#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-04-26 13:44:23 +0300 (Thu, 26 Apr 2018) $ #$Revision: 546 $ #$URL: svn://172.16.1.111/rod/cif/8/10/00/8100009.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_8100009 loop_ _publ_author_name 'Sahl, K.' _publ_section_title ; Zur kristallstruktur von lanarkit, Pb2O(SO4) Locality: synthetic ; _journal_name_full 'Zeitschrift fur Kristallographie' _journal_page_first 99 _journal_page_last 117 _journal_volume 132 _journal_year 1970 _chemical_compound_source R080116 _chemical_formula_sum 'O5 Pb2 S' _chemical_name_mineral Lanarkite _space_group_IT_number 12 _symmetry_space_group_name_Hall '-C 2y' _symmetry_space_group_name_H-M 'C 1 2/m 1' _cell_angle_alpha 90 _cell_angle_beta 115.93 _cell_angle_gamma 90 _cell_length_a 13.769 _cell_length_b 5.698 _cell_length_c 7.079 _cell_volume 499.477 _exptl_crystal_density_diffrn 7.001 _cod_original_formula_sum 'Pb2 S O5' _cod_database_code 9011421 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 780 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 12 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R080116.rod _rod_data_source.block 3500000 _rod_database.code 8100009 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9011421 COD http://www.crystallography.net/cod/9011421.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 130.1285 0.0000000E+00 130.6107 1.286377 131.0928 3.482605 131.5749 8.562561 132.0570 12.51794 132.5391 17.29224 133.0212 24.74615 133.5034 33.97345 133.9855 47.51489 134.4676 63.56665 134.9497 83.89539 135.4318 109.2048 135.9139 139.4622 136.3960 174.6121 136.8782 214.7524 137.3603 260.4714 137.8424 310.0822 138.3245 363.6757 138.8066 421.0039 139.2887 481.0720 139.7709 543.0171 140.2530 609.1965 140.7351 681.5118 141.2172 758.5316 141.6993 845.0039 142.1814 940.5399 142.6636 1045.956 143.1457 1164.253 143.6278 1289.923 144.1099 1438.347 144.5920 1613.054 145.0741 1814.363 145.5563 2052.744 146.0384 2342.054 146.5205 2684.536 147.0026 3051.168 147.4847 3519.100 147.9668 3957.344 148.4490 4329.241 148.9311 4614.863 149.4132 4760.188 149.8953 4665.777 150.3774 4231.477 150.8595 3733.966 151.3417 3133.586 151.8238 2528.942 152.3059 1989.036 152.7880 1543.362 153.2701 1182.140 153.7522 888.6537 154.2344 706.0048 154.7165 555.4662 155.1986 442.4578 155.6807 357.1944 156.1628 290.1232 156.6449 237.6781 157.1271 197.8450 157.6092 164.5953 158.0913 138.4686 158.5734 116.7905 159.0555 100.0179 159.5376 86.44571 160.0198 73.91685 160.5019 62.04465 160.9840 51.30838 161.4661 42.39598 161.9482 35.85379 162.4303 30.28683 162.9125 24.95862 163.3946 19.93422 163.8767 15.37733 164.3588 11.44879 164.8409 8.131760 165.3230 5.327103 165.8052 3.128159 166.2873 1.366074 166.7694 2.9450001E-03 167.2515 0.8604280 167.7336 1.617294 168.2157 2.596344 168.6979 3.569778 169.1800 4.229797 169.6621 4.379089 170.1442 4.203888 170.6263 4.246048 171.1084 4.663330 171.5906 5.033142 172.0727 5.085632 172.5548 5.047928 173.0369 5.319580 173.5190 6.253052 174.0011 7.679970 174.4833 8.302505 174.9654 7.034966 175.4475 5.990059 175.9296 5.672333 176.4117 5.923088 176.8938 6.393860 177.3760 6.870247 177.8581 7.360634 178.3402 7.719604 178.8223 7.927719 179.3044 8.037552 179.7865 7.995102 180.2687 7.849663 180.7508 7.710381 181.2329 7.647827 181.7150 7.662323 182.1971 7.829903 182.6792 8.390976 183.1614 8.883034 183.6435 8.934914 184.1256 8.574455 184.6077 8.240036 185.0898 8.364426 185.5719 8.978584 186.0541 9.399147 186.5362 9.459488 187.0183 9.404877 187.5004 9.460411 187.9825 7.115494 188.4646 4.643303 