#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-05-24 15:47:25 +0300 (Thu, 24 May 2018) $ #$Revision: 772 $ #$URL: svn://172.16.1.111/rod/cif/8/10/00/8100021.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_8100021 loop_ _publ_author_name 'Sahl, K.' _publ_section_title ; Zur kristallstruktur von lanarkit, Pb2O(SO4) Locality: synthetic ; _journal_name_full 'Zeitschrift fur Kristallographie' _journal_page_first 99 _journal_page_last 117 _journal_volume 132 _journal_year 1970 _chemical_compound_source R080116 _chemical_formula_sum 'O5 Pb2 S' _chemical_name_mineral Lanarkite _space_group_IT_number 12 _symmetry_space_group_name_Hall '-C 2y' _symmetry_space_group_name_H-M 'C 1 2/m 1' _cell_angle_alpha 90 _cell_angle_beta 115.93 _cell_angle_gamma 90 _cell_length_a 13.769 _cell_length_b 5.698 _cell_length_c 7.079 _cell_volume 499.477 _exptl_crystal_density_diffrn 7.001 _cod_original_formula_sum 'Pb2 S O5' _cod_database_code 9011421 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 15 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R080116.rod _rod_data_source.block 3500000 _rod_database.code 8100021 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9011421 COD http://www.crystallography.net/cod/9011421.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 130.4407 0.0000000E+00 130.9229 6.236328 131.4050 428.1543 131.8871 872.7695 132.3692 1287.809 132.8513 1762.992 133.3334 2224.658 133.8156 2636.900 134.2977 3037.195 134.7798 3496.230 135.2619 4039.963 135.7440 4672.762 136.2261 5376.742 136.7083 6130.105 137.1904 6927.020 137.6725 7784.738 138.1546 8722.031 138.6367 9742.801 139.1188 10853.64 139.6010 12056.26 140.0831 13340.95 140.5652 14711.01 141.0473 16156.66 141.5294 17698.63 142.0115 19327.25 142.4937 20995.63 142.9758 22867.48 143.4579 24984.41 143.9400 27322.15 144.4221 30082.92 144.9042 33230.68 145.3864 36807.30 145.8685 40869.38 146.3506 45756.95 146.8327 50738.87 147.3148 55864.75 147.7969 62216.82 148.2791 66237.28 148.7612 68152.59 149.2433 67787.25 149.7254 64597.39 150.2075 56464.84 150.6896 47407.04 151.1718 38868.52 151.6539 30183.38 152.1360 22924.96 152.6181 17357.41 153.1002 13249.84 153.5823 9960.708 154.0645 7706.224 154.5466 6007.438 155.0287 4650.338 155.5108 3729.021 155.9929 2967.327 156.4750 2366.956 156.9572 1907.133 157.4393 1524.446 157.9214 1220.115 158.4035 971.5220 158.8856 766.0684 159.3677 608.7529 159.8499 454.7158 160.3320 322.1233 160.8141 211.6477 161.2962 115.7390 161.7783 37.47925 162.2604 28.00635 162.7426 83.45459 163.2247 126.9702 163.7068 163.8003 164.1889 196.9939 164.6710 225.6895 165.1531 247.9490 165.6353 259.5591 166.1174 265.0144 166.5995 269.3926 167.0816 277.6812 167.5637 283.1516 168.0458 281.1357 168.5280 271.3491 169.0101 258.5923 169.4922 242.4246 169.9743 225.6626 170.4564 211.8147 170.9385 205.2441 171.4207 200.5103 171.9028 192.2090 172.3849 179.7817 172.8670 167.7332 173.3491 160.5955 173.8312 156.4663 174.3134 151.8950 174.7955 143.1326 175.2776 133.7046 175.7597 128.4880 176.2418 128.4138 176.7239 128.4778 177.2061 123.4269 177.6882 115.2472 178.1703 108.9790 178.6524 108.3422 179.1345 110.9912 179.6166 112.8860 180.0988 113.9528 180.5809 114.3336 181.0630 113.9587 181.5451 113.0784 182.0272 112.0837 182.5093 