#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 10:40:57 +0300 (Thu, 07 Jun 2018) $
#$Revision: 917 $
#$URL: svn://172.16.1.111/rod/cif/8/10/00/8100025.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_8100025
loop_
_publ_author_name
'Newnham, R. E.'
'de Haan, Y. M.'
_publ_section_title
;
 Refinement of the alpha Al2O3, Ti2O3, V2O3 and Cr2O3 structures Locality:
 synthetic
;
_journal_name_full               'Zeitschrift fur Kristallographie'
_journal_page_first              235
_journal_page_last               237
_journal_volume                  117
_journal_year                    1962
_chemical_compound_source        R040096
_chemical_formula_sum            'Al2 O3'
_chemical_name_mineral           Corundum
_space_group_IT_number           167
_symmetry_space_group_name_Hall  '-R 3 2"c'
_symmetry_space_group_name_H-M   'R -3 c :H'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_length_a                   4.7589
_cell_length_b                   4.7589
_cell_length_c                   12.991
_cell_volume                     254.792
_exptl_crystal_density_diffrn    3.987
_cod_original_sg_symbol_H-M      'R -3 c'
_cod_database_code               9008081
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R040096.rod
_rod_data_source.block           3500000
_rod_database.code               8100025
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9008081 COD http://www.crystallography.net/cod/9008081.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
147.6079 0.0000000E+00
148.0901 5.562500
148.5722 10.19238
149.0543 12.61133
149.5364 8.908203
150.0185 4.577148
150.5006 1.544922
150.9828 0.4414060
151.4649 8.311523
151.9470 24.35742
152.4291 45.79785
152.9112 83.50684
153.3933 120.7510
153.8755 146.4023
154.3576 149.7236
154.8397 150.5127
155.3218 152.0488
155.8039 154.3018
156.2860 157.8652
156.7682 170.6006
157.2503 182.5898
157.7324 187.8516
158.2145 156.8252
158.6966 121.4541
159.1787 98.94824
159.6609 80.54199
160.1430 99.74121
160.6251 207.6689
161.1072 361.1631
161.5893 467.5811
162.0714 480.3438
162.5536 442.2422
163.0357 379.0527
163.5178 263.9980
163.9999 163.5781
164.4820 119.9023
164.9641 124.5078
165.4463 130.3066
165.9284 113.6445
166.4105 83.96387
166.8926 53.74023
167.3747 16.83301
167.8568 9.709961
168.3390 9.775391
168.8211 17.86328
169.3032 49.25000
169.7853 75.41309
170.2674 88.29004
170.7495 92.82617
171.2317 85.75293
171.7138 71.74219
172.1959 54.62695
172.6780 33.02051
173.1601 17.80762
173.6422 22.15820
174.1244 40.25684
174.6065 57.93262
175.0886 72.40430
175.5707 76.08496
176.0528 73.76172
176.5349 59.88770
177.0171 50.65430
177.4992 72.04980
177.9813 119.5879
178.4634 164.2510
178.9455 189.3115
179.4276 194.5439
179.9098 179.1631
180.3919 131.1162
180.8740 79.74414
181.3561 43.80469
181.8382 36.41895
182.3203 40.79102
182.8025 45.66211
183.2846 35.55176
183.7667 30.64746
184.2488 33.09668
184.7309 44.95410
185.2130 80.99023
185.6951 149.3535
186.1773 214.2510
186.6594 220.0537
187.1415 172.1377
187.6236 122.4570
188.1057 97.33203
188.5878 93.87891
189.0700 98.46387
189.5521 114.5957
190.0342 129.5771
190.5163 106.8818
190.9984 44.52539
191.4805 1.681641
