#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 13:43:51 +0300 (Thu, 26 Apr 2018) $
#$Revision: 538 $
#$URL: svn://172.16.1.111/rod/cif/4/02/00/4020000.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4020000
loop_
_publ_author_name
'Morgenstern-Badarau I'
'Michel, A.'
_publ_section_title
;
 Sur l'existence d'un oxyhydroxyde double de fer(III) et d'etain(IV)
 Locality: synthetic
;
_journal_name_full               'Journal of Inorganic and Nuclear Chemistry'
_journal_page_first              1400
_journal_page_last               1402
_journal_paper_doi               10.1016/0022-1902(76)80168-6
_journal_volume                  38
_journal_year                    1976
_chemical_compound_source        R070724
_chemical_formula_sum            'Fe O6 Sn'
_chemical_name_mineral           Jeanbandyite
_space_group_IT_number           201
_symmetry_space_group_name_Hall  '-P 2ab 2bc 3'
_symmetry_space_group_name_H-M   'P n -3 :2'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   7.757
_cell_length_b                   7.757
_cell_length_c                   7.757
_cell_volume                     466.747
_exptl_crystal_density_diffrn    3.850
_cod_original_sg_symbol_H-M      'P n 3'
_cod_original_formula_sum        'Sn Fe O6'
_cod_database_code               9012832
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R070724.rod
_rod_data_source.block           3500000
_rod_database.code               4020000
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9012832 COD http://www.crystallography.net/cod/9012832.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
205.3402 0.0000000E+00
205.8223 42.08789
206.3044 65.18359
206.7865 98.62500
207.2687 59.15039
207.7508 13.22461
208.2329 17.75977
208.7150 6.677734
209.1971 105.4668
209.6792 193.3984
210.1614 180.4023
210.6435 101.9141
211.1256 35.06641
211.6077 9.615234
212.0898 14.24414
212.5719 28.00195
213.0541 55.98633
213.5362 79.80078
214.0183 84.16797
214.5004 74.72461
214.9825 64.91992
215.4646 60.36523
215.9468 61.46875
216.4289 69.84375
216.9110 89.92383
217.3931 110.6348
217.8752 123.2734
218.3573 130.8535
218.8395 142.2480
219.3216 163.8730
219.8037 195.1973
220.2858 231.5527
220.7679 293.7910
221.2500 336.9258
221.7322 319.2148
222.2143 260.2168
222.6964 219.9980
223.1785 260.5352
223.6606 387.0254
224.1427 484.1484
224.6249 541.3535
225.1070 576.7070
225.5891 577.9375
226.0712 556.9668
226.5533 547.1836
227.0354 581.5625
227.5176 666.0469
227.9997 744.9609
228.4818 829.5586
228.9639 898.3418
229.4460 929.4648
229.9281 930.8418
230.4103 932.3984
230.8924 963.5801
231.3745 1027.301
231.8566 1109.580
232.3387 1259.740
232.8208 1386.533
233.3030 1420.225
233.7851 1375.418
234.2672 1334.203
234.7493 1396.848
235.2314 1612.180
235.7135 1753.338
236.1957 1767.176
236.6778 1764.396
237.1599 1804.119
237.6420 1889.752
238.1241 1987.711
238.6062 2059.121
239.0884 2095.830
239.5705 2131.389
240.0526 2142.791
240.5347 2170.186
241.0168 2255.678
241.4989 2396.756
241.9811 2543.352
242.4632 2622.863
242.9453 2603.463
243.4274 2643.275
243.9095 2787.992
244.3916 2962.723
244.8738 3101.998
245.3559 3189.877
245.8380 3248.682
246.3201 3300.471
246.8022 3322.676
247.2843 3375.746
247.7665 3468.715
248.2486 3537.988
248.7307 3570.105
249.2128 3563.758
249.6949 3547.232
250.1770 3550.652
250.6592 3584.568
251.1413 3600.938
251.6234 3586.533
252.1055 3564.670
252.5876 3553.115
253.0697 3554.000
253.5519 3557.508
254.0340 3554.014
254.5161 3543.008
254.9982 3522.037
255.4803 3499.518
