#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:47:25 +0300 (Thu, 24 May 2018) $
#$Revision: 772 $
#$URL: svn://172.16.1.111/rod/cif/8/10/00/8100021.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_8100021
loop_
_publ_author_name
'Sahl, K.'
_publ_section_title
;
 Zur kristallstruktur von lanarkit, Pb2O(SO4) Locality: synthetic
;
_journal_name_full               'Zeitschrift fur Kristallographie'
_journal_page_first              99
_journal_page_last               117
_journal_volume                  132
_journal_year                    1970
_chemical_compound_source        R080116
_chemical_formula_sum            'O5 Pb2 S'
_chemical_name_mineral           Lanarkite
_space_group_IT_number           12
_symmetry_space_group_name_Hall  '-C 2y'
_symmetry_space_group_name_H-M   'C 1 2/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 115.93
_cell_angle_gamma                90
_cell_length_a                   13.769
_cell_length_b                   5.698
_cell_length_c                   7.079
_cell_volume                     499.477
_exptl_crystal_density_diffrn    7.001
_cod_original_formula_sum        'Pb2 S O5'
_cod_database_code               9011421
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R080116.rod
_rod_data_source.block           3500000
_rod_database.code               8100021
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9011421 COD http://www.crystallography.net/cod/9011421.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
130.4407 0.0000000E+00
130.9229 6.236328
131.4050 428.1543
131.8871 872.7695
132.3692 1287.809
132.8513 1762.992
133.3334 2224.658
133.8156 2636.900
134.2977 3037.195
134.7798 3496.230
135.2619 4039.963
135.7440 4672.762
136.2261 5376.742
136.7083 6130.105
137.1904 6927.020
137.6725 7784.738
138.1546 8722.031
138.6367 9742.801
139.1188 10853.64
139.6010 12056.26
140.0831 13340.95
140.5652 14711.01
141.0473 16156.66
141.5294 17698.63
142.0115 19327.25
142.4937 20995.63
142.9758 22867.48
143.4579 24984.41
143.9400 27322.15
144.4221 30082.92
144.9042 33230.68
145.3864 36807.30
145.8685 40869.38
146.3506 45756.95
146.8327 50738.87
147.3148 55864.75
147.7969 62216.82
148.2791 66237.28
148.7612 68152.59
149.2433 67787.25
149.7254 64597.39
150.2075 56464.84
150.6896 47407.04
151.1718 38868.52
151.6539 30183.38
152.1360 22924.96
152.6181 17357.41
153.1002 13249.84
153.5823 9960.708
154.0645 7706.224
154.5466 6007.438
155.0287 4650.338
155.5108 3729.021
155.9929 2967.327
156.4750 2366.956
156.9572 1907.133
157.4393 1524.446
157.9214 1220.115
158.4035 971.5220
158.8856 766.0684
159.3677 608.7529
159.8499 454.7158
160.3320 322.1233
160.8141 211.6477
161.2962 115.7390
161.7783 37.47925
162.2604 28.00635
162.7426 83.45459
163.2247 126.9702
163.7068 163.8003
164.1889 196.9939
164.6710 225.6895
165.1531 247.9490
165.6353 259.5591
166.1174 265.0144
166.5995 269.3926
167.0816 277.6812
167.5637 283.1516
168.0458 281.1357
168.5280 271.3491
169.0101 258.5923
169.4922 242.4246
169.9743 225.6626
170.4564 211.8147
170.9385 205.2441
171.4207 200.5103
171.9028 192.2090
172.3849 179.7817
172.8670 167.7332
173.3491 160.5955
173.8312 156.4663
174.3134 151.8950
174.7955 143.1326
175.2776 133.7046
175.7597 128.4880
176.2418 128.4138
176.7239 128.4778
177.2061 123.4269
177.6882 115.2472
178.1703 108.9790
178.6524 108.3422
179.1345 110.9912
179.6166 112.8860
180.0988 113.9528
180.5809 114.3336
181.0630 113.9587
181.5451 113.0784
182.0272 112.0837
182.5093 111.2659
182.9915 110.6154
183.4736 110.0834
183.9557 109.9124