111.2659 182.9915 110.6154 183.4736 110.0834 183.9557 109.9124 184.4378 109.2816 184.9199 106.2380 185.4020 101.1544 185.8842 97.75781 186.3663 99.16235 186.8484 104.0731 187.3305 107.1558 187.8126 107.5791 188.2947 45.12329 188.7769 21.04834 189.2590 88.01001 189.7411 157.5186 190.2232 230.7065 190.7053 306.6971 191.1874 382.8512 191.6696 458.4609 192.1517 533.9930 192.6338 611.3896 193.1159 690.6420 193.5980 767.6483 194.0801 838.8029 194.5623 904.5147 195.0444 971.1870 195.5265 1039.626 196.0086 1108.815 196.4907 1176.688 196.9728 1243.073 197.4550 1308.672 197.9371 1374.090 198.4192 1439.334 198.9013 1503.444 199.3834 1566.884 199.8655 1628.654 200.3477 1685.527 200.8298 1736.681 201.3119 1786.896 201.7940 1839.286 202.2761 1894.141 202.7582 1947.275 203.2404 1998.403 203.7225 2047.403 204.2046 2093.578 204.6867 2136.285 205.1688 2178.006 205.6509 2221.326 206.1331 2267.413 206.6152 2307.846 207.0973 2340.662 207.5794 2368.244 208.0615 2398.018 208.5436 2431.172 209.0258 2463.872 209.5079 2493.599 209.9900 2519.867 210.4721 2545.847 210.9542 2572.027 211.4363 2598.127 211.9185 2623.164 212.4006 2647.199 212.8827 2670.262 213.3648 2692.555 213.8469 2714.741 214.3290 2731.934 214.8112 2743.570 215.2933 2750.577 215.7754 2755.161 216.2575 2756.363 216.7396 2755.667 217.2217 2754.974 217.7039 2755.552 218.1860 2751.202 218.6681 2740.061 219.1502 2722.401 219.6323 2702.407 220.1144 2680.770 220.5966 2656.306 221.0787 2628.839 221.5608 2598.725 222.0429 2566.526 222.5250 2532.992 223.0071 2498.043 223.4893 2460.440 223.9714 2420.053 224.4535 2378.320 224.9356 2335.301 225.4177 2289.899 225.8998 2247.262 226.3820 2209.402 226.8641 2174.982 227.3462 2138.773 227.8283 2099.452 228.3104 2060.280 228.7925 2022.585 229.2747 1986.683 229.7568 1951.398 230.2389 1917.404 230.7210 1884.148 231.2031 1849.634 231.6852 1813.354 232.1674 1776.154 232.6495 1738.463 233.1316 1699.213 233.6137 1661.781 234.0958 1626.090 234.5779 1592.031 235.0601 1559.841 235.5422 1530.515 236.0243 1502.036 236.5064 1473.314 236.9885 1444.374 237.4706 1414.454 237.9528 1382.576 238.4349 1350.148 238.9170 1320.846 239.3991 1296.369 239.8812 1272.601 240.3633 1247.723 240.8455 1220.815 241.3276 1194.931 241.8097 1169.351 242.2918 1145.078 242.7739 1124.706 243.2560 1110.386 243.7382 1096.906 244.2203 1082.154 244.7024 1065.747 245.1845 1048.208 245.6666 1028.074 246.1487 1011.194 246.6309 1002.404 247.1130 1000.319 247.5951 1000.395 248.0772 1001.308 248.5593 1003.412 249.0414 1004.260 249.5236 1002.735 250.0057 1000.611 250.4878 1001.044 250.9699 1004.520 251.4520 1009.790 251.9341 1015.979 252.4163 1022.974 252.8984 1031.700 253.3805 1042.773 253.8626 1055.346 254.3447 1067.082 254.8268 1076.641 255.3090 1088.831 255.7911 1104.801 256.2732 1124.842 256.7553 1147.479 257.2374 1173.676 257.7195 1201.718 258.2017 1228.896 258.6838 1253.268 259.1659 1281.974 259.6480 1317.571 260.1301 1359.794 260.6122 1404.702 261.0944 1452.043 261.5765 1502.759 262.0586 1557.736 262.5407 1615.919 263.0228 1680.826 263.5049 1753.165 263.9871 1833.517 264.4692 1915.872 264.9513 2000.598 265.4334 2088.019 265.9155 2180.334 266.3976 2275.486 266.8798 2376.417 267.3619 2483.885 267.8440 2597.887 268.3261 2709.370 268.8082 2816.810 269.2903 2924.396 