188.9468 1.967964 189.4289 0.8397290 189.9110 3.735420 190.3931 6.892677 190.8752 10.05015 191.3573 12.68937 191.8395 14.55772 192.3216 16.49413 192.8037 19.27303 193.2858 22.60802 193.7679 25.89955 194.2500 28.90154 194.7322 31.65450 195.2143 34.28370 195.6964 36.76445 196.1785 39.15137 196.6606 41.44159 197.1427 43.66221 197.6249 45.87797 198.1070 48.11241 198.5891 50.36879 199.0712 52.69361 199.5533 55.16143 200.0354 57.63001 200.5176 60.04257 200.9997 62.40986 201.4818 64.79006 201.9639 67.32963 202.4460 70.04922 202.9281 72.07681 203.4103 72.44913 203.8924 72.97170 204.3745 74.18430 204.8566 76.01345 205.3387 78.17597 205.8208 80.49283 206.3030 83.03739 206.7851 85.03101 207.2672 86.11976 207.7493 87.05203 208.2314 88.05877 208.7135 89.16833 209.1957 90.33136 209.6778 91.50519 210.1599 92.68984 210.6420 93.90639 211.1241 95.30186 211.6062 96.59202 212.0884 97.62961 212.5705 98.41737 213.0526 99.02790 213.5347 99.48182 214.0168 99.75592 214.4989 100.2771 214.9811 101.1029 215.4632 102.1039 215.9453 103.3718 216.4274 104.7917 216.9095 105.9012 217.3916 106.2877 217.8737 105.9323 218.3559 105.6080 218.8380 105.4020 219.3201 105.1527 219.8022 104.6553 220.2843 103.9031 220.7664 103.2782 221.2486 103.3044 221.7307 103.7629 222.2128 103.7347 222.6949 102.7837 223.1770 101.4206 223.6591 100.2145 224.1413 99.21020 224.6234 98.24801 225.1055 97.27965 225.5876 96.30035 226.0697 95.28719 226.5518 94.33015 227.0340 93.30980 227.5161 92.02921 227.9982 90.45934 228.4803 88.80321 228.9624 87.06419 229.4445 85.32003 229.9267 83.70741 230.4088 82.33202 230.8909 81.05507 231.3730 79.59789 231.8551 77.87627 232.3372 76.13062 232.8194 74.65533 233.3015 73.27522 233.7836 71.72447 234.2657 69.82761 234.7478 67.73969 235.2299 65.82968 235.7121 64.11412 236.1942 62.57323 236.6763 61.30882 237.1584 60.15681 237.6405 58.95728 238.1227 57.64637 238.6048 56.25008 239.0869 54.80725 239.5690 53.19610 240.0511 51.74376 240.5332 50.63470 241.0154 49.60604 241.4975 48.37858 241.9796 46.84352 242.4617 45.18166 242.9438 43.82044 243.4259 42.85806 243.9081 42.01463 244.3902 41.46631 244.8723 40.94721 245.3544 40.15322 245.8365 39.10468 246.3186 37.98322 246.8008 37.19030 247.2829 36.70010 247.7650 36.50285 248.2471 36.88269 248.7292 37.37123 249.2113 37.41409 249.6935 36.84239 250.1756 36.07633 250.6577 35.96161 251.1398 37.18523 251.6219 38.10670 252.1040 38.55883 252.5862 38.79895 253.0683 38.98673 253.5504 39.17336 254.0325 39.43207 254.5146 39.87846 254.9967 40.50123 255.4789 41.39265 255.9610 42.75787 256.4431 44.26276 256.9252 45.55016 257.4073 46.55952 257.8894 47.61211 258.3716 49.17644 258.8537 51.56107 259.3358 53.66747 259.8179 55.05284 260.3000 56.43666 260.7821 58.46218 261.2643 61.23405 261.7464 64.39504 262.2285 67.59282 262.7106 70.84602 263.1927 74.23396 263.6748 77.79633 264.1570 81.46213 264.6391 85.04610 265.1212 88.54801 265.6033 92.31873 266.0854 96.72344 266.5675 101.7997 267.0497 106.7138 267.5318 111.4093 268.0139 115.9385 268.4960 120.1795 268.9781 124.1537 269.4602 128.3672 269.9424 133.2781 270.4245 138.8100 270.9066 144.1996 271.3887 149.3733 271.8708 154.4632 272.3529 159.4568 272.8351 164.3903 273.3172 169.4949 273.7993 174.9686 274.2814 180.7576 274.7635 186.5801 275.2456 192.0501 275.7278 197.9338 276.2099 204.9653 276.6920 213.0286 277.1741 221.1397 277.6562 228.6221 278.1383 236.0154 278.6205 244.2836 279.1026 253.9179 279.5847 263.5562 280.0668 272.2449 280.5489 280.1412 281.0310 288.0205 281.5132 296.3790 281.9953 304.5741 282.4774 311.9859 282.9595 318.7198 283.4416 324.1497 283.9237 328.0704 