#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 13:28:26 +0300 (Thu, 26 Apr 2018) $
#$Revision: 474 $
#$URL: svn://172.16.1.111/rod/cif/8/10/00/8100005.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_8100005
loop_
_publ_author_name
'Boucher, M. L.'
'Peacor, D. R.'
_publ_section_title
;
 The crystal structure of alamosite, PbSiO3 Locality: Alamos, Sonora,
 Mexico
;
_journal_name_full               'Zeitschrift fur Kristallographie'
_journal_page_first              98
_journal_page_last               111
_journal_volume                  126
_journal_year                    1968
_chemical_compound_source        R060067
_chemical_formula_sum            'O3 Pb Si'
_chemical_name_mineral           Alamosite
_space_group_IT_number           13
_symmetry_space_group_name_Hall  '-P 2yac'
_symmetry_space_group_name_H-M   'P 1 2/n 1'
_cell_angle_alpha                90
_cell_angle_beta                 113.25
_cell_angle_gamma                90
_cell_length_a                   11.23
_cell_length_b                   7.08
_cell_length_c                   12.26
_cell_volume                     895.613
_exptl_crystal_density_diffrn    6.303
_cod_original_formula_sum        'Pb Si O3'
_cod_database_code               9008141
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060067.rod
_rod_data_source.block           3500000
_rod_database.code               8100005
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9008141 COD http://www.crystallography.net/cod/9008141.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
130.6109 0.0000000E+00
131.0930 1.706848
131.5751 0.2502440
132.0572 0.4564210
132.5394 0.8118900
133.0215 3.603027
133.5036 8.954468
133.9857 16.42114
134.4678 26.74500
134.9499 40.03381
135.4321 56.16187
135.9142 75.24060
136.3963 97.38684
136.8784 122.2638
137.3605 147.6301
137.8426 173.9332
138.3248 200.3143
138.8069 227.7117
139.2890 255.6038
139.7711 281.0233
140.2532 302.3632
140.7353 319.5788
141.2175 333.1367
141.6996 347.5833
142.1817 357.0287
142.6638 355.0524
143.1459 340.8149
143.6280 318.6010
144.1102 287.1956
144.5923 250.2405
145.0744 212.9385
145.5565 175.4863
146.0386 139.2382
146.5207 108.2145
147.0029 83.87744
147.4850 63.30164
147.9671 44.13116
148.4492 26.89539
148.9313 12.74622
149.4134 2.296082
149.8955 4.476196
150.3777 6.943542
150.8598 2.539612
151.3419 4.492126
151.8240 12.76917
152.3061 22.47363
152.7882 34.66278
153.2704 50.64960
153.7525 71.26929
154.2346 93.20941
154.7167 116.6211
155.1988 141.0802
155.6809 166.6169
156.1631 193.2252
156.6452 220.5957
157.1273 248.7396
157.6094 280.8666
158.0915 305.9523
158.5736 319.8892
159.0558 328.9396
159.5379 339.3411
160.0200 352.7003
160.5021 366.1627
160.9842 374.4983
161.4663 376.3759
161.9485 378.6415
162.4306 381.2184
162.9127 385.3766
163.3948 393.6160
163.8769 406.9987
164.3590 424.7471
164.8412 445.3528
165.3233 469.0049
165.8054 494.0367
166.2875 522.2762
166.7696 552.6776
167.2517 577.0724
167.7339 594.4892
168.2160 602.1539
168.6981 597.6514
169.1802 580.0151
169.6623 554.5920
170.1444 526.1760
170.6266 494.8704
171.1087 460.2443
171.5908 417.9202
172.0729 374.6870
172.5550 334.0341
173.0371 296.9265
173.5193 264.3871
174.0014 237.5659
174.4835 217.0007
174.9656 202.1192
175.4477 192.9684
175.9298 188.0511
176.4120 186.7953
176.8941 188.9796
177.3762 193.5267
177.8583 197.4866
178.3404 200.5721
178.8225 203.3959
179.3047 206.1719
179.7868 208.9355
180.2689 212.1843
180.7510 216.2560
181.2331 220.3409
181.7152 219.8824
182.1974 213.4167
182.6795 203.8493
