#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:22:40 +0300 (Thu, 24 May 2018) $
#$Revision: 690 $
#$URL: svn://172.16.1.111/rod/cif/8/10/00/8100017.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_8100017
loop_
_publ_author_name
'Boucher, M. L.'
'Peacor, D. R.'
_publ_section_title
;
 The crystal structure of alamosite, PbSiO3 Locality: Alamos, Sonora,
 Mexico
;
_journal_name_full               'Zeitschrift fur Kristallographie'
_journal_page_first              98
_journal_page_last               111
_journal_volume                  126
_journal_year                    1968
_chemical_compound_source        R060067
_chemical_formula_sum            'O3 Pb Si'
_chemical_name_mineral           Alamosite
_space_group_IT_number           13
_symmetry_space_group_name_Hall  '-P 2yac'
_symmetry_space_group_name_H-M   'P 1 2/n 1'
_cell_angle_alpha                90
_cell_angle_beta                 113.25
_cell_angle_gamma                90
_cell_length_a                   11.23
_cell_length_b                   7.08
_cell_length_c                   12.26
_cell_volume                     895.613
_exptl_crystal_density_diffrn    6.303
_cod_original_formula_sum        'Pb Si O3'
_cod_database_code               9008141
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060067.rod
_rod_data_source.block           3500000
_rod_database.code               8100017
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9008141 COD http://www.crystallography.net/cod/9008141.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
125.5345 0.0000000E+00
126.0167 3.932983
126.4988 0.7539060
126.9809 0.6274410
127.4630 2.907410
127.9451 9.276062
128.4272 17.54303
128.9093 26.54419
129.3915 36.26886
129.8736 47.05878
130.3557 58.04382
130.8378 65.84546
131.3199 71.48071
131.8020 79.30859
132.2842 88.90051
132.7663 99.00092
133.2484 109.6788
133.7305 122.4035
134.2126 138.7369
134.6947 158.4772
135.1769 179.0335
135.6590 199.9613
136.1411 221.5283
136.6232 244.4479
137.1053 268.4263
137.5874 294.2749
138.0696 323.6695
138.5517 356.7067
139.0338 389.5308
139.5159 421.6180
139.9980 452.6978
140.4801 483.6492
140.9623 516.8064
141.4444 545.9174
141.9265 565.8671
142.4086 577.5251
142.8907 577.9333
143.3728 565.9692
143.8550 541.4761
144.3371 507.7463
144.8192 462.5110
145.3013 409.9781
145.7834 357.5886
146.2655 302.5988
146.7477 250.6809
147.2298 202.4585
147.7119 157.2148
148.1940 118.6784
148.6761 88.05847
149.1582 63.78937
149.6404 43.77972
150.1225 27.70422
150.6046 15.83289
151.0867 8.471863
151.5688 6.879517
152.0509 7.682251
152.5331 10.68982
153.0152 16.01141
153.4973 24.05640
153.9794 35.03174
154.4615 48.44598
154.9436 64.12915
155.4258 83.73706
155.9079 103.4213
156.3900 123.8745
156.8721 144.5063
157.3542 162.9628
157.8363 178.9345
158.3185 192.4090
158.8006 203.3381
159.2827 211.3929
159.7648 217.3237
160.2469 220.1664
160.7290 220.3461
161.2112 221.5563
161.6933 224.4385
162.1754 229.0890
162.6575 235.5861
163.1396 242.7064
163.6217 252.7511
164.1039 266.6575
164.5860 284.4138
165.0681 305.3551
165.5502 331.9346
166.0323 360.6116
166.5145 387.6790
166.9966 414.6217
167.4787 437.4414
167.9608 454.9526
168.4429 467.2767
168.9250 471.0286
169.4072 462.7714
169.8893 444.7770
170.3714 420.7233
170.8535 388.2762
171.3356 352.6125
171.8177 317.0836
172.2999 281.6500
172.7820 248.4634
173.2641 217.9945
173.7462 190.9589
174.2283 168.6514
174.7104 151.6045
175.1926 139.3232
175.6747 131.6833
176.1568 128.7574
176.6389 129.5468
177.1210 133.9609
177.6031 141.5316