284.4059 330.4219 284.8880 330.9688 285.3701 329.6431 285.8522 326.2667 286.3343 320.9771 286.8164 313.8504 287.2986 305.0974 287.7807 294.5590 288.2628 282.4261 288.7449 269.3293 289.2270 255.0343 289.7091 240.2463 290.1913 225.0050 290.6734 209.5970 291.1555 194.7486 291.6376 180.8387 292.1197 167.8244 292.6018 155.4717 293.0840 143.9756 293.5661 132.8660 294.0482 121.4339 294.5303 110.1868 295.0124 100.0247 295.4945 91.53776 295.9767 84.31005 296.4588 77.70370 296.9409 71.78661 297.4230 66.25119 297.9051 60.85638 298.3872 55.72534 298.8694 51.03375 299.3515 46.81451 299.8336 43.07723 300.3157 39.89403 300.7978 37.31149 301.2799 34.89615 301.7621 32.37383 302.2442 30.00687 302.7263 28.06228 303.2084 26.61424 303.6905 25.42455 304.1726 24.18946 304.6548 22.89538 305.1369 21.95152 305.6190 21.57855 306.1011 21.52588 306.5832 21.61475 307.0653 21.83949 307.5475 22.22860 308.0296 22.85859 308.5117 23.68819 308.9938 24.39725 309.4759 24.62328 309.9580 25.16714 310.4402 26.68883 310.9223 28.98807 311.4044 31.30666 311.8865 32.99367 312.3686 34.24436 312.8507 35.97537 313.3329 38.29620 313.8150 40.95331 314.2971 43.86520 314.7792 46.98102 315.2613 50.23186 315.7434 53.61330 316.2256 57.12477 316.7077 60.73254 317.1898 64.43733 317.6719 68.25809 318.1540 72.11776 318.6361 76.14288 319.1183 80.57235 319.6004 85.60856 320.0825 90.74232 320.5646 95.12083 321.0467 98.54675 321.5288 102.4230 322.0110 107.4084 322.4931 112.9546 322.9752 118.6631 323.4573 124.4415 323.9394 130.3911 324.4215 136.7849 324.9037 143.5726 325.3858 150.0087 325.8679 155.7042 326.3500 161.2795 326.8321 166.9410 327.3142 172.7536 327.7964 179.0606 328.2785 186.5098 328.7606 194.8092 329.2427 202.5179 329.7248 209.5297 330.2069 215.9433 330.6891 221.6669 331.1712 226.8959 331.6533 232.1245 332.1354 238.0379 332.6175 243.9157 333.0996 248.2653 333.5818 251.0148 334.0639 252.3349 334.5460 251.9611 335.0281 250.3333 335.5102 247.7396 335.9923 244.1783 336.4745 239.8061 336.9566 234.9661 337.4387 229.7381 337.9208 223.0095 338.4029 213.4427 338.8850 202.8039 339.3671 192.9534 339.8492 184.0498 340.3314 175.0925 340.8135 165.1516 341.2956 154.3496 341.7777 143.9543 342.2598 134.1231 342.7419 124.8834 343.2241 116.2444 343.7062 108.1228 344.1883 100.3438 344.6704 92.63168 345.1525 85.22648 345.6346 78.79102 346.1168 73.59359 346.5989 68.63436 347.0810 62.88323 347.5631 56.92320 348.0452 51.84031 348.5273 48.28288 349.0095 45.38632 349.4916 42.13058 349.9737 38.51492 350.4558 35.21295 350.9379 32.71278 351.4200 30.64973 351.9022 28.38857 352.3843 25.82420 352.8664 23.30762 353.3485 21.07500 353.8306 19.09274 354.3127 17.22991 354.7949 15.43309 355.2770 13.76417 355.7591 12.32170 356.2412 11.10165 356.7233 9.874397 357.2054 8.530197 357.6876 7.136322 358.1697 5.704147 358.6518 4.188972 359.1339 2.972107 359.6160 2.588112 360.0981 2.865524 360.5803 2.883316 361.0624 2.449196 361.5445 1.779922 362.0266 0.8953090 362.5087 0.1472240 362.9908 0.9009400 363.4730 0.9941330 363.9551 0.6948390 364.4372 0.8699720 364.9193 1.849350 365.4014 2.709969 365.8835 2.928333 366.3657 2.771042 366.8478 2.786629 367.3299 3.166023 367.8120 3.727730 368.2941 4.221554 368.7762 4.662590 369.2584 4.982048 369.7405 5.126286 370.2226 5.167526 370.7047 5.151302 371.1868 5.091740 371.6689 5.019794 372.1511 4.956123 372.6332 4.902164 373.1153 4.910156 373.5974 5.119659 374.0795 5.252110 374.5616 5.120956 375.0438 4.801960 375.5259 4.499363 376.0080 4.325790 376.4901 4.243336 376.9722 4.118107 377.4543 3.953152 377.9365 3.743347 378.4186 3.401958 378.9007 3.054424 379.3828 