#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 13:44:23 +0300 (Thu, 26 Apr 2018) $
#$Revision: 546 $
#$URL: svn://172.16.1.111/rod/cif/8/10/00/8100009.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_8100009
loop_
_publ_author_name
'Sahl, K.'
_publ_section_title
;
 Zur kristallstruktur von lanarkit, Pb2O(SO4) Locality: synthetic
;
_journal_name_full               'Zeitschrift fur Kristallographie'
_journal_page_first              99
_journal_page_last               117
_journal_volume                  132
_journal_year                    1970
_chemical_compound_source        R080116
_chemical_formula_sum            'O5 Pb2 S'
_chemical_name_mineral           Lanarkite
_space_group_IT_number           12
_symmetry_space_group_name_Hall  '-C 2y'
_symmetry_space_group_name_H-M   'C 1 2/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 115.93
_cell_angle_gamma                90
_cell_length_a                   13.769
_cell_length_b                   5.698
_cell_length_c                   7.079
_cell_volume                     499.477
_exptl_crystal_density_diffrn    7.001
_cod_original_formula_sum        'Pb2 S O5'
_cod_database_code               9011421
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R080116.rod
_rod_data_source.block           3500000
_rod_database.code               8100009
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9011421 COD http://www.crystallography.net/cod/9011421.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
130.1285 0.0000000E+00
130.6107 1.286377
131.0928 3.482605
131.5749 8.562561
132.0570 12.51794
132.5391 17.29224
133.0212 24.74615
133.5034 33.97345
133.9855 47.51489
134.4676 63.56665
134.9497 83.89539
135.4318 109.2048
135.9139 139.4622
136.3960 174.6121
136.8782 214.7524
137.3603 260.4714
137.8424 310.0822
138.3245 363.6757
138.8066 421.0039
139.2887 481.0720
139.7709 543.0171
140.2530 609.1965
140.7351 681.5118
141.2172 758.5316
141.6993 845.0039
142.1814 940.5399
142.6636 1045.956
143.1457 1164.253
143.6278 1289.923
144.1099 1438.347
144.5920 1613.054
145.0741 1814.363
145.5563 2052.744
146.0384 2342.054
146.5205 2684.536
147.0026 3051.168
147.4847 3519.100
147.9668 3957.344
148.4490 4329.241
148.9311 4614.863
149.4132 4760.188
149.8953 4665.777
150.3774 4231.477
150.8595 3733.966
151.3417 3133.586
151.8238 2528.942
152.3059 1989.036
152.7880 1543.362
153.2701 1182.140
153.7522 888.6537
154.2344 706.0048
154.7165 555.4662
155.1986 442.4578
155.6807 357.1944
156.1628 290.1232
156.6449 237.6781
157.1271 197.8450
157.6092 164.5953
158.0913 138.4686
158.5734 116.7905
159.0555 100.0179
159.5376 86.44571
160.0198 73.91685
160.5019 62.04465
160.9840 51.30838
161.4661 42.39598
161.9482 35.85379
162.4303 30.28683
162.9125 24.95862
163.3946 19.93422
163.8767 15.37733
164.3588 11.44879
164.8409 8.131760
165.3230 5.327103
165.8052 3.128159
166.2873 1.366074
166.7694 2.9450001E-03
167.2515 0.8604280
167.7336 1.617294
168.2157 2.596344
168.6979 3.569778
169.1800 4.229797
169.6621 4.379089
170.1442 4.203888
170.6263 4.246048
171.1084 4.663330
171.5906 5.033142
172.0727 5.085632
172.5548 5.047928
173.0369 5.319580
173.5190 6.253052
174.0011 7.679970
174.4833 8.302505
174.9654 7.034966
175.4475 5.990059
175.9296 5.672333
176.4117 5.923088
176.8938 6.393860
177.3760 6.870247
177.8581 7.360634
178.3402 7.719604
178.8223 7.927719
179.3044 8.037552
179.7865 7.995102
180.2687 7.849663
180.7508 7.710381
181.2329 7.647827
181.7150 7.662323
182.1971 7.829903
182.6792 8.390976
