#------------------------------------------------------------------------------
#$Date: 2018-04-12 17:00:38 +0300 (Thu, 12 Apr 2018) $
#$Revision: 434 $
#$URL: svn://172.16.1.111/rod/cif/7/20/00/7200003.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7200003
loop_
_publ_author_name
'Schnering, H. G.'
'Nesper, R.'
'Pelshenke, H.'
_publ_section_title
;
 Sn21Cl16(OH)14O6, das sogenannte basische zinn(II)-clorid Locality:
 synthetic
;
_journal_name_full               'Zeitschrift fur Naturforschung B'
_journal_page_first              1551
_journal_page_last               1560
_journal_volume                  36
_journal_year                    1981
_chemical_formula_sum            'Cl16 H14 O20 Sn21'
_chemical_name_mineral           Abhurite
_space_group_IT_number           155
_symmetry_space_group_name_Hall  'R 3 2"'
_symmetry_space_group_name_H-M   'R 3 2 :H'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_length_a                   10.018
_cell_length_b                   10.018
_cell_length_c                   44.03
_cell_volume                     3826.849
_exptl_crystal_density_diffrn    4.418
_cod_original_sg_symbol_H-M      'R 3 2'
_cod_original_formula_sum        'Sn21 Cl16 O20 H14'
_cod_database_code               9009804
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            abhurite.rod
_rod_data_source.block
/var/www/html/rod/tmp/uploads/1523541542.7799-3D5DBAC35AF88B07.rod
_rod_database.code               7200003
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9009804 COD http://www.crystallography.net/cod/9009804.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
91.82715 0.0000000E+00
92.30927 31.98134
92.79138 0.8471250
93.27350 77.50757
93.75562 179.1463
94.23773 262.7868
94.71985 344.8448
95.20197 416.1551
95.68408 484.8727
96.16620 538.0795
96.64832 573.3671
97.13043 607.0661
97.61255 629.4664
98.09467 610.9578
98.57678 572.5031
99.05890 495.6049
99.54102 390.0825
100.0231 280.0151
100.5052 182.6078
100.9874 103.3462
101.4695 40.52100
101.9516 3.415306
102.4337 13.60025
102.9158 9.798512
103.3979 21.00814
103.8801 17.77219
104.3622 64.25665
104.8443 107.7665
105.3264 146.2668
105.8085 207.8214
106.2906 297.3848
106.7728 397.9781
107.2549 500.5750
107.7370 606.7121
108.2191 723.0694
108.7012 856.2199
109.1833 1006.024
109.6655 1163.183
110.1476 1321.229
110.6297 1483.554
111.1118 1660.328
111.5939 1857.279
112.0760 2059.134
112.5582 2262.927
113.0403 2467.033
113.5224 2636.613
114.0045 2761.373
114.4866 2840.200
114.9688 2842.070
115.4509 2728.363
115.9330 2550.304
116.4151 2322.202
116.8972 2049.055
117.3793 1756.824
117.8615 1470.936
118.3436 1179.780
118.8257 930.9579
119.3078 722.2639
119.7899 550.9741
120.2720 418.3689
120.7542 326.4984
121.2363 272.3028
121.7184 239.5643
122.2005 237.0599
122.6826 274.1317
123.1647 359.5161
123.6468 462.6115
124.1290 580.5257
124.6111 697.4951
125.0932 813.8602
125.5753 926.1539
126.0574 1030.597
126.5395 1124.542
127.0217 1219.754
127.5038 1298.518
127.9859 1359.340
128.4680 1396.206
128.9501 1420.256
129.4323 1435.571
129.9144 1442.547
130.3965 1441.870
130.8786 1433.847
131.3607 1418.424
131.8428 1397.174
132.3250 1367.485
132.8071 1332.353
133.2892 1298.479
133.7713 1266.178
134.2534 1236.714
134.7355 1214.040
135.2177 1198.868
135.6998 1190.424
136.1819 1186.102
136.6640 1186.473
137.1461 1193.518
137.6282 1210.564
138.1104 1238.236
138.5925 1270.241
139.0746 1309.228
139.5567 1350.535
140.0388 1392.768
140.5209 1435.743
141.0031 1480.383