191.9627 29.84961
192.4448 130.1357
192.9269 187.3027
193.4090 169.6396
193.8911 104.0049
194.3732 71.94922
194.8554 78.71582
195.3375 98.94727
195.8196 110.0010
196.3017 114.2178
196.7838 112.1221
197.2659 101.8789
197.7481 85.26367
198.2302 69.22363
198.7123 50.40723
199.1944 42.84082
199.6765 79.75684
200.1586 172.1885
200.6408 227.5391
201.1229 193.9121
201.6050 69.58008
202.0871 1.828125
202.5692 9.005859
203.0513 19.80176
203.5335 39.51367
204.0156 49.63965
204.4977 55.55957
204.9798 58.67090
205.4619 59.54785
205.9440 60.11816
206.4262 58.28613
206.9083 57.32129
207.3904 69.02832
207.8725 99.36816
208.3546 125.4902
208.8367 132.1396
209.3189 114.0088
209.8010 98.22656
210.2831 87.32031
210.7652 80.45898
211.2473 75.97266
211.7294 78.54785
212.2116 74.84863
212.6937 47.53809
213.1758 19.79590
213.6579 55.07129
214.1400 37.62695
214.6221 28.31836
215.1043 77.00391
215.5864 111.7988
216.0685 126.1875
216.5506 104.9824
217.0327 23.99902
217.5148 29.99805
217.9970 29.62598
218.4791 29.24512
218.9612 67.31836
219.4433 74.83789
219.9254 70.42871
220.4075 78.92871
220.8897 106.1494
221.3718 133.4600
221.8539 156.5371
222.3360 177.6289
222.8181 182.5156
223.3002 160.8623
223.7824 129.2207
224.2645 120.8408
224.7466 153.6562
225.2287 178.6924
225.7108 172.2363
226.1929 115.1426
226.6750 84.56836
227.1572 86.48145
227.6393 112.5098
228.1214 144.7549
228.6035 194.2041
229.0856 235.3408
229.5677 250.0947
230.0499 222.6660
230.5320 207.2178
231.0141 210.3223
231.4962 227.4355
231.9783 240.7002
232.4604 252.8311
232.9426 256.9971
233.4247 247.3457
233.9068 214.2217
234.3889 187.0850
234.8710 168.8623
235.3531 159.1377
235.8353 155.0898
236.3174 161.7305
236.7995 168.6621
237.2816 167.6064
237.7637 153.6143
238.2458 141.1572
238.7280 130.0596
239.2101 120.5029
239.6922 125.3633
240.1743 163.8359
240.6564 197.7295
241.1385 185.6172
241.6207 84.37598
242.1028 13.22852
242.5849 0.6826170
243.0670 47.09570
243.5491 100.2725
244.0313 168.5352
244.5134 233.7627
244.9955 273.0615
245.4776 271.1934
245.9597 270.5879
246.4418 288.2383
246.9240 333.8867
247.4061 339.2646
247.8882 282.8799
248.3703 202.1299
248.8524 152.1953
249.3345 142.5254
249.8167 145.5518
250.2988 152.8174
250.7809 162.6621
251.2630 167.7197
251.7451 166.2539
252.2272 161.7100
252.7094 160.5488
253.1915 163.6230
253.6736 168.4951
254.1557 173.6250
254.6378 176.5146
255.1199 189.4600
255.6021 226.6602
256.0842 267.3506
256.5663 259.4521
257.0484 164.6172
257.5305 80.00586
258.0126 57.02930
258.4948 126.9639
258.9769 171.9072
259.4590 181.3320
259.9411 164.5918
260.4232 159.9590
260.9053 177.3271
261.3875 193.1855
261.8696 194.5244
262.3517 175.3760
262.8338 159.4209
263.3159 145.2041
263.7980 138.1035
264.2802 151.2510
264.7623 188.4531
265.2444 222.6904
265.7265 244.2217
266.2086 252.4951
266.6907 251.0889
267.1729 231.5918
267.6550 202.9834
268.1371 205.4004
268.6192 252.5566
269.1013 299.4736
269.5834 309.7598
270.0656 272.2031
270.5477 250.4697
271.0298 257.1973
271.5119 282.4326
271.9940 284.1221
272.4761 256.0508
272.9583 224.8213
273.4404 213.9932
273.9225 228.0342
274.4046 238.3838
274.8867 240.6934
275.3688 233.8594
275.8510 224.5908
276.3331 216.5557