184.4378 109.2816
184.9199 106.2380
185.4020 101.1544
185.8842 97.75781
186.3663 99.16235
186.8484 104.0731
187.3305 107.1558
187.8126 107.5791
188.2947 45.12329
188.7769 21.04834
189.2590 88.01001
189.7411 157.5186
190.2232 230.7065
190.7053 306.6971
191.1874 382.8512
191.6696 458.4609
192.1517 533.9930
192.6338 611.3896
193.1159 690.6420
193.5980 767.6483
194.0801 838.8029
194.5623 904.5147
195.0444 971.1870
195.5265 1039.626
196.0086 1108.815
196.4907 1176.688
196.9728 1243.073
197.4550 1308.672
197.9371 1374.090
198.4192 1439.334
198.9013 1503.444
199.3834 1566.884
199.8655 1628.654
200.3477 1685.527
200.8298 1736.681
201.3119 1786.896
201.7940 1839.286
202.2761 1894.141
202.7582 1947.275
203.2404 1998.403
203.7225 2047.403
204.2046 2093.578
204.6867 2136.285
205.1688 2178.006
205.6509 2221.326
206.1331 2267.413
206.6152 2307.846
207.0973 2340.662
207.5794 2368.244
208.0615 2398.018
208.5436 2431.172
209.0258 2463.872
209.5079 2493.599
209.9900 2519.867
210.4721 2545.847
210.9542 2572.027
211.4363 2598.127
211.9185 2623.164
212.4006 2647.199
212.8827 2670.262
213.3648 2692.555
213.8469 2714.741
214.3290 2731.934
214.8112 2743.570
215.2933 2750.577
215.7754 2755.161
216.2575 2756.363
216.7396 2755.667
217.2217 2754.974
217.7039 2755.552
218.1860 2751.202
218.6681 2740.061
219.1502 2722.401
219.6323 2702.407
220.1144 2680.770
220.5966 2656.306
221.0787 2628.839
221.5608 2598.725
222.0429 2566.526
222.5250 2532.992
223.0071 2498.043
223.4893 2460.440
223.9714 2420.053
224.4535 2378.320
224.9356 2335.301
225.4177 2289.899
225.8998 2247.262
226.3820 2209.402
226.8641 2174.982
227.3462 2138.773
227.8283 2099.452
228.3104 2060.280
228.7925 2022.585
229.2747 1986.683
229.7568 1951.398
230.2389 1917.404
230.7210 1884.148
231.2031 1849.634
231.6852 1813.354
232.1674 1776.154
232.6495 1738.463
233.1316 1699.213
233.6137 1661.781
234.0958 1626.090
234.5779 1592.031
235.0601 1559.841
235.5422 1530.515
236.0243 1502.036
236.5064 1473.314
236.9885 1444.374
237.4706 1414.454
237.9528 1382.576
238.4349 1350.148
238.9170 1320.846
239.3991 1296.369
239.8812 1272.601
240.3633 1247.723
240.8455 1220.815
241.3276 1194.931
241.8097 1169.351
242.2918 1145.078
242.7739 1124.706
243.2560 1110.386
243.7382 1096.906
244.2203 1082.154
244.7024 1065.747
245.1845 1048.208
245.6666 1028.074
246.1487 1011.194
246.6309 1002.404
247.1130 1000.319
247.5951 1000.395
248.0772 1001.308
248.5593 1003.412
249.0414 1004.260
249.5236 1002.735
250.0057 1000.611
250.4878 1001.044
250.9699 1004.520
251.4520 1009.790
251.9341 1015.979
252.4163 1022.974
252.8984 1031.700
253.3805 1042.773
253.8626 1055.346
254.3447 1067.082
254.8268 1076.641
255.3090 1088.831
255.7911 1104.801
256.2732 1124.842
256.7553 1147.479
257.2374 1173.676
257.7195 1201.718
258.2017 1228.896
258.6838 1253.268
259.1659 1281.974
259.6480 1317.571
260.1301 1359.794
260.6122 1404.702
261.0944 1452.043
261.5765 1502.759
262.0586 1557.736
262.5407 1615.919
263.0228 1680.826
263.5049 1753.165
263.9871 1833.517
264.4692 1915.872
264.9513 2000.598
265.4334 2088.019
265.9155 2180.334
266.3976 2275.486
266.8798 2376.417
267.3619 2483.885
267.8440 2597.887
268.3261 2709.370
268.8082 2816.810
269.2903 2924.396
269.7725 3035.671
270.2546 3150.703
270.7367 3261.309
271.2188 3363.194
271.7009 3458.993
272.1830 3563.594
272.6652 3678.412
273.1473 3795.727
273.6294 3911.392
274.1115 4024.579
274.5936 4139.881
275.0757 4257.326
275.5579 4378.626
276.0400 4505.258
276.5221 4637.623
277.0042 4773.372
277.4863 4911.150