183.1614 8.883034
183.6435 8.934914
184.1256 8.574455
184.6077 8.240036
185.0898 8.364426
185.5719 8.978584
186.0541 9.399147
186.5362 9.459488
187.0183 9.404877
187.5004 9.460411
187.9825 7.115494
188.4646 4.643303
188.9468 1.967964
189.4289 0.8397290
189.9110 3.735420
190.3931 6.892677
190.8752 10.05015
191.3573 12.68937
191.8395 14.55772
192.3216 16.49413
192.8037 19.27303
193.2858 22.60802
193.7679 25.89955
194.2500 28.90154
194.7322 31.65450
195.2143 34.28370
195.6964 36.76445
196.1785 39.15137
196.6606 41.44159
197.1427 43.66221
197.6249 45.87797
198.1070 48.11241
198.5891 50.36879
199.0712 52.69361
199.5533 55.16143
200.0354 57.63001
200.5176 60.04257
200.9997 62.40986
201.4818 64.79006
201.9639 67.32963
202.4460 70.04922
202.9281 72.07681
203.4103 72.44913
203.8924 72.97170
204.3745 74.18430
204.8566 76.01345
205.3387 78.17597
205.8208 80.49283
206.3030 83.03739
206.7851 85.03101
207.2672 86.11976
207.7493 87.05203
208.2314 88.05877
208.7135 89.16833
209.1957 90.33136
209.6778 91.50519
210.1599 92.68984
210.6420 93.90639
211.1241 95.30186
211.6062 96.59202
212.0884 97.62961
212.5705 98.41737
213.0526 99.02790
213.5347 99.48182
214.0168 99.75592
214.4989 100.2771
214.9811 101.1029
215.4632 102.1039
215.9453 103.3718
216.4274 104.7917
216.9095 105.9012
217.3916 106.2877
217.8737 105.9323
218.3559 105.6080
218.8380 105.4020
219.3201 105.1527
219.8022 104.6553
220.2843 103.9031
220.7664 103.2782
221.2486 103.3044
221.7307 103.7629
222.2128 103.7347
222.6949 102.7837
223.1770 101.4206
223.6591 100.2145
224.1413 99.21020
224.6234 98.24801
225.1055 97.27965
225.5876 96.30035
226.0697 95.28719
226.5518 94.33015
227.0340 93.30980
227.5161 92.02921
227.9982 90.45934
228.4803 88.80321
228.9624 87.06419
229.4445 85.32003
229.9267 83.70741
230.4088 82.33202
230.8909 81.05507
231.3730 79.59789
231.8551 77.87627
232.3372 76.13062
232.8194 74.65533
233.3015 73.27522
233.7836 71.72447
234.2657 69.82761
234.7478 67.73969
235.2299 65.82968
235.7121 64.11412
236.1942 62.57323
236.6763 61.30882
237.1584 60.15681
237.6405 58.95728
238.1227 57.64637
238.6048 56.25008
239.0869 54.80725
239.5690 53.19610
240.0511 51.74376
240.5332 50.63470
241.0154 49.60604
241.4975 48.37858
241.9796 46.84352
242.4617 45.18166
242.9438 43.82044
243.4259 42.85806
243.9081 42.01463
244.3902 41.46631
244.8723 40.94721
245.3544 40.15322
245.8365 39.10468
246.3186 37.98322
246.8008 37.19030
247.2829 36.70010
247.7650 36.50285
248.2471 36.88269
248.7292 37.37123
249.2113 37.41409
249.6935 36.84239
250.1756 36.07633
250.6577 35.96161
251.1398 37.18523
251.6219 38.10670
252.1040 38.55883
252.5862 38.79895
253.0683 38.98673
253.5504 39.17336
254.0325 39.43207
254.5146 39.87846
254.9967 40.50123
255.4789 41.39265
255.9610 42.75787
256.4431 44.26276
256.9252 45.55016
257.4073 46.55952
257.8894 47.61211
258.3716 49.17644
258.8537 51.56107
259.3358 53.66747
259.8179 55.05284
260.3000 56.43666
260.7821 58.46218
261.2643 61.23405
261.7464 64.39504
262.2285 67.59282
262.7106 70.84602
263.1927 74.23396
263.6748 77.79633
264.1570 81.46213
264.6391 85.04610
265.1212 88.54801
265.6033 92.31873
266.0854 96.72344
266.5675 101.7997
267.0497 106.7138
267.5318 111.4093
268.0139 115.9385
268.4960 120.1795
268.9781 124.1537
269.4602 128.3672
269.9424 133.2781
270.4245 138.8100
270.9066 144.1996
271.3887 149.3733
271.8708 154.4632
272.3529 159.4568
272.8351 164.3903
273.3172 169.4949
273.7993 174.9686
274.2814 180.7576
274.7635 186.5801
275.2456 192.0501
275.7278 197.9338