141.4852 1528.602
141.9673 1584.923
142.4494 1632.342
142.9315 1679.554
143.4136 1714.325
143.8958 1730.428
144.3779 1725.709
144.8600 1699.947
145.3421 1651.953
145.8242 1575.696
146.3063 1484.229
146.7885 1372.219
147.2706 1246.647
147.7527 1113.800
148.2348 974.4969
148.7169 832.8892
149.1990 694.5090
149.6812 564.7768
150.1633 442.7401
150.6454 336.5638
151.1275 243.4452
151.6096 157.2554
152.0917 76.50257
152.5739 1.085449
153.0560 54.33736
153.5381 16.74458
154.0202 81.54396
154.5023 42.86637
154.9844 1.266388
155.4665 34.96826
155.9487 65.98396
156.4308 39.82304
156.9129 21.15089
157.3950 10.35508
157.8771 7.659554
158.3592 14.44947
158.8414 33.95680
159.3235 55.55768
159.8056 68.35833
160.2877 49.27166
160.7698 27.32800
161.2519 3.157654
161.7341 26.17110
162.2162 61.97791
162.6983 44.49500
163.1804 4.136467
163.6625 51.37122
164.1446 62.86815
164.6268 19.40132
165.1089 22.79763
165.5910 63.92882
166.0731 105.8933
166.5552 151.4946
167.0373 194.8780
167.5195 236.1762
168.0016 274.3962
168.4837 307.9641
168.9658 335.7717
169.4479 357.8624
169.9300 375.9553
170.4122 392.7512
170.8943 404.1144
171.3764 404.8542
171.8585 397.1356
172.3406 390.3018
172.8227 392.0617
173.3049 401.3611
173.7870 405.5305
174.2691 399.6856
174.7512 391.9814
175.2333 387.5187
175.7154 386.3551
176.1976 390.5657
176.6797 403.3124
177.1618 422.9417
177.6439 446.1350
178.1260 471.0368
178.6081 499.5576
179.0903 534.7569
179.5724 577.1128
180.0545 624.8284
180.5366 674.8723
181.0187 728.8593
181.5008 790.5214
181.9830 861.8524
182.4651 941.9101
182.9472 1028.918
183.4293 1124.997
183.9114 1225.381
184.3935 1327.645
184.8757 1431.740
185.3578 1538.484
185.8399 1648.623
186.3220 1762.052
186.8041 1874.349
187.2862 1985.094
187.7684 2095.502
188.2505 2205.528
188.7326 2315.441
189.2147 2425.865
189.6968 2536.755
190.1789 2648.500
190.6611 2760.316
191.1432 2870.634
191.6253 2983.130
192.1074 3097.570
192.5895 3214.600
193.0716 3336.267
193.5538 3463.706
194.0359 3597.760
194.5180 3734.947
195.0001 3871.995
195.4822 4014.145
195.9643 4164.074
196.4465 4321.297
196.9286 4484.606
197.4107 4652.397
197.8928 4825.179
198.3749 5000.832
198.8570 5180.792
199.3392 5362.077
199.8213 5544.909
200.3034 5728.934
200.7855 5909.276
201.2676 6084.331
201.7497 6253.034
202.2319 6405.464
202.7140 6548.445
203.1961 6670.911
203.6782 6767.124
204.1603 6837.372
204.6424 6871.247
205.1246 6856.068
205.6067 6794.573
206.0888 6691.361
206.5709 6543.479
207.0530 6355.285
207.5351 6128.943
208.0173 5859.889
208.4994 5565.910
208.9815 5247.118
209.4636 4912.719
209.9457 4582.056
210.4278 4254.558
210.9100 3930.758
211.3921 3622.151
211.8742 3325.956
212.3563 3047.845
212.8384 2787.102
213.3205 2540.632
213.8027 2307.881
214.2848 2091.914
214.7669 1891.879
215.2490 1711.047
215.7311 1554.118
216.2132 1410.935
216.6954 1276.238
217.1775 1149.740
217.6596 1030.431
218.1417 919.6687
218.6238 817.4741
219.1059 724.7370
219.5881 642.4355
220.0702 567.2755
220.5523 502.8159
221.0344 448.7700
221.5165 400.3339
221.9986 357.7961
222.4808 322.6154
222.9629 293.9604
223.4450 273.8916
223.9271 255.8083
224.4092 236.6565
224.8913 218.5778
225.3735 205.5848
225.8556 200.4991
226.3377 203.0513
226.8198 205.5848
227.3019 207.0820
227.7840 208.8633
228.2662 209.9930
228.7483 211.8236
229.2304 216.8772
229.7125 226.9212
230.1946 241.3993
230.6767 254.6436
231.1589 262.1096
231.6410 273.3243
232.1231 292.1698
232.6052 316.1867
233.0873 340.5128
233.5694 362.1090
234.0516 381.8956
234.5337 406.0701