277.9684 5050.880
278.4506 5193.925
278.9327 5341.387
279.4148 5490.925
279.8969 5639.356
280.3790 5787.458
280.8611 5929.053
281.3433 6064.078
281.8254 6193.012
282.3075 6305.109
282.7896 6404.313
283.2717 6479.586
283.7538 6511.732
284.2360 6500.265
284.7181 6460.619
285.2002 6404.547
285.6823 6329.222
286.1644 6206.292
286.6465 6034.589
287.1287 5823.856
287.6108 5578.986
288.0929 5301.166
288.5750 5012.416
289.0571 4715.356
289.5392 4412.470
290.0214 4118.552
290.5035 3834.641
290.9856 3560.542
291.4677 3296.603
291.9498 3042.090
292.4319 2800.375
292.9141 2568.451
293.3962 2349.758
293.8783 2152.469
294.3604 1977.583
294.8425 1819.994
295.3246 1677.639
295.8068 1547.963
296.2889 1425.047
296.7710 1305.740
297.2531 1192.503
297.7352 1089.877
298.2173 998.2153
298.6995 916.9618
299.1816 850.6467
299.6637 794.5823
300.1458 740.3612
300.6279 685.4133
301.1100 632.8879
301.5922 587.0918
302.0743 547.5232
302.5564 512.3856
303.0385 480.7810
303.5206 452.7693
304.0027 427.2974
304.4849 403.9525
304.9670 385.3857
305.4491 376.7838
305.9312 375.3855
306.4133 374.5637
306.8954 368.1763
307.3776 362.3446
307.8597 363.2603
308.3418 371.3899
308.8239 384.2245
309.3060 400.4126
309.7881 420.2479
310.2703 443.7783
310.7524 471.2915
311.2345 502.2538
311.7166 535.6967
312.1987 571.6763
312.6808 611.3259
313.1630 656.0996
313.6451 704.9817
314.1272 757.2627
314.6093 810.0400
315.0914 867.9885
315.5735 934.3368
316.0557 1007.855
316.5378 1082.725
317.0199 1156.087
317.5020 1229.881
317.9841 1306.621
318.4662 1385.669
318.9484 1467.214
319.4305 1553.318
319.9126 1641.915
320.3947 1727.799
320.8768 1805.671
321.3589 1883.946
321.8411 1967.172
322.3232 2055.579
322.8053 2146.552
323.2874 2241.116
323.7695 2337.717
324.2516 2433.807
324.7338 2527.629
325.2159 2621.892
325.6980 2717.185
326.1801 2813.813
326.6622 2911.622
327.1443 3014.423
327.6265 3117.398
328.1086 3216.085
328.5907 3307.147
329.0728 3396.821
329.5549 3487.724
330.0370 3580.284
330.5192 3664.572
331.0013 3743.778
331.4834 3812.677
331.9655 3868.658
332.4476 3912.596
332.9297 3942.330
333.4119 3957.134
333.8940 3957.476
334.3761 3945.150
334.8582 3922.426
335.3403 3884.118
335.8224 3827.988
336.3046 3754.035
336.7867 3660.544
337.2688 3543.839
337.7509 3409.814
338.2330 3265.908
338.7151 3111.383
339.1973 2952.437
339.6794 2787.809
340.1615 2618.470
340.6436 2454.417
341.1257 2297.753
341.6078 2145.723
342.0900 1991.995
342.5721 1838.293
343.0542 1696.336
343.5363 1572.920
344.0184 1465.426
344.5005 1358.370
344.9827 1251.832
345.4648 1151.813
345.9469 1068.320
346.4290 998.3885
346.9111 927.7655
347.3932 851.2660
347.8754 774.7979
348.3575 712.7480
348.8396 664.4736
349.3217 619.7300
349.8038 571.5972
350.2859 522.3303
350.7681 477.8104
351.2502 439.1990
351.7323 403.4983
352.2144 366.9324
352.6965 330.1680
353.1786 296.4440
353.6608 268.1759
354.1429 243.4357
354.6250 220.7288
355.1071 200.0900
355.5892 179.0128
356.0714 153.8290
356.5535 127.3644
357.0356 103.8011
357.5177 86.18396
357.9998 70.61267
358.4819 54.80371
358.9641 38.90796
359.4462 24.32202
359.9283 12.37390
360.4104 1.705933
360.8925 8.867676
361.3746 20.05701
361.8568 30.47180
362.3389 39.37646
362.8210 47.04907
363.3031 54.44373
363.7852 61.81677
364.2673 69.01746
364.7495 76.42786
365.2316 84.82654
365.7137 90.75159
366.1958 91.31274
366.6779 89.70349
367.1600 89.73376
367.6422 94.46863
368.1243 98.13757
368.6064 99.20398
369.0885 97.52686
369.5706 96.10364
370.0527 94.57410
370.5349 93.58093
371.0170 93.65747
371.4991 95.43066