178.0853 150.8380
178.5674 161.6484
179.0495 173.5435
179.5316 186.4467
180.0137 200.9214
180.4958 215.4810
180.9780 229.6552
181.4601 242.7486
181.9422 252.4368
182.4243 257.8937
182.9064 258.6392
183.3885 251.1724
183.8707 237.0651
184.3528 218.3624
184.8349 196.4150
185.3170 171.6251
185.7991 146.1505
186.2812 120.2884
186.7633 94.90082
187.2455 73.20587
187.7276 55.56354
188.2097 41.57349
188.6918 30.14636
189.1739 21.31873
189.6560 15.09912
190.1382 11.61121
190.6203 10.87244
191.1024 12.48907
191.5845 16.70667
192.0666 22.99432
192.5487 30.08215
193.0309 37.92499
193.5130 47.06268
193.9951 58.62439
194.4772 72.49152
194.9593 85.98926
195.4414 98.68439
195.9236 110.7389
196.4057 122.2422
196.8878 133.1682
197.3699 143.8395
197.8520 154.4133
198.3341 164.9805
198.8163 175.6244
199.2984 186.3721
199.7805 197.2474
200.2626 208.2153
200.7447 219.0677
201.2268 230.6391
201.7090 243.7999
202.1911 258.6858
202.6732 273.8472
203.1553 288.5386
203.6374 303.1124
204.1195 319.6083
204.6017 338.2144
205.0838 358.2524
205.5659 378.9209
206.0480 400.0383
206.5301 422.9479
207.0122 447.9365
207.4944 474.9687
207.9765 502.6616
208.4586 530.8671
208.9407 560.0244
209.4228 590.9083
209.9049 624.0181
210.3871 657.0938
210.8692 689.9630
211.3513 722.4082
211.8334 752.3513
212.3155 780.4644
212.7976 805.0076
213.2798 824.5681
213.7619 839.8438
214.2440 848.0845
214.7261 848.5690
215.2082 841.3318
215.6903 827.5459
216.1725 806.7920
216.6546 780.3922
217.1367 749.4058
217.6188 712.7009
218.1009 673.9224
218.5830 632.9543
219.0652 589.2087
219.5473 547.5535
220.0294 507.6315
220.5115 469.1690
220.9936 432.3237
221.4757 396.5450
221.9579 362.8453
222.4400 331.1179
222.9221 301.0694
223.4042 273.9526
223.8863 249.8656
224.3684 228.0286
224.8506 207.0477
225.3327 186.7339
225.8148 168.1514
226.2969 152.0793
226.7790 138.5116
227.2611 125.0689
227.7433 111.0526
228.2254 97.52271
228.7075 85.70068
229.1896 75.84555
229.6717 66.96884
230.1538 58.83667
230.6360 51.53174
231.1181 44.54654
231.6002 37.89713
232.0823 31.53928
232.5644 25.39423
233.0465 19.08237
233.5287 13.53729
234.0108 9.101746
234.4929 5.807770
234.9750 2.499084
235.4571 0.9566350
235.9392 4.229614
236.4214 6.970459
236.9035 8.922241
237.3856 10.76416
237.8677 12.69220
238.3498 14.78061
238.8319 16.40674
239.3141 17.48434
239.7962 18.16455
240.2783 18.64474
240.7604 18.98969
241.2425 18.99799
241.7246 18.58838
242.2068 17.75311
242.6889 16.78821
243.1710 15.66379
243.6531 14.44186
244.1352 13.23801
244.6173 12.32047
245.0995 10.92139
245.5816 8.909698
246.0637 6.285400
246.5458 3.097717
247.0279 0.8148800
247.5100 5.139648
247.9922 9.543427
248.4743 14.04984
248.9564 18.69543
249.4385 23.45703
249.9206 28.34097
250.4027 33.69965
250.8848 39.65607
251.3670 45.97543
251.8491 52.44333
252.3312 59.28607
252.8133 65.88589
253.2954 72.11334
253.7775 77.99500
254.2597 83.93445
254.7418 89.72800
255.2239 95.86084
255.7060 102.7404
256.1881 110.6316
256.6703 118.7386
257.1524 126.9525
257.6345 135.3041
258.1166 144.0948
258.5987 153.1990
259.0808 162.7859
259.5630 173.0371
260.0451 183.8082
260.5272 195.1276
261.0093 206.7669
261.4914 218.8801
261.9735 232.1519
262.4557 246.5622
262.9378 261.9819
263.4199 278.4545
263.9020 296.5479
264.3841 313.8145
264.8662 330.1649
265.3484 345.5506
265.8305 360.7469
266.3126 376.5020
266.7947 390.2370
267.2768 400.3672
267.7589 406.9617
268.2411 410.3132
268.7232 410.6245
269.2053 407.6288
269.6874 400.4250
270.1695 388.3849
270.6516 373.4462
271.1338 356.2144
271.6159 335.9848