276.2099 204.9653
276.6920 213.0286
277.1741 221.1397
277.6562 228.6221
278.1383 236.0154
278.6205 244.2836
279.1026 253.9179
279.5847 263.5562
280.0668 272.2449
280.5489 280.1412
281.0310 288.0205
281.5132 296.3790
281.9953 304.5741
282.4774 311.9859
282.9595 318.7198
283.4416 324.1497
283.9237 328.0704
284.4059 330.4219
284.8880 330.9688
285.3701 329.6431
285.8522 326.2667
286.3343 320.9771
286.8164 313.8504
287.2986 305.0974
287.7807 294.5590
288.2628 282.4261
288.7449 269.3293
289.2270 255.0343
289.7091 240.2463
290.1913 225.0050
290.6734 209.5970
291.1555 194.7486
291.6376 180.8387
292.1197 167.8244
292.6018 155.4717
293.0840 143.9756
293.5661 132.8660
294.0482 121.4339
294.5303 110.1868
295.0124 100.0247
295.4945 91.53776
295.9767 84.31005
296.4588 77.70370
296.9409 71.78661
297.4230 66.25119
297.9051 60.85638
298.3872 55.72534
298.8694 51.03375
299.3515 46.81451
299.8336 43.07723
300.3157 39.89403
300.7978 37.31149
301.2799 34.89615
301.7621 32.37383
302.2442 30.00687
302.7263 28.06228
303.2084 26.61424
303.6905 25.42455
304.1726 24.18946
304.6548 22.89538
305.1369 21.95152
305.6190 21.57855
306.1011 21.52588
306.5832 21.61475
307.0653 21.83949
307.5475 22.22860
308.0296 22.85859
308.5117 23.68819
308.9938 24.39725
309.4759 24.62328
309.9580 25.16714
310.4402 26.68883
310.9223 28.98807
311.4044 31.30666
311.8865 32.99367
312.3686 34.24436
312.8507 35.97537
313.3329 38.29620
313.8150 40.95331
314.2971 43.86520
314.7792 46.98102
315.2613 50.23186
315.7434 53.61330
316.2256 57.12477
316.7077 60.73254
317.1898 64.43733
317.6719 68.25809
318.1540 72.11776
318.6361 76.14288
319.1183 80.57235
319.6004 85.60856
320.0825 90.74232
320.5646 95.12083
321.0467 98.54675
321.5288 102.4230
322.0110 107.4084
322.4931 112.9546
322.9752 118.6631
323.4573 124.4415
323.9394 130.3911
324.4215 136.7849
324.9037 143.5726
325.3858 150.0087
325.8679 155.7042
326.3500 161.2795
326.8321 166.9410
327.3142 172.7536
327.7964 179.0606
328.2785 186.5098
328.7606 194.8092
329.2427 202.5179
329.7248 209.5297
330.2069 215.9433
330.6891 221.6669
331.1712 226.8959
331.6533 232.1245
332.1354 238.0379
332.6175 243.9157
333.0996 248.2653
333.5818 251.0148
334.0639 252.3349
334.5460 251.9611
335.0281 250.3333
335.5102 247.7396
335.9923 244.1783
336.4745 239.8061
336.9566 234.9661
337.4387 229.7381
337.9208 223.0095
338.4029 213.4427
338.8850 202.8039
339.3671 192.9534
339.8492 184.0498
340.3314 175.0925
340.8135 165.1516
341.2956 154.3496
341.7777 143.9543
342.2598 134.1231
342.7419 124.8834
343.2241 116.2444
343.7062 108.1228
344.1883 100.3438
344.6704 92.63168
345.1525 85.22648
345.6346 78.79102
346.1168 73.59359
346.5989 68.63436
347.0810 62.88323
347.5631 56.92320
348.0452 51.84031
348.5273 48.28288
349.0095 45.38632
349.4916 42.13058
349.9737 38.51492
350.4558 35.21295
350.9379 32.71278
351.4200 30.64973
351.9022 28.38857
352.3843 25.82420
352.8664 23.30762
353.3485 21.07500
353.8306 19.09274
354.3127 17.22991
354.7949 15.43309
355.2770 13.76417
355.7591 12.32170
356.2412 11.10165
356.7233 9.874397
357.2054 8.530197
357.6876 7.136322
358.1697 5.704147
358.6518 4.188972
359.1339 2.972107
359.6160 2.588112
360.0981 2.865524
360.5803 2.883316
361.0624 2.449196
361.5445 1.779922
362.0266 0.8953090
362.5087 0.1472240
362.9908 0.9009400
363.4730 0.9941330
363.9551 0.6948390
364.4372 0.8699720
364.9193 1.849350
365.4014 2.709969
365.8835 2.928333
366.3657 2.771042
366.8478 2.786629
367.3299 3.166023
367.8120 3.727730
368.2941 4.221554
368.7762 4.662590