276.8152 203.3486
277.2973 175.0371
277.7794 128.1855
278.2615 99.47559
278.7437 100.4189
279.2258 124.3232
279.7079 138.9277
280.1900 141.1133
280.6721 146.1982
281.1542 178.6396
281.6364 240.9619
282.1185 270.6279
282.6006 239.9580
283.0827 169.5117
283.5648 153.7822
284.0469 203.6396
284.5291 251.5615
285.0112 216.5928
285.4933 102.0830
285.9754 16.28613
286.4575 6.939453
286.9396 16.93945
287.4217 40.76855
287.9038 65.49023
288.3860 85.20801
288.8681 91.07129
289.3502 84.34570
289.8323 79.02539
290.3144 78.47949
290.7965 81.79199
291.2787 85.59277
291.7608 89.60938
292.2429 97.45703
292.7250 122.2520
293.2071 158.0762
293.6892 174.1602
294.1714 150.9502
294.6535 106.1035
295.1356 77.89941
295.6177 67.04102
296.0998 61.57617
296.5819 49.69531
297.0641 33.91699
297.5462 22.21777
298.0283 16.85938
298.5104 17.46973
298.9925 27.88086
299.4746 48.01465
299.9568 62.79199
300.4389 53.31836
300.9210 30.38672
301.4031 14.68262
301.8852 14.13379
302.3673 23.92676
302.8495 43.79102
303.3316 72.95703
303.8137 95.83789
304.2958 99.79492
304.7779 88.17773
305.2600 66.59668
305.7422 23.56055
306.2243 19.87500
306.7064 48.56543
307.1885 62.27734
307.6706 51.35156
308.1527 14.26367
308.6349 103.8369
309.1170 173.2949
309.5991 213.7217
310.0812 224.1943
310.5633 188.1963
311.0454 109.0352
311.5276 43.72070
312.0097 44.36230
312.4918 71.34863
312.9739 80.56250
313.4560 27.23438
313.9381 23.89746
314.4203 28.30371
314.9024 10.09375
315.3845 40.04199
315.8666 23.32715
316.3487 6.312500
316.8308 17.94531
317.3130 13.69336
317.7951 49.87207
318.2772 80.23145
318.7593 104.0869
319.2414 114.0928
319.7235 106.4980
320.2057 84.80273
320.6878 51.82812
321.1699 29.46289
321.6520 83.64453
322.1341 74.01465
322.6162 7.859375
323.0984 39.00488
323.5805 23.91992
324.0626 1.611328
324.5447 9.018555
325.0268 110.0830
325.5089 176.3682
325.9911 172.7256
326.4732 106.4131
326.9553 58.13281
327.4374 37.55273
327.9195 32.43555
328.4016 35.43945
328.8838 53.16602
329.3659 70.19531
329.8480 87.33008
330.3301 103.4004
330.8122 112.1211
331.2943 105.2461
331.7765 99.06348
332.2586 103.5225
332.7407 128.3955
333.2228 144.9746
333.7049 139.6221
334.1870 124.4531
334.6692 153.9990
335.1513 255.0273
335.6334 358.7822
336.1155 432.4033
336.5976 483.1758
337.0797 479.0625
337.5619 398.7969
338.0440 270.8975
338.5261 179.7227
339.0082 132.0615
339.4903 100.3750
339.9724 70.58203
340.4546 41.63477
340.9367 21.26953
341.4188 9.771484
341.9009 7.045898
342.3830 18.71973
342.8651 47.43457
343.3473 67.04004
343.8294 57.23535
344.3115 20.69824
344.7936 5.746094
345.2757 20.22754
345.7578 26.55566
346.2400 31.82617
346.7221 35.62207
347.2042 31.28613
347.6863 15.82031
348.1684 10.39551
348.6505 51.04590
349.1327 109.9932
349.6148 166.7100
350.0969 196.4141
350.5790 202.3789
351.0611 197.9033
351.5432 185.3711
352.0254 167.0996
352.5075 141.0859
352.9896 105.3857
353.4717 81.17188
353.9538 96.24902
354.4359 136.7627
354.9181 174.9199
355.4002 206.2568
355.8823 225.9482
356.3644 226.4727
356.8465 208.1553
357.3286 185.3613
357.8108 165.2148
358.2929 146.6211
358.7750 127.7900
359.2571 95.08691
359.7392 73.20898
360.2213 79.23340
360.7035 111.8818
361.1856 150.7949