255.9624 3462.135
256.4445 3385.480
256.9267 3270.500
257.4088 3161.971
257.8909 3113.348
258.3730 3145.273
258.8551 3128.658
259.3372 3014.662
259.8194 2883.771
260.3015 2805.686
260.7836 2786.971
261.2657 2782.344
261.7478 2749.930
262.2299 2684.691
262.7121 2614.109
263.1942 2539.355
263.6763 2464.271
264.1584 2401.826
264.6405 2352.439
265.1227 2301.717
265.6048 2234.824
266.0869 2148.945
266.5690 2072.574
267.0511 2026.482
267.5332 1973.955
268.0154 1869.014
268.4975 1712.068
268.9796 1569.283
269.4617 1504.822
269.9438 1518.012
270.4259 1497.381
270.9081 1419.674
271.3902 1321.582
271.8723 1228.400
272.3544 1141.152
272.8365 1056.770
273.3186 973.6973
273.8008 891.2617
274.2829 805.2266
274.7650 701.3535
275.2471 604.5312
275.7292 542.7500
276.2113 513.5586
276.6935 475.9023
277.1756 394.8359
277.6577 279.4629
278.1398 197.6387
278.6219 175.0488
279.1040 164.9395
279.5862 134.2773
280.0683 85.15820
280.5504 39.21875
281.0325 13.17383
281.5146 0.3437500
281.9967 27.71094
282.4789 93.12500
282.9610 153.8613
283.4431 181.9707
283.9252 181.1680
284.4073 169.5918
284.8894 150.2988
285.3716 130.6758
285.8537 131.0938
286.3358 166.2246
286.8179 202.1094
287.3000 220.7480
287.7821 224.4688
288.2643 224.4062
288.7464 232.0977
289.2285 232.1875
289.7106 187.7832
290.1927 73.59375
290.6748 35.30859
291.1570 94.63086
291.6391 119.0859
292.1212 153.7031
292.6033 217.8125
293.0854 299.2812
293.5675 373.9453
294.0497 443.1230
294.5318 506.2207
295.0139 558.9688
295.4960 605.6074
295.9781 652.8672
296.4602 699.1211
296.9424 754.9160
297.4245 843.5469
297.9066 970.0840
298.3887 1093.896
298.8708 1190.393
299.3529 1277.932
299.8351 1392.627
300.3172 1548.174
300.7993 1717.396
301.2814 1857.305
301.7635 1961.828
302.2456 2089.551
302.7278 2270.152
303.2099 2474.838
303.6920 2658.840
304.1741 2811.137
304.6562 2962.986
305.1383 3151.066
305.6205 3375.445
306.1026 3620.328
306.5847 3891.910
307.0668 4178.945
307.5489 4471.053
308.0310 4768.084
308.5132 5069.375
308.9953 5376.680
309.4774 5690.494
309.9595 5998.393
310.4416 6275.631
310.9237 6564.027
311.4059 6903.406
311.8880 7291.330
312.3701 7694.227
312.8522 8096.326
313.3343 8492.053
313.8164 8861.986
314.2986 9188.852
314.7807 9504.350
315.2628 9830.488
315.7449 10161.72
316.2270 10480.30
316.7091 10775.72
317.1913 11046.66
317.6734 11290.81
318.1555 11490.75
318.6376 11687.85
319.1197 11917.72
319.6018 12157.97
320.0840 12356.71
320.5661 12485.99
321.0482 12560.02
321.5303 12619.70
322.0124 12690.41
322.4945 12717.56
322.9767 12662.38
323.4588 12563.21
323.9409 12484.33
324.4230 12452.27
324.9051 12429.53
325.3872 12335.88
325.8694 12110.97
326.3515 11922.55
326.8336 11827.83
327.3157 11754.71
327.7978 11618.10
328.2799 11398.83
328.7621 11157.28
329.2442 10979.52
329.7263 10922.86
330.2084 10783.85
330.6905 10483.69
331.1726 10162.03
331.6548 9928.705
332.1369 9789.504
332.6190 9664.779
333.1011 9468.949
333.5832 9181.438
334.0653 8939.672
334.5475 8779.184
335.0296 8622.371
335.5117 8423.932
335.9938 8193.359
336.4759 7970.453
336.9580 7788.371
337.4402 7645.445
337.9223 7475.074
338.4044 7248.287
338.8865 7027.391
339.3686 6830.309
339.8507 6648.803
340.3329 6468.252
340.8150 6281.162
341.2971 6090.732
341.7792 5902.121
342.2613 5714.646
342.7434 5532.625
343.2256 5347.875
343.7077 5171.535
344.1898 5019.797
344.6719 4899.396
345.1540 4793.504
345.6361 4664.957
346.1183 4498.814
346.6004 4338.984
347.0825 4189.855
347.5646 4050.531
348.0467 3921.193
348.5288 3801.734
349.0110 3691.242