183.1616 191.9971
183.6437 177.5507
184.1258 160.1124
184.6079 139.3060
185.0900 115.7601
185.5722 96.10822
186.0543 81.28033
186.5364 68.79089
187.0185 56.87988
187.5006 45.84406
187.9827 36.14648
188.4649 27.95221
188.9470 22.76508
189.4291 21.32135
189.9112 24.92474
190.3933 30.82129
190.8754 37.76306
191.3576 45.73114
191.8397 54.19635
192.3218 63.23694
192.8039 72.47815
193.2860 81.15894
193.7681 89.28613
194.2503 96.81366
194.7324 103.8137
195.2145 110.3744
195.6966 115.8788
196.1787 119.0374
196.6608 121.1433
197.1430 123.6373
197.6251 127.0352
198.1072 130.9207
198.5893 134.3147
199.0714 136.5327
199.5535 140.2031
200.0357 147.0938
200.5178 155.6705
200.9999 164.1313
201.4820 171.4147
201.9641 178.4554
202.4462 187.9060
202.9284 200.7655
203.4105 214.6738
203.8926 229.5259
204.3747 244.6875
204.8568 259.0246
205.3389 271.4926
205.8211 283.1730
206.3032 298.7787
206.7853 320.8417
207.2674 344.3195
207.7495 369.0341
208.2316 394.2962
208.7138 419.5119
209.1959 444.1854
209.6780 468.3979
210.1601 492.1917
210.6422 516.8802
211.1243 539.6971
211.6065 560.7968
212.0886 579.6481
212.5707 595.6494
213.0528 608.5217
213.5349 618.0778
214.0170 621.6395
214.4992 619.2375
214.9813 611.6346
215.4634 597.9599
215.9455 579.1591
216.4276 556.5283
216.9097 530.7238
217.3919 501.9874
217.8740 472.8623
218.3561 442.0546
218.8382 412.3713
219.3203 385.6207
219.8024 361.0805
220.2845 336.5436
220.7667 310.3256
221.2488 283.0405
221.7309 258.1371
222.2130 235.4049
222.6951 214.9286
223.1772 197.1944
223.6594 181.9031
224.1415 167.7653
224.6236 154.1616
225.1057 141.1111
225.5878 128.4230
226.0699 115.6145
226.5521 103.6254
227.0342 93.47983
227.5163 84.96027
227.9984 76.00388
228.4805 64.47440
228.9626 52.42099
229.4448 43.76236
229.9269 40.29416
230.4090 37.94022
230.8911 32.95883
231.3732 25.36069
231.8553 18.26636
232.3375 12.95941
232.8196 9.055145
233.3017 6.392090
233.7838 5.430145
234.2659 4.514038
234.7480 1.484039
235.2302 3.969940
235.7123 8.509888
236.1944 10.05853
236.6765 10.57938
237.1586 11.70685
237.6407 13.82922
238.1229 16.09052
238.6050 17.59628
239.0871 18.33823
239.5692 18.29831
240.0513 16.42563
240.5334 14.36508
241.0156 13.44952
241.4977 13.98306
241.9798 14.78104
242.4619 14.24777
242.9440 12.07895
243.4261 9.734100
243.9083 7.756714
244.3904 5.490631
244.8725 2.252533
245.3546 1.969604
245.8367 6.344360
246.3188 9.651642
246.8010 11.48434
247.2831 13.55954
247.7652 16.22644
248.2473 19.06543
248.7294 21.61484
249.2115 23.91101
249.6937 26.56467
250.1758 30.57901
250.6579 36.79959
251.1400 42.02304
251.6221 45.10071
252.1042 48.20035
252.5864 52.70969
253.0685 58.69522
253.5506 65.07602
254.0327 70.54291
254.5148 74.61752
254.9969 79.26407
255.4790 84.56061
255.9612 90.26706
256.4433 96.24341
256.9254 102.4763
257.4075 109.0515
257.8896 115.9858
258.3718 123.1504
258.8539 131.3017
259.3360 140.6218
259.8181 150.5085
260.3002 160.5885
260.7823 170.9138
261.2645 181.8674
261.7466 193.8978
262.2287 207.2073
262.7108 220.0724
263.1929 231.9096
263.6750 243.9044
264.1572 257.1774
264.6393 271.3394
265.1214 285.0921
265.6035 297.6487
266.0856 308.9917
266.5677 317.6711
267.0499 323.9610
267.5320 328.1045
268.0141 330.7385
268.4962 331.4873
268.9783 329.0290
269.4604 322.2080
269.9426 311.2674
270.4247 299.7996
270.9068 288.2289
271.3889 275.8189
271.8710 261.6186
272.3531 246.3015
272.8352 231.3489
273.3174 217.4805
273.7995 204.7434
274.2816 193.4671
274.7637 185.2063
275.2458 176.3133
275.7279 165.4510
276.2101 153.1518
276.6922 140.3099