371.9812 97.17615
372.4633 99.48010
372.9454 101.6719
373.4276 101.0164
373.9097 96.17249
374.3918 90.88477
374.8739 86.91589
375.3560 84.68665
375.8381 82.08850
376.3203 79.47083
376.8024 76.01245
377.2845 69.50366
377.7666 58.99939
378.2487 50.88257
378.7308 48.55542
379.2130 50.78381
379.6951 48.46436
380.1772 41.00171
380.6593 32.21875
381.1414 25.88855
381.6235 21.69287
382.1057 16.48169
382.5878 9.457275
383.0699 1.302856
383.5520 6.808472
384.0341 14.92249
384.5162 23.15149
384.9984 32.32568
385.4805 41.60706
385.9626 48.89661
386.4447 53.70532
386.9268 58.04260
387.4089 63.45447
387.8911 69.94458
388.3732 77.50928
388.8553 87.23108
389.3374 97.33801
389.8195 106.1117
390.3016 113.5183
390.7838 120.3447
391.2659 126.9773
391.7480 133.2833
392.2301 139.1403
392.7122 144.6431
393.1943 149.5463
393.6765 152.9103
394.1586 155.4991
394.6407 159.4742
395.1228 167.7319
395.6049 175.9144
396.0870 181.4376
396.5692 182.6936
397.0513 185.6235
397.5334 192.2765
398.0155 200.8977
398.4976 209.2682
398.9797 218.2870
399.4619 225.7732
399.9440 230.9491
400.4261 233.8408
400.9082 236.6665
401.3903 238.3259
401.8724 240.8817
402.3546 245.9404
402.8367 255.8300
403.3188 262.7892
403.8009 265.1678
404.2830 264.9364
404.7651 266.7358
405.2473 270.3239
405.7294 276.5753
406.2115 285.0133
406.6936 295.4641
407.1757 312.2021
407.6578 334.5054
408.1400 365.2633
408.6221 406.3951
409.1042 458.0212
409.5863 526.2461
410.0684 618.1105
410.5505 723.3312
411.0327 826.7413
411.5148 928.4047
411.9969 1017.415
412.4790 1084.725
412.9611 1134.784
413.4432 1175.548
413.9254 1206.961
414.4075 1235.247
414.8896 1265.415
415.3717 1297.669
415.8538 1332.391
416.3359 1366.819
416.8181 1405.477
417.3002 1452.114
417.7823 1507.293
418.2644 1567.531
418.7465 1627.603
419.2286 1694.308
419.7108 1772.708
420.1929 1857.430
420.6750 1964.389
421.1571 2092.779
421.6392 2247.843
422.1213 2440.434
422.6035 2683.291
423.0856 2954.551
423.5677 3253.442
424.0498 3587.377
424.5319 3915.340
425.0140 4237.215
425.4962 4552.844
425.9783 4866.736
426.4604 5231.643
426.9425 5523.413
427.4246 5766.161
427.9067 5937.499
428.3889 5850.485
428.8710 5427.428
429.3531 4885.514
429.8352 4300.224
430.3173 3645.069
430.7994 3125.341
431.2816 2756.919
431.7637 2509.306
432.2458 2351.922
432.7279 2286.745
433.2100 2276.809
433.6921 2312.939
434.1743 2394.124
434.6564 2516.576
435.1385 2682.067
435.6206 2881.796
436.1027 3112.916
436.5848 3372.204
437.0670 3651.677
437.5491 3951.395
438.0312 4270.149
438.5133 4627.555
438.9954 5008.639
439.4775 5371.958
439.9597 5814.187
440.4418 6155.095
440.9239 6246.051
441.4060 6078.695
441.8881 5678.472
442.3702 4888.736
442.8524 3956.480
443.3345 3110.531
443.8166 2381.788
444.2987 1783.581
444.7808 1347.892
445.2629 1049.413
445.7451 812.1719
446.2272 653.2828
446.7093 530.8877
447.1914 433.3118
447.6735 364.0927
448.1556 306.2780
448.6378 263.4683
449.1199 230.1547
449.6020 201.4604
450.0841 180.0376
450.5662 158.8407
451.0483 135.8358
451.5305 112.2498
452.0126 94.53619
452.4947 83.61041
452.9768 75.19061
453.4589 66.97632
453.9410 58.86902
454.4232 51.78162
454.9053 45.58777
455.3874 40.38647
455.8695 36.63062
456.3516 34.11066
456.8337 31.38263
457.3159 27.70673
457.7980 23.61676
458.2801 19.68494
458.7622 16.06543
459.2443 13.62048
459.7264 13.76361
460.2086 15.24048
460.6907 16.33801
461.1728 16.65948
461.6549 17.07623
462.1370 18.05585
462.6191 19.70087
463.1013 22.15839
463.5834 25.82788
464.0655 29.88483
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