349.4931 3595.162
349.9752 3517.980
350.4573 3435.688
350.9394 3338.266
351.4215 3240.986
351.9037 3146.373
352.3858 3056.871
352.8679 2978.551
353.3500 2924.926
353.8321 2894.666
354.3142 2837.383
354.7964 2743.746
355.2785 2631.660
355.7606 2489.668
356.2427 2336.797
356.7248 2209.879
357.2069 2139.107
357.6891 2103.266
358.1712 2039.363
358.6533 1930.602
359.1354 1830.830
359.6175 1775.662
360.0996 1736.209
360.5818 1675.701
361.0639 1574.750
361.5460 1467.619
362.0281 1401.170
362.5102 1377.893
362.9923 1370.420
363.4745 1401.562
363.9566 1423.209
364.4387 1380.637
364.9208 1261.418
365.4029 1131.668
365.8850 1027.377
366.3672 950.5918
366.8493 916.9102
367.3314 952.0156
367.8135 999.1504
368.2956 1000.385
368.7777 959.2402
369.2599 905.2051
369.7420 841.7227
370.2241 775.6406
370.7062 718.2617
371.1883 670.7539
371.6704 632.1602
372.1526 605.7676
372.6347 588.9395
373.1168 566.6016
373.5989 528.7988
374.0810 490.5781
374.5631 471.5840
375.0453 468.2070
375.5274 447.5391
376.0095 380.1797
376.4916 283.6758
376.9737 232.7441
377.4558 261.7402
377.9380 290.7129
378.4201 288.5879
378.9022 266.3867
379.3843 244.5801
379.8664 231.1191
380.3485 222.5469
380.8307 211.2461
381.3128 185.5020
381.7949 179.2949
382.2770 223.0762
382.7591 271.8184
383.2412 275.7832
383.7234 228.6328
384.2055 167.0586
384.6876 133.2324
385.1697 132.1387
385.6518 139.7871
386.1339 164.2148
386.6161 188.4043
387.0982 207.1914
387.5803 218.8320
388.0624 219.8398
388.5445 205.5742
389.0266 178.6680
389.5088 168.1582
389.9909 186.9160
390.4730 208.7500
390.9551 232.6074
391.4372 255.8555
391.9193 261.2578
392.4015 305.6035
392.8836 330.1074
393.3657 335.8633
393.8478 266.1582
394.3299 294.2461
394.8120 283.3320
395.2942 270.9668
395.7763 313.2422
396.2584 255.3008
396.7405 297.0488
397.2226 299.2500
397.7047 319.8047
398.1869 301.1719
398.6690 294.9141
399.1511 328.2520
399.6332 340.0176
400.1153 317.7344
400.5974 332.2051
401.0796 294.3867
401.5617 201.2324
402.0438 155.6270
402.5259 170.8633
403.0080 181.6465
403.4901 137.4844
403.9723 70.69531
404.4544 32.57812
404.9365 45.63477
405.4186 65.84180
405.9007 49.32031
406.3828 4.330078
406.8650 22.97266
407.3471 14.02734
407.8292 17.51367
408.3113 53.64648
408.7934 98.13867
409.2755 129.1191
409.7577 129.8457
410.2398 116.6191
410.7219 112.4492
411.2040 121.4043
411.6861 132.2812
412.1682 134.3262
412.6504 126.3105
413.1325 115.4727
413.6146 82.50195
414.0967 64.11133
414.5788 106.0918
415.0609 183.9141
415.5431 221.9707
416.0252 169.3906
416.5073 48.34961
416.9894 38.15820
417.4715 71.32031
417.9536 91.09766
418.4358 102.1934
418.9179 100.9453
419.4000 81.08008
419.8821 41.35352
420.3642 10.56641
420.8463 70.44141
421.3285 160.1621
421.8106 195.3203
422.2927 110.8926
422.7748 31.92383
423.2569 28.83594
423.7390 89.85547
424.2212 155.0410
424.7033 177.7559
425.1854 165.1758
425.6675 162.2148
426.1496 173.8496
426.6317 186.8730
427.1139 195.0801
427.5960 201.8574
428.0781 209.7949
428.5602 217.6094
429.0423 233.2969
429.5244 278.5625
430.0066 354.7324
430.4887 400.0938
430.9708 381.7500
431.4529 338.6738
431.9350 312.8145
432.4171 304.3223
432.8993 309.4004
433.3814 337.5801
433.8635 375.4355
434.3456 396.0215
434.8277 394.2168
435.3098 388.7461
435.7920 392.9375
436.2741 407.4082
436.7562 430.0625
437.2383 470.2148
437.7204 509.8789
438.2025 534.6113
438.6847 549.6602
439.1668 572.0020
439.6489 610.9473
440.1310 659.5410
440.6131 699.5215
441.0952 728.7266
441.5774 750.8594
442.0595 752.8242
442.5416 756.1602
443.0237 790.2637