272.0980 315.7722
272.5801 295.4581
273.0622 275.2433
273.5443 256.0974
274.0265 238.1571
274.5086 220.9309
274.9907 204.2627
275.4728 188.0894
275.9549 173.1189
276.4370 159.6684
276.9192 147.0235
277.4013 133.6719
277.8834 119.3626
278.3655 105.7945
278.8476 93.77646
279.3297 83.23535
279.8118 73.44171
280.2939 64.42212
280.7761 56.33359
281.2582 49.61279
281.7403 44.32700
282.2224 39.67307
282.7045 35.39499
283.1866 31.49228
283.6688 27.92566
284.1509 24.61954
284.6330 21.84036
285.1151 20.01480
285.5972 19.13544
286.0793 18.41501
286.5615 17.50204
287.0436 16.51691
287.5257 16.06308
288.0078 16.14960
288.4899 16.53644
288.9720 17.04123
289.4542 17.65677
289.9363 18.24930
290.4184 18.57413
290.9005 18.89514
291.3826 20.08188
291.8647 22.16666
292.3469 24.52206
292.8290 26.71484
293.3111 28.64578
293.7932 30.23407
294.2753 31.34845
294.7574 32.34741
295.2396 33.94650
295.7217 36.11462
296.2038 38.16577
296.6859 39.22644
297.1680 39.76743
297.6501 41.22430
298.1323 44.26776
298.6144 47.65280
299.0965 49.68823
299.5786 50.55463
300.0607 51.02081
300.5428 51.92139
301.0250 52.75946
301.5071 52.57181
301.9892 51.07846
302.4713 48.94553
302.9534 46.83374
303.4355 44.76508
303.9177 42.71255
304.3998 40.67261
304.8819 38.71335
305.3640 36.76379
305.8461 34.68494
306.3282 32.86633
306.8104 31.55118
307.2925 30.72427
307.7746 30.40448
308.2567 30.55310
308.7388 31.23785
309.2209 32.61783
309.7031 34.71704
310.1852 37.14182
310.6673 39.84927
311.1494 42.68549
311.6315 45.43323
312.1136 47.75110
312.5958 50.13763
313.0779 53.00659
313.5600 56.31473
314.0421 59.72379
314.5242 62.91046
315.0063 66.11584
315.4885 69.56915
315.9706 73.64935
316.4527 77.70703
316.9348 81.71634
317.4169 85.56631
317.8990 88.76877
318.3812 91.49286
318.8633 93.29605
319.3454 93.95230
319.8275 94.22177
320.3096 92.11035
320.7917 86.61105
321.2739 78.27747
321.7560 68.48141
322.2381 56.07327
322.7202 43.47913
323.2023 31.62277
323.6844 20.15918
324.1666 10.50241
324.6487 3.164368
325.1308 2.217957
325.6129 6.138123
326.0950 8.268860
326.5771 9.326721
327.0593 9.526062
327.5414 8.920990
328.0235 7.291077
328.5056 4.641937
328.9877 0.9501950
329.4698 3.743011
329.9520 9.705750
330.4341 16.38660
330.9162 23.82816
331.3983 32.04919
331.8804 40.46988
332.3625 48.81479
332.8447 57.50162
333.3268 66.94357
333.8089 77.56729
334.2910 88.24313
334.7731 98.95328
335.2552 109.7360
335.7374 120.3603
336.2195 130.5719
336.7016 141.1779
337.1837 152.7981
337.6658 165.4708
338.1479 178.7400
338.6301 192.6236
339.1122 206.8687
339.5943 220.6488
340.0764 233.5158
340.5585 247.0562
341.0406 261.7253
341.5228 277.7639
342.0049 294.1386
342.4870 310.9733
342.9691 328.1444
343.4512 344.8764
343.9333 361.2072
344.4155 378.9804
344.8976 399.1407
345.3797 421.3298
345.8618 442.5338
346.3439 462.9562
346.8260 482.3172
347.3082 500.9325
347.7903 518.6037
348.2724 534.6961
348.7545 549.5892
349.2366 562.3169
349.7188 571.1809
350.2009 576.2617
350.6830 577.4130
351.1651 574.8318
351.6472 568.2634
352.1293 556.9692
352.6115 540.7184
353.0936 520.4401
353.5757 495.9894
354.0578 468.0163
354.5399 438.4701
355.0220 407.3429
355.5042 375.6338
355.9863 344.6070
356.4684 314.5412
356.9505 285.9813
357.4326 259.0445
357.9147 234.0168
358.3969 211.4771
358.8790 191.7177
359.3611 174.2704
359.8432 158.8196
360.3253 145.3097
360.8074 133.8336
361.2896 124.4028
361.7717 116.8348
362.2538 110.9887
362.7359 107.1914
363.2180 104.7259
363.7001 103.6089
364.1823 103.6319
364.6644 104.1672
365.1465 105.0573
365.6286 106.3819