235.0158 436.0825
235.4979 467.5857
235.9800 498.9346
236.4621 530.8679
236.9443 565.5518
237.4264 604.5667
237.9085 646.8649
238.3906 687.6378
238.8727 726.4703
239.3548 764.6127
239.8370 800.8145
240.3191 836.4187
240.8012 874.9199
241.2833 918.5928
241.7654 965.7275
242.2475 1011.299
242.7297 1055.031
243.2118 1098.018
243.6939 1139.134
244.1760 1179.380
244.6581 1221.907
245.1402 1268.332
245.6224 1317.442
246.1045 1366.544
246.5866 1415.508
247.0687 1465.096
247.5508 1516.348
248.0329 1568.237
248.5151 1618.740
248.9972 1667.744
249.4793 1714.731
249.9614 1759.862
250.4435 1803.766
250.9256 1843.658
251.4078 1879.662
251.8899 1910.920
252.3720 1934.665
252.8541 1950.518
253.3362 1956.951
253.8183 1954.386
254.3005 1943.009
254.7826 1924.002
255.2647 1898.507
255.7468 1866.202
256.2289 1825.126
256.7110 1773.645
257.1931 1713.985
257.6753 1648.850
258.1574 1578.608
258.6395 1505.385
259.1216 1428.791
259.6037 1349.864
260.0858 1273.217
260.5680 1200.047
261.0501 1128.789
261.5322 1056.960
262.0143 985.4205
262.4964 916.7925
262.9785 853.1155
263.4607 794.1394
263.9428 736.2051
264.4249 678.1680
264.9070 623.7670
265.3891 574.5850
265.8712 529.6978
266.3534 487.4971
266.8355 446.6199
267.3176 407.7378
267.7997 373.6928
268.2818 347.1273
268.7639 321.6671
269.2461 294.7535
269.7282 267.3234
270.2103 240.5457
270.6924 214.8234
271.1745 190.4204
271.6566 168.7406
272.1388 150.9665
272.6209 134.4018
273.1030 118.1080
273.5851 102.4102
274.0672 87.99615
274.5493 75.09391
275.0315 63.40903
275.5136 52.42397
275.9957 42.23415
276.4778 32.52089
276.9599 23.03049
277.4420 13.97857
277.9242 5.692280
278.4063 1.805752
278.8884 8.885714
279.3705 16.66764
279.8526 26.55482
280.3347 34.02702
280.8169 30.65381
281.2990 27.16154
281.7811 22.89777
282.2632 17.26694
282.7453 10.67161
283.2274 3.369493
283.7096 5.723534
284.1917 12.56247
284.6738 16.50076
285.1559 13.71047
285.6380 12.02331
286.1201 11.36087
286.6023 10.27385
287.0844 6.845697
287.5665 0.3036730
288.0486 5.252811
288.5307 10.45202
289.0128 14.26550
289.4950 15.40454
289.9771 14.42898
290.4592 13.19607
290.9413 13.44252
291.4234 15.32705
291.9055 16.58734
292.3877 13.25206
292.8698 10.48269
293.3519 8.765200
293.8340 7.836241
294.3161 7.128291
294.7982 6.248839
295.2804 5.214993
295.7625 4.399420
296.2446 3.077794
296.7267 2.802969
297.2088 4.705861
297.6909 7.695771
298.1731 7.448062
298.6552 4.945288
299.1373 3.514758
299.6194 2.628904
300.1015 3.038516
300.5836 3.086317
301.0658 2.989550
301.5479 2.309512
302.0300 0.3232060
302.5121 3.222212
302.9942 7.472474
303.4763 3.728704
303.9585 2.035247
304.4406 0.1845060
304.9227 0.2447320
305.4048 4.005258
305.8869 8.447657
306.3690 13.03881
306.8512 17.88420
307.3333 23.13160
307.8154 28.84246
308.2975 34.86273
308.7796 41.43470
309.2617 48.07228
309.7439 54.49190
310.2260 60.67753
310.7081 66.78660
311.1902 73.02039
311.6723 79.53097
312.1544 85.14606
312.6366 89.11774
313.1187 93.07539
313.6008 97.14423
314.0829 101.6989
314.5650 107.4444
315.0471 114.9557
315.5293 124.1167
316.0114 133.4071
316.4935 144.2590
316.9756 153.6812
317.4577 160.0166
317.9398 164.7191
318.4220 169.8937
318.9041 176.6128
319.3862 184.5020
319.8683 192.4538
320.3504 201.0206
320.8326 208.8411
321.3147 214.8038
321.7968 220.4980
322.2789 227.6613
322.7610 236.7803
323.2431 246.8963
323.7253 256.2988
324.2074 264.4136
324.6895 272.9723
325.1716 282.4475
325.6537 291.9868
326.1358 301.2249
326.6180 310.0119
327.1001 318.1989
327.5822 325.5097