269.7725 3035.671 270.2546 3150.703 270.7367 3261.309 271.2188 3363.194 271.7009 3458.993 272.1830 3563.594 272.6652 3678.412 273.1473 3795.727 273.6294 3911.392 274.1115 4024.579 274.5936 4139.881 275.0757 4257.326 275.5579 4378.626 276.0400 4505.258 276.5221 4637.623 277.0042 4773.372 277.4863 4911.150 277.9684 5050.880 278.4506 5193.925 278.9327 5341.387 279.4148 5490.925 279.8969 5639.356 280.3790 5787.458 280.8611 5929.053 281.3433 6064.078 281.8254 6193.012 282.3075 6305.109 282.7896 6404.313 283.2717 6479.586 283.7538 6511.732 284.2360 6500.265 284.7181 6460.619 285.2002 6404.547 285.6823 6329.222 286.1644 6206.292 286.6465 6034.589 287.1287 5823.856 287.6108 5578.986 288.0929 5301.166 288.5750 5012.416 289.0571 4715.356 289.5392 4412.470 290.0214 4118.552 290.5035 3834.641 290.9856 3560.542 291.4677 3296.603 291.9498 3042.090 292.4319 2800.375 292.9141 2568.451 293.3962 2349.758 293.8783 2152.469 294.3604 1977.583 294.8425 1819.994 295.3246 1677.639 295.8068 1547.963 296.2889 1425.047 296.7710 1305.740 297.2531 1192.503 297.7352 1089.877 298.2173 998.2153 298.6995 916.9618 299.1816 850.6467 299.6637 794.5823 300.1458 740.3612 300.6279 685.4133 301.1100 632.8879 301.5922 587.0918 302.0743 547.5232 302.5564 512.3856 303.0385 480.7810 303.5206 452.7693 304.0027 427.2974 304.4849 403.9525 304.9670 385.3857 305.4491 376.7838 305.9312 375.3855 306.4133 374.5637 306.8954 368.1763 307.3776 362.3446 307.8597 363.2603 308.3418 371.3899 308.8239 384.2245 309.3060 400.4126 309.7881 420.2479 310.2703 443.7783 310.7524 471.2915 311.2345 502.2538 311.7166 535.6967 312.1987 571.6763 312.6808 611.3259 313.1630 656.0996 313.6451 704.9817 314.1272 757.2627 314.6093 810.0400 315.0914 867.9885 315.5735 934.3368 316.0557 1007.855 316.5378 1082.725 317.0199 1156.087 317.5020 1229.881 317.9841 1306.621 318.4662 1385.669 318.9484 1467.214 319.4305 1553.318 319.9126 1641.915 320.3947 1727.799 320.8768 1805.671 321.3589 1883.946 321.8411 1967.172 322.3232 2055.579 322.8053 2146.552 323.2874 2241.116 323.7695 2337.717 324.2516 2433.807 324.7338 2527.629 325.2159 2621.892 325.6980 2717.185 326.1801 2813.813 326.6622 2911.622 327.1443 3014.423 327.6265 3117.398 328.1086 3216.085 328.5907 3307.147 329.0728 3396.821 329.5549 3487.724 330.0370 3580.284 330.5192 3664.572 331.0013 3743.778 331.4834 3812.677 331.9655 3868.658 332.4476 3912.596 332.9297 3942.330 333.4119 3957.134 333.8940 3957.476 334.3761 3945.150 334.8582 3922.426 335.3403 3884.118 335.8224 3827.988 336.3046 3754.035 336.7867 3660.544 337.2688 3543.839 337.7509 3409.814 338.2330 3265.908 338.7151 3111.383 339.1973 2952.437 339.6794 2787.809 340.1615 2618.470 340.6436 2454.417 341.1257 2297.753 341.6078 2145.723 342.0900 1991.995 342.5721 1838.293 343.0542 1696.336 343.5363 1572.920 344.0184 1465.426 344.5005 1358.370 344.9827 1251.832 345.4648 1151.813 345.9469 1068.320 346.4290 998.3885 346.9111 927.7655 347.3932 851.2660 347.8754 774.7979 348.3575 712.7480 348.8396 664.4736 349.3217 619.7300 349.8038 571.5972 350.2859 522.3303 350.7681 477.8104 351.2502 439.1990 351.7323 403.4983 352.2144 366.9324 352.6965 330.1680 353.1786 296.4440 353.6608 268.1759 354.1429 243.4357 354.6250 220.7288 355.1071 200.0900 355.5892 179.0128 356.0714 153.8290 