361.6677 215.7334
362.1498 268.7686
362.6319 277.9434
363.1140 157.7451
363.5962 69.80078
364.0783 75.69141
364.5604 163.2588
365.0425 243.8164
365.5246 309.7930
366.0067 359.9307
366.4889 388.4639
366.9710 358.2012
367.4531 348.5537
367.9352 381.8193
368.4173 446.1074
368.8994 488.3096
369.3815 478.8389
369.8636 471.8584
370.3458 490.7012
370.8279 549.1729
371.3100 609.4375
371.7921 664.7148
372.2742 723.0117
372.7563 800.6602
373.2385 891.0547
373.7206 1004.673
374.2027 1141.358
374.6848 1296.440
375.1669 1488.553
375.6490 1700.198
376.1312 1964.042
376.6133 2345.514
377.0954 2860.681
377.5775 3440.573
378.0596 4152.354
378.5417 4972.203
379.0239 5492.058
379.5060 5708.584
379.9881 5622.719
380.4702 5128.184
380.9523 4232.228
381.4344 3346.174
381.9166 2556.620
382.3987 1887.089
382.8808 1372.581
383.3629 1020.231
383.8450 771.2500
384.3271 601.7393
384.8093 497.3145
385.2914 419.8311
385.7735 363.8193
386.2556 324.0771
386.7377 289.1025
387.2198 261.3164
387.7020 259.7295
388.1841 342.5625
388.6662 446.2959
389.1483 481.7490
389.6304 399.2920
390.1125 288.9238
390.5947 206.0869
391.0768 147.9199
391.5589 107.4834
392.0410 92.23730
392.5231 86.71973
393.0052 79.11426
393.4874 64.63867
393.9695 54.97559
394.4516 54.00293
394.9337 60.69434
395.4158 73.26367
395.8979 97.43555
396.3801 121.5674
396.8622 137.0801
397.3443 136.1055
397.8264 151.8174
398.3085 211.9131
398.7906 282.4912
399.2728 321.9004
399.7549 288.9482
400.2370 270.4619
400.7191 279.4922
401.2012 316.4775
401.6833 380.4707
402.1655 477.9453
402.6476 595.2959
403.1297 724.9922
403.6118 881.3428
404.0939 1016.809
404.5760 1119.449
405.0582 1195.382
405.5403 1268.695
406.0224 1333.743
406.5045 1408.488
406.9866 1503.413
407.4688 1618.332
407.9509 1757.076
408.4330 1921.786
408.9151 2109.146
409.3972 2304.601
409.8793 2506.970
410.3615 2749.766
410.8436 3049.976
411.3257 3408.601
411.8078 3805.238
412.2899 4228.275
412.7720 4747.295
413.2542 5359.121
413.7363 6112.156
414.2184 7169.598
414.7005 8577.298
415.1826 10331.74
415.6647 12552.17
416.1469 15228.33
416.6290 17939.61
417.1111 21247.60
417.5932 24160.82
418.0753 25296.05
418.5574 23358.24
419.0396 20320.38
419.5217 16611.08
420.0038 12431.25
420.4859 8862.120
420.9680 6468.629
421.4501 4770.164
421.9323 3506.564
422.4144 2788.449
422.8965 2237.340
423.3786 1814.276
423.8607 1510.899
424.3428 1296.556
424.8250 1213.655
425.3071 1178.251
425.7892 1164.030
426.2713 1172.754
426.7534 1196.510
427.2355 1220.463
427.7177 1268.430
428.1998 1383.412
428.6819 1601.711
429.1640 1805.684
429.6461 1976.864
430.1282 2111.602
430.6104 2170.274
431.0925 2149.401
431.5746 2059.837
432.0567 1888.872
432.5388 1633.521
433.0209 1400.206
433.5031 1212.745
433.9852 1060.249
434.4673 918.4678
434.9494 787.8809
435.4315 653.2275
435.9136 479.7197
436.3958 295.4355
436.8779 176.7998
437.3600 145.3232
437.8421 155.3760
438.3242 170.3467
438.8063 188.4141
439.2885 204.1982
439.7706 203.1973
440.2527 205.5107
440.7348 242.5000
441.2169 322.3340
441.6990 373.8916
442.1812 332.0938
442.6633 248.1309
443.1454 182.6328
443.6275 154.8711
444.1096 147.8975
444.5917 166.6777
445.0739 208.3223
445.5560 236.4219
446.0381 233.6436