2.880684 379.8649 2.918377 380.3470 2.996765 380.8292 2.870220 381.3113 2.448669 381.7934 2.081623 382.2755 1.710831 382.7576 1.435051 383.2397 1.439709 383.7219 1.619034 384.2040 1.628044 384.6861 1.165302 385.1682 0.2712290 385.6503 0.3981290 386.1324 0.6679840 386.6146 0.8922650 387.0967 1.033794 387.5788 1.194347 388.0609 1.574741 388.5430 2.256264 389.0251 2.975479 389.5073 3.120419 389.9894 2.155140 390.4715 1.753124 390.9536 2.301331 391.4357 3.120922 391.9178 3.876732 392.4000 4.486572 392.8821 4.961815 393.3642 5.302837 393.8463 5.507374 394.3284 5.635269 394.8105 5.565434 395.2927 5.558578 395.7748 5.680950 396.2569 5.926964 396.7390 6.307198 397.2211 6.858486 397.7032 7.486057 398.1854 7.953045 398.6675 8.188034 399.1496 8.472046 399.6317 9.066547 400.1138 9.642204 400.5959 9.870487 401.0781 9.702488 401.5602 9.517647 402.0423 9.690231 402.5244 10.20042 403.0065 10.73310 403.4886 11.29642 403.9708 11.78169 404.4529 11.95790 404.9350 11.98841 405.4171 12.34660 405.8992 13.38098 406.3813 14.76864 406.8635 15.92097 407.3456 16.78419 407.8277 18.01535 408.3098 19.89672 408.7919 22.42412 409.2740 25.53699 409.7562 29.36172 410.2383 33.43792 410.7204 37.94946 411.2025 42.55692 411.6846 46.27923 412.1667 48.83290 412.6489 50.56155 413.1310 51.72253 413.6131 52.35877 414.0952 52.81291 414.5773 52.63971 415.0594 52.64824 415.5416 53.61690 416.0237 55.54049 416.5058 57.91632 416.9879 60.38118 417.4700 63.04746 417.9521 66.52294 418.4343 71.33600 418.9164 76.16882 419.3985 80.30016 419.8806 84.34970 420.3627 89.11063 420.8448 94.84736 421.3270 101.4781 421.8091 108.7902 422.2912 116.2889 422.7733 126.1545 423.2554 138.3596 423.7375 152.6770 424.2197 169.5142 424.7018 188.3541 425.1839 208.1402 425.6660 228.3405 426.1481 248.5483 426.6302 266.6168 427.1124 284.8362 427.5945 297.3451 428.0766 305.6488 428.5587 306.9556 429.0408 297.2837 429.5229 275.8674 430.0051 247.5125 430.4872 217.2442 430.9693 183.3163 431.4514 155.3310 431.9335 135.2196 432.4156 119.9415 432.8978 109.1425 433.3799 102.3371 433.8620 98.61562 434.3441 97.70369 434.8262 99.29810 435.3083 102.4017 435.7905 106.5764 436.2726 113.5116 436.7547 124.0031 437.2368 137.5125 437.7189 154.0146 438.2010 173.5605 438.6832 195.3363 439.1653 220.0293 439.6474 246.8002 440.1295 272.6439 440.6116 300.0059 441.0938 320.3808 441.5759 327.8083 442.0580 323.1695 442.5401 305.1974 443.0222 264.9998 443.5043 217.2250 443.9865 173.5632 444.4686 134.4972 444.9507 102.0501 445.4328 77.78251 445.9149 60.31208 446.3970 46.83118 446.8792 37.63255 447.3613 30.49196 447.8434 25.49675 448.3255 21.89227 448.8076 18.93142 449.2897 16.43301 449.7719 14.26564 450.2540 12.29434 450.7361 10.50599 451.2182 9.138535 451.7003 8.458008 452.1824 7.834911 452.6646 7.044552 453.1467 6.148342 453.6288 5.237705 454.1109 4.351059 454.5930 3.574924 455.0751 3.069771 455.5573 2.943298 456.0394 2.879303 456.5215 3.054516 457.0036 3.141094 457.4857 2.805714 457.9678 2.166290 458.4500 1.673958 458.9321 1.734467 459.4142 2.217468 459.8963 2.293705 460.3784 1.633255 460.8605 1.146873 461.3427 1.183926 461.8248 1.422741 462.3069 1.529285 462.7890 1.426601 463.2711 1.365608 463.7532 1.651653 464.2354 2.237038 464.7175 2.552185 465.1996 2.404446 465.6817 2.195763 466.1638 2.164139 466.6459 2.289326 467.1281 2.549160 467.6102 3.100628 468.0923 3.631138 468.5744 3.658676 469.0565 3.252556 469.5386 3.133587 470.0208 3.672810 470.5029 4.528194 470.9850 5.106361 471.4671 5.395016 471.9492 5.608887 472.4313 5.679108 472.9135 5.766636 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