356.5535 127.3644 357.0356 103.8011 357.5177 86.18396 357.9998 70.61267 358.4819 54.80371 358.9641 38.90796 359.4462 24.32202 359.9283 12.37390 360.4104 1.705933 360.8925 8.867676 361.3746 20.05701 361.8568 30.47180 362.3389 39.37646 362.8210 47.04907 363.3031 54.44373 363.7852 61.81677 364.2673 69.01746 364.7495 76.42786 365.2316 84.82654 365.7137 90.75159 366.1958 91.31274 366.6779 89.70349 367.1600 89.73376 367.6422 94.46863 368.1243 98.13757 368.6064 99.20398 369.0885 97.52686 369.5706 96.10364 370.0527 94.57410 370.5349 93.58093 371.0170 93.65747 371.4991 95.43066 371.9812 97.17615 372.4633 99.48010 372.9454 101.6719 373.4276 101.0164 373.9097 96.17249 374.3918 90.88477 374.8739 86.91589 375.3560 84.68665 375.8381 82.08850 376.3203 79.47083 376.8024 76.01245 377.2845 69.50366 377.7666 58.99939 378.2487 50.88257 378.7308 48.55542 379.2130 50.78381 379.6951 48.46436 380.1772 41.00171 380.6593 32.21875 381.1414 25.88855 381.6235 21.69287 382.1057 16.48169 382.5878 9.457275 383.0699 1.302856 383.5520 6.808472 384.0341 14.92249 384.5162 23.15149 384.9984 32.32568 385.4805 41.60706 385.9626 48.89661 386.4447 53.70532 386.9268 58.04260 387.4089 63.45447 387.8911 69.94458 388.3732 77.50928 388.8553 87.23108 389.3374 97.33801 389.8195 106.1117 390.3016 113.5183 390.7838 120.3447 391.2659 126.9773 391.7480 133.2833 392.2301 139.1403 392.7122 144.6431 393.1943 149.5463 393.6765 152.9103 394.1586 155.4991 394.6407 159.4742 395.1228 167.7319 395.6049 175.9144 396.0870 181.4376 396.5692 182.6936 397.0513 185.6235 397.5334 192.2765 398.0155 200.8977 398.4976 209.2682 398.9797 218.2870 399.4619 225.7732 399.9440 230.9491 400.4261 233.8408 400.9082 236.6665 401.3903 238.3259 401.8724 240.8817 402.3546 245.9404 402.8367 255.8300 403.3188 262.7892 403.8009 265.1678 404.2830 264.9364 404.7651 266.7358 405.2473 270.3239 405.7294 276.5753 406.2115 285.0133 406.6936 295.4641 407.1757 312.2021 407.6578 334.5054 408.1400 365.2633 408.6221 406.3951 409.1042 458.0212 409.5863 526.2461 410.0684 618.1105 410.5505 723.3312 411.0327 826.7413 411.5148 928.4047 411.9969 1017.415 412.4790 1084.725 412.9611 1134.784 413.4432 1175.548 413.9254 1206.961 414.4075 1235.247 414.8896 1265.415 415.3717 1297.669 415.8538 1332.391 416.3359 1366.819 416.8181 1405.477 417.3002 1452.114 417.7823 1507.293 418.2644 1567.531 418.7465 1627.603 419.2286 1694.308 419.7108 1772.708 420.1929 1857.430 420.6750 1964.389 421.1571 2092.779 421.6392 2247.843 422.1213 2440.434 422.6035 2683.291 423.0856 2954.551 423.5677 3253.442 424.0498 3587.377 424.5319 3915.340 425.0140 4237.215 425.4962 4552.844 425.9783 4866.736 426.4604 5231.643 426.9425 5523.413 427.4246 5766.161 427.9067 5937.499 428.3889 5850.485 428.8710 5427.428 429.3531 4885.514 429.8352 4300.224 430.3173 3645.069 430.7994 3125.341 431.2816 2756.919 431.7637 2509.306 432.2458 2351.922 432.7279 2286.745 433.2100 2276.809 433.6921 2312.939 434.1743 2394.124 434.6564 2516.576 435.1385 2682.067 435.6206 2881.796 436.1027 3112.916 436.5848 3372.204 437.0670 3651.677 437.5491 3951.395 438.0312 4270.149 438.5133 4627.555 438.9954 5008.639 439.4775 5371.958 439.9597 5814.187 440.4418 6155.095 440.9239 6246.051 441.4060 6078.695 441.8881 5678.472 442.3702 4888.736 442.8524 3956.480 443.3345 