328.0643 331.5183
328.5464 338.3814
329.0285 346.8501
329.5107 355.3359
329.9928 363.0784
330.4749 370.2880
330.9570 377.6339
331.4391 385.6947
331.9212 394.3805
332.4034 402.2613
332.8855 409.3661
333.3676 415.6366
333.8497 420.2831
334.3318 424.2647
334.8139 428.7841
335.2961 434.4087
335.7782 441.0597
336.2603 448.5238
336.7424 459.1010
337.2245 466.0647
337.7066 466.5645
338.1888 464.8199
338.6709 464.6505
339.1530 467.0373
339.6351 471.2466
340.1172 476.4121
340.5993 483.1096
341.0815 489.2293
341.5636 494.0710
342.0457 498.2177
342.5278 501.8741
343.0099 505.6289
343.4920 509.9492
343.9742 515.5778
344.4563 522.7311
344.9384 528.2725
345.4205 528.3965
345.9026 529.9042
346.3847 535.9127
346.8669 544.5394
347.3490 552.3125
347.8311 556.9006
348.3132 559.5312
348.7953 565.1136
349.2774 576.8441
349.7596 586.5712
350.2417 591.1661
350.7238 594.3141
351.2059 599.9306
351.6880 609.3153
352.1701 620.1722
352.6523 628.6633
353.1344 634.1396
353.6165 639.3353
354.0986 644.8825
354.5807 650.0706
355.0628 654.5033
355.5450 657.9371
356.0271 660.3441
356.5092 661.6080
356.9913 661.6315
357.4734 661.3453
357.9555 660.4714
358.4377 659.4099
358.9198 658.7474
359.4019 658.0948
359.8840 656.6094
360.3661 653.8406
360.8482 649.8736
361.3304 645.5258
361.8125 640.7494
362.2946 634.9075
362.7767 627.7320
363.2588 619.9811
363.7409 611.8414
364.2231 603.2080
364.7052 594.7879
365.1873 588.4361
365.6694 584.5848
366.1515 577.4361
366.6336 563.1526
367.1158 547.3624
367.5979 534.5555
368.0800 524.6728
368.5621 514.2836
369.0442 499.9726
369.5263 482.7798
370.0085 468.0444
370.4906 457.1992
370.9727 446.9882
371.4548 435.1115
371.9369 422.1899
372.4190 409.4426
372.9012 397.8469
373.3833 386.4358
373.8654 373.2756
374.3475 358.1062
374.8296 343.9254
375.3117 332.4977
375.7939 322.9561
376.2760 314.1461
376.7581 306.4012
377.2402 298.2411
377.7223 288.3582
378.2044 277.0731
378.6866 265.6525
379.1687 254.1451
379.6508 242.9960
380.1329 232.7809
380.6150 223.4872
381.0971 214.4792
381.5793 205.4790
382.0614 196.6254
382.5435 188.1053
383.0256 179.8976
383.5077 172.1549
383.9898 165.0710
384.4720 158.5857
384.9541 151.8163
385.4362 143.9589
385.9183 136.5588
386.4004 130.9692
386.8825 126.7401
387.3647 122.3541
387.8468 117.2901
388.3289 111.3674
388.8110 103.7082
389.2931 92.64999
389.7752 83.60978
390.2574 79.18950
390.7395 76.71451
391.2216 72.97153
391.7037 67.26989
392.1858 60.92194
392.6679 55.46360
393.1501 51.11092
393.6322 46.60478
394.1143 40.38041
394.5964 35.38885
395.0785 34.92428
395.5606 37.37597
396.0428 37.73742
396.5249 32.46086
397.0070 22.94995
397.4891 16.59412
397.9712 16.67539
398.4533 16.09204
398.9355 13.46099
399.4176 10.07912
399.8997 7.446867
400.3818 6.007747
400.8639 4.979581
401.3460 3.128357
401.8282 2.2157000E-02
402.3103 2.666578
402.7924 0.8988890
403.2745 0.7770070
403.7566 1.426680
404.2387 0.5160800
404.7209 0.1211160
405.2030 0.5237440
405.6851 0.7496860
406.1672 1.219702
406.6493 2.297726
407.1314 3.004376
407.6136 2.773956
408.0957 2.901816
408.5778 2.761233
409.0599 2.029436
409.5420 1.408069
410.0241 1.693708
410.5063 2.923640
410.9884 1.995307
411.4705 2.123657
411.9526 2.672352
412.4347 2.338300
412.9168 1.073444
413.3990 0.3999370
413.8811 1.607135
414.3632 2.002531
414.8453 1.633184
415.3274 1.851079
415.8095 0.6582040
416.2917 0.1666790
416.7738 0.4495890
417.2559 0.1452260
417.7380 0.7606680
418.2201 0.9574590
418.7022 1.498975
419.1844 0.9502140
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