279 12.816107
436.3638 31.57608 12.599547
437.32809 31.23065 12.237852
438.2923 30.85792 11.848954
439.2565 30.556641 11.531604
440.22079 30.44433 11.403316
441.185 30.46291 11.406014
442.14929 30.46236 11.389677
443.11349 30.330151 11.241776
444.0777 30.03661 10.932639
445.04199 29.67605 10.556577
446.0062 29.333549 10.198668
446.9704 29.024481 9.8742838
447.93469 28.73167 9.5662518
448.8989 28.442789 9.2622423
449.8631 28.095711 8.9001303
450.82739 27.741211 8.5306873
451.7916 27.46533 8.2399569
452.7558 27.36294 8.1228094
453.72009 27.447849 8.1930523
454.6843 27.58642 8.31705
455.6485 27.648621 8.364769
456.61279 27.53421 8.2359667
457.577 27.376431 8.0638876
458.5412 27.325541 7.9987884
459.50549 27.4993 8.1584282
460.4697 27.78826 8.4333591
461.4339 28.0396 8.670763
462.39819 28.139391 8.7567024
463.3624 28.09864 8.7021933
464.3266 28.03229 8.6221724
465.29089 28.041361 8.6176615
466.2551 28.15127 8.7140779
467.2193 28.32263 8.872035
468.18359 28.504589 9.0406761
469.1478 28.76849 9.2913494
470.112 29.033701 9.5434208
471.07629 29.202591 9.6992569
472.0405 29.150869 9.6345701
473.0047 28.929371 9.4001932
473.96899 28.71113 9.169158
474.9332 28.65283 9.0981541
475.8974 28.794769 9.2274742
476.86169 29.022869 9.4430389
477.8259 29.19121 9.5989323
478.7901 29.245581 9.6409407
479.75439 29.238831 9.621913
480.7186 29.24745 9.6183395
481.6828 29.229321 9.5881042
482.64709 29.217699 9.5644579
483.6113 29.28459 9.6194105
484.5755 29.52615 9.8491163
485.53979 29.94776 10.258954
486.504 30.413111 10.712617
487.4682 30.76675 11.054653
488.4325 30.952591 11.228971
489.3967 31.042351 11.307292
490.3609 31.18321 11.436795
491.3252 31.36117 11.603481
492.2894 31.58777 11.81889
493.2536 31.881241 12.101251
494.2179 32.283569 12.492549
495.1821 32.779758 12.97779
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1875 17.195499 0.60623884
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1899.106 17.2479 0.65111285
1900.0699 17.37641 0.77931148
1901.035 17.271589 0.67417943
1901.999 17.11949 0.52176791
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1905.856 17.080851 0.48187554
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1908.749 16.94804 0.34812015
1909.713 16.916981 0.31674528
1910.677 16.943291 0.34273928
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1912.605 17.17062 0.5694356
1913.5699 17.171459 0.56995761
1914.5341 17.039289 0.43747064
1915.498 16.97653 0.37439376
1916.462 17.02191 0.41945571
1917.427 17.138201 0.53542852
1918.391 17.196621 0.5935306
1919.355 17.166349 0.56294072
1920.319 17.10231 0.49858305
1921.2841 17.04002 0.43597388
1922.248 16.94874 0.34437522
1923.212 16.89827 0.29358608
1924.176 16.904739 0.29973692
1925.141 16.970461 0.36513916
1926.105 16.997511 0.3918702
1927.069 16.910801 0.30484122
1928.033 16.80983 0.20355102
1928.9969 16.807911 0.20131326
1929.962 17.06702 0.46010351
1930.926 17.298071 0.69083512
1931.89 17.41124 0.80368507
1932.854 17.35066 0.74278706
1933.819 17.33206 0.72386783
1934.783 17.47624 0.86772966
1935.7469 17.690029 1.0812005
1936.7111 17.755989 1.1468422
1937.676 17.48674 0.87727505
1938.64 17.15081 0.54102755
1939.604 16.89278 0.28268024
1940.568 16.67959 0.069173001
1941.532 16.59338 -0.017354112
1942.4969 16.75263 0.14157926
1943.4611 17.112 0.50063229
1944.425 17.366409 0.75472611
1945.389 17.36018 0.74818116
1946.354 17.218639 0.60632515
1947.318 17.07259 0.45996088
1948.282 16.89007 0.27712658
1949.246 16.76635 0.15309249
1950.2111 16.783159 0.16958813
1951.175 16.946939 0.33305535
1952.139 17.078051 0.46385393
1953.103 17.033331 0.41882223
1954.068 16.89134 0.27651978
1955.032 16.81498 0.19984815
1955.996 16.92091 0.30546811
1956.96 17.078699 0.46294752
1957.924 17.20875 0.59268904
1958.889 17.314819 0.69844967
1959.853 17.372391 0.75571316
1960.817 17.346609 0.72962427
1961.781 17.248211 0.63091946
1962.746 17.13409 0.51649278
1963.71 17.00305 0.38514709
1964.674 16.87776 0.25955272
1965.6379 16.778509 0.15999825
1966.603 16.681061 0.062246643
1967.567 16.65299 0.033874072
1968.531 16.82947 0.2100521
1969.495 17.21446 0.5947423
1970.459 17.51375 0.89373237
1971.424 17.53204 0.91172284
1972.3879 17.316851 0.69623595
1973.3521 17.18327 0.56235772
1974.316 17.164551 0.54334295
1975.281 17.189501 0.56799752
1976.245 17.148439 0.52664191
1977.209 17.02339 0.40129912
1978.173 16.90658 0.28419703
1979.1379 16.857679 0.23500489
1980.1021 16.885469 0.26250473
1981.066 16.90114 0.27788633
1982.03 16.901369 0.27782708
1982.995 16.887751 0.26392132
1983.959 16.85639 0.23227476
1984.923 16.78916 0.1647597
1985.887 16.74304 0.11835632
1986.851 16.769791 0.14482434
1987.816 16.923571 0.29832262
1988.78 17.00333 0.37780204
1989.744 16.946859 0.32105213
1990.708 16.782869 0.15678436
1991.673 16.74218 0.11581806
1992.637 16.962099 0.33546197
1993.601 17.201151 0.57423985
1994.5649 17.27113 0.64394575
1995.53 16.927179 0.29972374
1996.494 16.710951 0.083225131
1997.458 16.70237 0.074375205
1998.422 16.919411 0.29114881
1999.386 17.042259 0.41373125
2000.351 16.99548 0.3666867
2001.3149 16.893209 0.26415333
2002.2791 16.838831 0.20951298
2003.243 16.87636 0.24678157
2004.208 16.921289 0.29145187
2005.172 16.96068 0.33058497
2006.136 16.993191 0.36283976
2007.1 17.02725 0.39664483
2008.0649 17.07906 0.44820094
2009.0291 17.130341 0.4992305
2009.993 17.16078 0.52942002
2010.957 17.18471 0.5531013
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2013.85 16.893431 0.261087
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