366.1107 108.3372
366.5928 111.8341
367.0750 114.1771
367.5571 114.4209
368.0392 113.4502
368.5213 112.5961
369.0034 112.6905
369.4855 112.2319
369.9677 110.5145
370.4498 107.1433
370.9319 104.6091
371.4140 103.6153
371.8961 102.9752
372.3782 101.4591
372.8604 98.07361
373.3425 95.50940
373.8246 94.19699
374.3067 94.07724
374.7888 94.59253
375.2709 95.78287
375.7531 97.56189
376.2352 99.90979
376.7173 102.8391
377.1994 106.3147
377.6815 110.4276
378.1636 115.0663
378.6458 119.9193
379.1279 125.0405
379.6100 130.3482
380.0921 135.9926
380.5742 141.9316
381.0563 147.7258
381.5385 153.4666
382.0206 158.6660
382.5027 162.7365
382.9848 165.6761
383.4669 167.3904
383.9490 167.9178
384.4312 167.2498
384.9133 165.4283
385.3954 162.4813
385.8775 158.1924
386.3596 152.1328
386.8417 144.6755
387.3239 136.3334
387.8060 127.0367
388.2881 117.3736
388.7702 107.5504
389.2523 97.80624
389.7344 88.91141
390.2166 81.32510
390.6987 74.66730
391.1808 68.64355
391.6629 63.19913
392.1450 58.09918
392.6271 52.99063
393.1093 48.22507
393.5914 44.31720
394.0735 41.87692
394.5556 39.90097
395.0377 38.02441
395.5198 36.23505
396.0020 34.49799
396.4841 32.90280
396.9662 31.29926
397.4483 29.56018
397.9304 27.09207
398.4125 25.27512
398.8947 24.25458
399.3768 24.01642
399.8589 24.53003
400.3410 26.03177
400.8231 28.06625
401.3052 30.75577
401.7874 34.56396
402.2695 37.14545
402.7516 37.69934
403.2337 37.61633
403.7158 38.56158
404.1979 41.35620
404.6800 43.42606
405.1621 44.23965
405.6443 43.91763
406.1264 43.28973
406.6085 42.29428
407.0906 41.15955
407.5727 40.15363
408.0548 39.33432
408.5370 37.81982
409.0191 35.37762
409.5012 32.56250
409.9833 30.55020
410.4654 29.32822
410.9475 27.86041
411.4297 25.57465
411.9118 22.65738
412.3939 19.72235
412.8760 16.82401
413.3581 13.95914
413.8402 11.13782
414.3224 8.384705
414.8045 5.650604
415.2866 2.781403
415.7687 0.1080020
416.2508 1.941284
416.7329 3.453705
417.2151 4.867218
417.6972 6.614075
418.1793 8.310944
418.6614 9.589966
419.1435 10.31897
419.6256 10.87198
420.1078 11.62631
420.5899 12.29065
421.0720 12.48074
421.5541 11.89053
422.0362 10.94650
422.5183 9.859558
423.0005 8.634399
423.4826 6.961700
423.9647 5.047577
424.4468 2.481628
424.9289 0.9714050
425.4110 5.712433
425.8932 10.88797
426.3753 16.35910
426.8574 22.19971
427.3395 28.75769
427.8216 36.58582
428.3037 44.31616
428.7859 51.44366
429.2680 57.85309
429.7501 64.51422
430.2322 71.75818
430.7143 78.75925
431.1964 84.37021
431.6786 88.31039
432.1607 92.37708
432.6428 97.09106
433.1249 102.0759
433.6070 105.8913
434.0891 108.4319
434.5713 111.0689
435.0534 114.8079
435.5355 119.4302
436.0176 123.7891
436.4997 127.6267
436.9818 131.9454
437.4640 137.9326
437.9461 145.4441
438.4282 154.0274
438.9103 163.7696
439.3924 174.3131
439.8745 185.2676
440.3567 196.5646
440.8388 208.4004
441.3209 221.5813
441.8030 235.0195
442.2851 247.8046
442.7672 260.2660
443.2494 270.8680
443.7315 279.4422
444.2136 285.4848
444.6957 287.9054
445.1778 286.4378
445.6599 281.2793
446.1421 272.1351
446.6242 258.8061
447.1063 243.2927
447.5884 224.0318
448.0705 203.6314
448.5526 184.1917
449.0348 165.1441
449.5169 147.6724
449.9990 131.6176
450.4811 117.0509
450.9632 104.5019
451.4453 94.15140
451.9275 85.30435
452.4096 77.76779
452.8917 71.72571
453.3738 66.30301
453.8559 61.44019
454.3380 57.54190
454.8202 55.26242
455.3023 54.63083
455.7844 54.44592
456.2665 54.31247
456.7486 54.65601
457.2307 56.43912
457.7129 59.58704
458.1950 63.47510
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