443.5058 854.8184
443.9879 915.1504
444.4701 925.8516
444.9522 873.6719
445.4343 860.9355
445.9164 923.1543
446.3985 986.6348
446.8806 1033.348
447.3628 1063.316
447.8449 1077.539
448.3270 1075.938
448.8091 1073.277
449.2912 1097.070
449.7733 1153.420
450.2555 1210.975
450.7376 1271.939
451.2197 1318.691
451.7018 1332.572
452.1839 1314.355
452.6660 1297.455
453.1482 1302.762
453.6303 1327.623
454.1124 1371.256
454.5945 1446.203
455.0766 1512.715
455.5587 1533.115
456.0409 1519.316
456.5230 1499.018
457.0051 1468.217
457.4872 1443.221
457.9693 1432.660
458.4514 1433.816
458.9336 1451.018
459.4157 1496.029
459.8978 1559.861
460.3799 1603.793
460.8620 1616.020
461.3441 1623.020
461.8262 1632.143
462.3083 1640.451
462.7905 1646.820
463.2726 1647.672
463.7547 1635.072
464.2368 1595.717
464.7189 1522.996
465.2010 1482.807
465.6832 1501.020
466.1653 1520.965
466.6474 1529.680
467.1295 1526.756
467.6116 1512.768
468.0938 1487.533
468.5759 1453.395
469.0580 1416.293
469.5401 1375.244
470.0222 1335.252
470.5043 1296.912
470.9865 1260.389
471.4686 1225.305
471.9507 1191.465
472.4328 1159.133
472.9149 1129.098
473.3970 1101.344
473.8792 1076.201
474.3613 1055.336
474.8434 1030.326
475.3255 993.0039
475.8076 948.2363
476.2897 904.0410
476.7719 856.2109
477.2540 816.8164
477.7361 811.0469
478.2182 822.2305
478.7003 788.7754
479.1824 679.9316
479.6646 555.0078
480.1467 512.4863
480.6288 585.6426
481.1109 636.5938
481.5930 664.3555
482.0751 663.6113
482.5573 609.1973
483.0394 516.7383
483.5215 442.7793
484.0036 430.5898
484.4857 469.4707
484.9678 489.3223
485.4500 489.0703
485.9321 468.3379
486.4142 403.7305
486.8963 332.2207
487.3784 293.7480
487.8605 296.8398
488.3427 310.4180
488.8248 298.5273
489.3069 260.0645
489.7890 221.2129
490.2711 180.5547
490.7532 143.4980
491.2354 108.0645
491.7175 77.83984
492.1996 60.92578
492.6817 67.77539
493.1638 82.26953
493.6459 82.25586
494.1281 69.20898
494.6102 66.19922
495.0923 87.48828
495.5744 116.5039
496.0565 123.0332
496.5386 104.3789
497.0208 82.05859
497.5029 51.44336
497.9850 25.13477
498.4671 19.49219
498.9492 33.71094
499.4313 52.47070
499.9135 65.86133
500.3956 72.97070
500.8777 60.76367
501.3598 7.017578
501.8419 39.19922
502.3240 72.98242
502.8062 93.49609
503.2883 98.08789
503.7704 86.65820
504.2525 67.34766
504.7346 43.82031
505.2167 10.93945
505.6989 12.71094
506.1810 82.96289
506.6631 150.5977
507.1452 190.7891
507.6273 202.7402
508.1094 183.7930
508.5916 115.2109
509.0737 37.08203
509.5558 10.27148
510.0379 32.95898
510.5200 51.41992
511.0021 47.01562
511.4843 30.06836
511.9664 13.50391
512.4485 4.160156
512.9306 12.89062
513.4127 8.759766
513.8948 4.597656
514.3770 34.93359
514.8591 76.53125
515.3412 94.23633
515.8233 57.83594
516.3054 20.02734
516.7875 57.47266
517.2697 0.8867190
517.7518 31.75781
518.2339 1.701172
518.7160 48.64258
519.1981 73.56641
519.6802 67.08008
520.1624 66.19727
520.6445 131.0449
521.1266 265.3223
521.6087 308.0879
522.0908 197.5996
522.5729 85.04102
523.0551 35.38281
523.5372 27.25586
524.0193 29.00586
524.5014 31.97461
524.9835 39.68164
525.4656 60.19336
525.9478 90.18164
526.4299 111.6113
526.9120 118.4902
527.3941 119.0469
527.8762 119.9941
528.3583 120.9180
528.8405 131.9355
529.3226 171.1582
529.8047 205.5742
530.2868 204.9844
530.7689 181.0312
531.2510 169.0098
531.7332 187.6797
532.2153 223.2422
532.6974 240.1729
533.1795 215.1436
533.6616 214.7451
534.1437 271.7168
534.6259 324.2207
535.1080 324.0967
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