3110.531 443.8166 2381.788 444.2987 1783.581 444.7808 1347.892 445.2629 1049.413 445.7451 812.1719 446.2272 653.2828 446.7093 530.8877 447.1914 433.3118 447.6735 364.0927 448.1556 306.2780 448.6378 263.4683 449.1199 230.1547 449.6020 201.4604 450.0841 180.0376 450.5662 158.8407 451.0483 135.8358 451.5305 112.2498 452.0126 94.53619 452.4947 83.61041 452.9768 75.19061 453.4589 66.97632 453.9410 58.86902 454.4232 51.78162 454.9053 45.58777 455.3874 40.38647 455.8695 36.63062 456.3516 34.11066 456.8337 31.38263 457.3159 27.70673 457.7980 23.61676 458.2801 19.68494 458.7622 16.06543 459.2443 13.62048 459.7264 13.76361 460.2086 15.24048 460.6907 16.33801 461.1728 16.65948 461.6549 17.07623 462.1370 18.05585 462.6191 19.70087 463.1013 22.15839 463.5834 25.82788 464.0655 29.88483 464.5476 33.67670 465.0297 37.37207 465.5118 42.31781 465.9940 50.43304 466.4761 58.49603 466.9582 64.45905 467.4403 65.20184 467.9224 69.49481 468.4045 79.83997 468.8867 92.77338 469.3688 103.3948 469.8509 109.8547 470.3330 117.1158 470.8151 126.5342 471.2972 137.8188 471.7794 148.3483 472.2615 158.1484 472.7436 167.5743 473.2257 176.5421 473.7078 185.0273 474.1899 194.4761 474.6721 205.0164 475.1542 216.6472 475.6363 230.0694 476.1184 244.8887 476.6005 258.6985 477.0826 269.2096 477.5648 278.9222 478.0469 293.1604 478.5290 311.4117 479.0111 329.0139 479.4932 342.5726 479.9753 353.7078 480.4575 364.4499 480.9396 375.4944 481.4217 385.1939 481.9038 392.0616 482.3859 396.8196 482.8680 400.4873 483.3502 402.7314 483.8323 404.6213 484.3144 408.1016 484.7965 412.7004 485.2786 412.1573 485.7607 401.9611 486.2429 389.0981 486.7250 376.9459 487.2071 366.0488 487.6892 355.1581 488.1713 344.9484 488.6534 334.3054 489.1356 320.8468 489.6177 302.8457 490.0998 287.1470 490.5819 276.1738 491.0640 268.5177 491.5461 256.7084 492.0283 240.1246 492.5104 223.8634 492.9925 211.7964 493.4746 203.0590 493.9567 194.8375 494.4388 186.8939 494.9210 178.9517 495.4031 170.3171 495.8852 161.3171 496.3673 152.5143 496.8494 144.0342 497.3315 136.0306 497.8137 128.3717 498.2958 121.1296 498.7779 115.0906 499.2600 111.9427 499.7421 109.2010 500.2242 104.8352 500.7064 97.99811 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527.7049 4.359741 528.1870 4.286621 528.6691 8.192383 529.1512 12.68958 529.6334 13.04852 530.1155 8.792480 530.5976 5.004639 531.0797 5.005249 531.5618 6.783691 532.0439 8.328125 532.5261 8.336365 533.0082 9.204834 533.4903 13.04132 533.9724 18.01996 534.4545 20.27289 534.9366 16.66461 535.4188 13.50055 535.9009 12.37531 536.3830 13.24097 536.8651 13.91022 537.3472 14.71240 537.8293 14.71387 538.3115 12.46759 538.7936 7.615234 539.2757 6.343750 539.7578 9.762512 540.2399 14.54248 540.7220 16.51483 541.2042 15.91705 541.6863 14.05072 542.1684 10.40930 542.6505 6.735901 543.1326 5.973145 543.6147 7.482300 544.0969 8.810486 544.5790 8.275818 545.0611 7.114746 545.5432 6.270752 546.0253 5.833801 546.5074 5.573608 546.9896 5.421082 547.4717 5.403137 547.9538 5.579773 548.4359 7.375244 548.9180 7.399231 549.4001 3.562988 549.8823 1.628845 550.3644 3.736694 550.8465 0.9254760 551.3286 1.474060 551.8107 2.046875 552.2928 1.053650 552.7750 0.4667360 553.2571 0.3792110 553.7392 0.2139890 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