277.1743 126.9692
277.6564 113.9091
278.1385 103.4359
278.6206 96.81723
279.1028 89.88297
279.5849 80.85376
280.0670 70.86832
280.5491 61.62448
281.0312 53.54132
281.5133 47.01678
281.9955 43.52484
282.4776 43.94455
282.9597 43.47244
283.4418 39.88620
283.9239 34.94843
284.4060 31.44803
284.8882 30.14423
285.3703 30.02393
285.8524 29.86700
286.3345 29.62875
286.8166 29.56403
287.2987 29.90143
287.7809 30.40112
288.2630 30.57086
288.7451 30.23187
289.2272 30.17279
289.7093 31.45975
290.1914 34.00714
290.6736 36.33273
291.1557 38.23358
291.6378 39.87796
292.1199 41.23215
292.6020 42.15784
293.0841 43.00180
293.5663 44.20230
294.0484 45.96381
294.5305 48.22656
295.0126 51.07614
295.4947 54.22443
295.9768 57.67950
296.4590 61.44858
296.9411 65.02130
297.4232 68.33667
297.9053 71.19254
298.3874 73.00089
298.8695 72.79895
299.3517 72.35434
299.8338 73.65021
300.3159 76.34399
300.7980 77.57114
301.2801 75.94730
301.7622 71.84506
302.2444 66.17902
302.7265 57.59885
303.2086 50.91980
303.6907 50.54501
304.1728 54.55203
304.6549 56.00803
305.1371 51.96429
305.6192 45.47174
306.1013 40.78882
306.5834 37.85815
307.0655 36.16528
307.5476 36.13095
308.0298 37.14407
308.5119 37.61972
308.9940 36.91296
309.4761 36.32578
309.9582 37.33356
310.4403 39.74484
310.9225 43.04761
311.4046 48.22507
311.8867 53.83188
312.3688 57.19727
312.8509 57.69659
313.3330 57.98135
313.8152 60.82516
314.2973 65.37741
314.7794 68.79001
315.2615 69.30280
315.7436 69.14206
316.2257 71.08960
316.7079 75.29025
317.1900 79.11362
317.6721 81.02310
318.1542 81.30896
318.6363 81.04590
319.1184 81.08728
319.6006 79.61728
320.0827 74.91541
320.5648 67.24023
321.0469 58.39209
321.5290 48.53076
322.0111 38.33624
322.4933 28.75250
322.9754 19.45413
323.4575 11.63992
323.9396 6.585663
324.4217 3.596863
324.9038 0.3439330
325.3860 4.341400
325.8681 8.512421
326.3502 9.240295
326.8323 6.668213
327.3144 3.433868
327.7965 0.6845700
328.2787 2.192932
328.7608 6.244904
329.2429 11.68161
329.7250 17.99316
330.2071 24.89404
330.6892 32.31683
331.1714 40.03830
331.6535 48.37744
332.1356 56.79575
332.6177 64.47659
333.0998 71.38654
333.5819 78.56564
334.0641 86.80463
334.5462 95.88626
335.0283 104.8886
335.5104 112.7481
335.9925 121.5316
336.4746 133.5100
336.9568 147.9521
337.4389 160.9249
337.9210 169.9633
338.4031 177.3078
338.8852 188.4526
339.3673 204.7390
339.8495 220.9114
340.3316 233.9865
340.8137 245.4822
341.2958 258.6595
341.7779 274.5935
342.2600 291.7967
342.7421 308.0023
343.2242 322.8652
343.7064 339.3875
344.1885 359.2769
344.6706 380.5346
345.1527 401.3394
345.6348 421.4902
346.1169 440.4337
346.5991 457.7335
347.0812 473.2112
347.5633 487.1594
348.0454 500.2328
348.5275 511.4050
349.0096 520.4987
349.4918 527.2648
349.9739 530.8757
350.4560 531.2745
350.9381 527.8053
351.4202 517.5281
351.9023 497.5900
352.3845 475.5547
352.8666 454.4191
353.3487 432.5498
353.8308 406.3209
354.3129 373.9297
354.7950 338.7769
355.2772 307.2209
355.7593 280.2817
356.2414 254.9500
356.7235 230.9541
357.2056 208.5306
357.6877 188.2420
358.1699 170.0617
358.6520 153.3055
359.1341 137.0404
359.6162 121.0883
360.0983 107.4187
360.5804 96.02524
361.0626 86.74820
361.5447 79.75262
362.0268 74.78033
362.5089 71.14835
362.9910 68.40741
363.4731 66.44611
363.9553 64.85852
364.4374 62.98489
364.9195 62.37088
365.4016 64.50461
365.8837 67.62927
366.3658 69.24905
366.8480 68.34570
367.3301 66.00671
367.8122 64.58301
368.2943 65.04767
368.7764 64.79245
369.2585 63.66162
369.7407 62.06009
370.2228 60.23279
370.7049 58.22342