369.2584 4.982048
369.7405 5.126286
370.2226 5.167526
370.7047 5.151302
371.1868 5.091740
371.6689 5.019794
372.1511 4.956123
372.6332 4.902164
373.1153 4.910156
373.5974 5.119659
374.0795 5.252110
374.5616 5.120956
375.0438 4.801960
375.5259 4.499363
376.0080 4.325790
376.4901 4.243336
376.9722 4.118107
377.4543 3.953152
377.9365 3.743347
378.4186 3.401958
378.9007 3.054424
379.3828 2.880684
379.8649 2.918377
380.3470 2.996765
380.8292 2.870220
381.3113 2.448669
381.7934 2.081623
382.2755 1.710831
382.7576 1.435051
383.2397 1.439709
383.7219 1.619034
384.2040 1.628044
384.6861 1.165302
385.1682 0.2712290
385.6503 0.3981290
386.1324 0.6679840
386.6146 0.8922650
387.0967 1.033794
387.5788 1.194347
388.0609 1.574741
388.5430 2.256264
389.0251 2.975479
389.5073 3.120419
389.9894 2.155140
390.4715 1.753124
390.9536 2.301331
391.4357 3.120922
391.9178 3.876732
392.4000 4.486572
392.8821 4.961815
393.3642 5.302837
393.8463 5.507374
394.3284 5.635269
394.8105 5.565434
395.2927 5.558578
395.7748 5.680950
396.2569 5.926964
396.7390 6.307198
397.2211 6.858486
397.7032 7.486057
398.1854 7.953045
398.6675 8.188034
399.1496 8.472046
399.6317 9.066547
400.1138 9.642204
400.5959 9.870487
401.0781 9.702488
401.5602 9.517647
402.0423 9.690231
402.5244 10.20042
403.0065 10.73310
403.4886 11.29642
403.9708 11.78169
404.4529 11.95790
404.9350 11.98841
405.4171 12.34660
405.8992 13.38098
406.3813 14.76864
406.8635 15.92097
407.3456 16.78419
407.8277 18.01535
408.3098 19.89672
408.7919 22.42412
409.2740 25.53699
409.7562 29.36172
410.2383 33.43792
410.7204 37.94946
411.2025 42.55692
411.6846 46.27923
412.1667 48.83290
412.6489 50.56155
413.1310 51.72253
413.6131 52.35877
414.0952 52.81291
414.5773 52.63971
415.0594 52.64824
415.5416 53.61690
416.0237 55.54049
416.5058 57.91632
416.9879 60.38118
417.4700 63.04746
417.9521 66.52294
418.4343 71.33600
418.9164 76.16882
419.3985 80.30016
419.8806 84.34970
420.3627 89.11063
420.8448 94.84736
421.3270 101.4781
421.8091 108.7902
422.2912 116.2889
422.7733 126.1545
423.2554 138.3596
423.7375 152.6770
424.2197 169.5142
424.7018 188.3541
425.1839 208.1402
425.6660 228.3405
426.1481 248.5483
426.6302 266.6168
427.1124 284.8362
427.5945 297.3451
428.0766 305.6488
428.5587 306.9556
429.0408 297.2837
429.5229 275.8674
430.0051 247.5125
430.4872 217.2442
430.9693 183.3163
431.4514 155.3310
431.9335 135.2196
432.4156 119.9415
432.8978 109.1425
433.3799 102.3371
433.8620 98.61562
434.3441 97.70369
434.8262 99.29810
435.3083 102.4017
435.7905 106.5764
436.2726 113.5116
436.7547 124.0031
437.2368 137.5125
437.7189 154.0146
438.2010 173.5605
438.6832 195.3363
439.1653 220.0293
439.6474 246.8002
440.1295 272.6439
440.6116 300.0059
441.0938 320.3808
441.5759 327.8083
442.0580 323.1695
442.5401 305.1974
443.0222 264.9998
443.5043 217.2250
443.9865 173.5632
444.4686 134.4972
444.9507 102.0501
445.4328 77.78251
445.9149 60.31208
446.3970 46.83118
446.8792 37.63255
447.3613 30.49196
447.8434 25.49675
448.3255 21.89227
448.8076 18.93142
449.2897 16.43301
449.7719 14.26564
450.2540 12.29434
450.7361 10.50599
451.2182 9.138535
451.7003 8.458008
452.1824 7.834911
452.6646 7.044552
453.1467 6.148342
453.6288 5.237705
454.1109 4.351059
454.5930 3.574924
455.0751 3.069771
455.5573 2.943298
456.0394 2.879303
456.5215 3.054516
457.0036 3.141094
457.4857 2.805714
457.9678 2.166290
458.4500 1.673958
458.9321 1.734467
459.4142 2.217468
459.8963 2.293705
460.3784 1.633255
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