371.1870 55.95575
371.6691 53.19534
372.1512 49.68106
372.6334 47.39105
373.1155 46.96341
373.5976 47.06479
374.0797 47.15311
374.5618 47.40045
375.0439 48.29190
375.5261 50.18982
376.0082 52.92841
376.4903 55.66617
376.9724 58.22034
377.4545 61.07025
377.9366 64.07498
378.4188 67.49249
378.9009 71.73639
379.3830 76.91348
379.8651 82.51041
380.3472 87.78189
380.8293 92.95459
381.3115 97.13531
381.7936 100.1102
382.2757 102.1873
382.7578 103.4070
383.2399 103.7780
383.7220 103.4143
384.2042 102.6517
384.6863 101.4892
385.1684 98.90359
385.6505 93.90515
386.1326 88.69821
386.6147 84.34744
387.0969 80.36801
387.5790 76.02606
388.0611 71.01547
388.5432 65.35181
389.0253 58.69452
389.5074 50.59085
389.9896 43.36319
390.4717 38.19989
390.9538 34.03958
391.4359 30.00986
391.9180 25.96582
392.4001 22.65646
392.8823 20.89938
393.3644 20.50885
393.8465 20.40326
394.3286 20.66272
394.8107 20.78732
395.2928 20.13663
395.7750 18.95493
396.2571 18.14822
396.7392 18.93073
397.2213 19.89206
397.7034 18.32950
398.1855 13.95322
398.6677 10.58752
399.1498 10.88791
399.6319 13.63538
400.1140 15.73178
400.5961 16.63452
401.0782 17.59818
401.5604 19.50012
402.0425 22.05902
402.5246 24.52060
403.0067 26.70242
403.4888 28.56137
403.9709 29.90805
404.4531 30.69559
404.9352 31.56253
405.4173 32.70474
405.8994 33.92688
406.3815 35.06461
406.8636 36.09451
407.3458 37.04678
407.8279 38.02444
408.3100 38.97165
408.7921 39.15387
409.2742 38.02902
409.7563 36.85550
410.2385 36.26004
410.7206 35.91022
411.2027 35.23141
411.6848 33.98721
412.1669 32.27036
412.6490 30.29321
413.1311 28.44012
413.6133 25.54510
414.0954 20.59290
414.5775 15.38843
415.0596 11.04596
415.5417 7.780762
416.0238 5.447327
416.5060 4.066376
416.9881 3.690491
417.4702 2.504578
417.9523 0.1913760
418.4344 2.990631
418.9165 6.192474
419.3987 9.125458
419.8808 10.70282
420.3629 10.37830
420.8450 9.147705
421.3271 9.243347
421.8092 11.50079
422.2914 12.96088
422.7735 12.79193
423.2556 12.17444
423.7377 12.01691
424.2198 12.24600
424.7019 11.92661
425.1841 10.14249
425.6662 7.002502
426.1483 3.594757
426.6304 0.4027400
427.1125 4.118225
427.5946 6.946442
428.0768 9.342224
428.5589 11.91785
429.0410 14.86749
429.5231 18.13910
430.0052 21.81335
430.4873 25.90543
430.9695 29.76431
431.4516 33.10034
431.9337 36.21295
432.4158 39.36002
432.8979 42.54517
433.3800 45.93942
433.8622 49.57965
434.3443 53.49023
434.8264 57.70123
435.3085 62.18893
435.7906 67.11713
436.2727 72.52237
436.7549 78.54794
437.2370 85.44949
437.7191 93.69220
438.2012 102.3290
438.6833 110.9648
439.1654 119.6274
439.6476 128.2884
440.1297 136.8508
440.6118 145.8180
441.0939 156.3147
441.5760 169.5871
442.0581 180.8661
442.5403 190.0858
443.0224 197.1327
443.5045 201.8335
443.9866 204.2389
444.4687 204.6913
444.9508 203.6364
445.4330 200.8626
445.9151 193.7221
446.3972 178.5170
446.8793 163.2875
447.3614 148.9218
447.8435 135.2567
448.3257 121.8810
448.8078 108.7219
449.2899 96.13559
449.7720 84.54169
450.2541 73.78299
450.7362 64.71564
451.2184 57.42667
451.7005 51.83630
452.1826 48.81534
452.6647 47.56393
453.1468 46.17734
453.6289 43.31033
454.1111 39.68976
454.5932 37.36728
455.0753 36.37259
455.5574 36.58072
456.0395 38.48303
456.5216 41.32578
457.0038 44.59448
457.4859 48.21945
457.9680 52.31888
458.4501 57.18585
458.9322 62.60291
459.4143 67.58014
459.8965 71.59381
460.3786 76.42297
460.8607 84.18228
461.3428 93.91983
461.8249 103.2524
462.3070 111.7157
462.7892 119.6062
463.2713 127.6448
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