446.5202 221.9395
447.0023 214.1201
447.4844 204.3223
447.9666 207.0703
448.4487 218.7305
448.9308 243.4756
449.4129 302.0449
449.8950 443.4160
450.3771 536.0518
450.8593 510.1816
451.3413 336.2744
451.8235 222.4902
452.3056 185.7930
452.7877 184.1689
453.2698 152.4863
453.7519 87.28516
454.2340 51.28516
454.7162 81.58203
455.1983 152.0430
455.6804 154.8047
456.1625 86.15820
456.6446 9.542969
457.1267 27.32812
457.6089 30.71484
458.0910 15.84473
458.5731 22.90430
459.0552 62.46582
459.5373 73.49902
460.0194 61.49512
460.5016 44.70312
460.9837 25.63672
461.4658 11.09668
461.9479 11.59570
462.4300 32.45312
462.9121 45.09863
463.3943 26.58496
463.8764 3.353516
464.3585 25.61328
464.8406 31.00195
465.3227 31.69434
465.8048 32.64551
466.2870 33.98535
466.7691 29.40332
467.2512 13.06836
467.7333 6.450195
468.2154 23.98145
468.6975 44.78320
469.1797 56.58984
469.6618 57.02539
470.1439 49.93945
470.6260 48.91113
471.1081 64.79590
471.5902 73.54980
472.0724 60.51270
472.5545 23.44531
473.0366 1.407227
473.5187 3.477539
474.0008 1.028320
474.4829 10.77734
474.9651 24.67383
475.4472 27.52246
475.9293 8.095703
476.4114 20.26660
476.8935 29.82324
477.3756 21.31152
477.8578 6.529297
478.3399 8.257813
478.8220 23.46094
479.3041 41.24512
479.7862 65.79883
480.2683 83.77832
480.7505 74.12500
481.2326 50.54102
481.7147 41.82129
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1253.583 294.1406
1254.065 280.2207
1254.547 274.3086
1255.030 274.4961
1255.512 282.5078
1255.994 288.0645
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1256.958 285.3828
1257.440 264.7051
1257.922 246.0410
1258.404 259.9219
1258.886 332.1113
1259.369 319.7695
1259.851 194.0000
1260.333 92.98047
1260.815 84.60547
1261.297 124.2324
1261.779 158.2168
1262.261 189.4160
1262.743 222.2266
1263.226 271.4414
1263.708 285.1758
1264.190 256.9219
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1265.154 206.4531
1265.636 207.0898
1266.118 252.5078
1266.600 303.2266
1267.083 274.0312
1267.565 168.6641
1268.047 98.80469
1268.529 45.44922
1269.011 23.84375
1269.493 70.12109
1269.975 115.9375
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1271.904 82.39844
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1273.350 48.49219
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1274.314 186.3789
1274.796 227.9844
1275.278 246.4023
1275.761 244.3477
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1277.207 183.7422
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1281.064 108.7383
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1284.921 77.12891
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1286.367 198.8086
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1288.296 143.9453
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1289.742 138.4297
1290.224 164.6016
1290.706 156.3047
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1291.670 46.52344
1292.153 7.132813
1292.635 5.898438
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1294.563 44.80078
1295.045 0.4921880
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1299.384 85.20312
1299.866 25.50781
1300.349 1.070313
1300.831 49.37891
1301.313 58.77734
1301.795 0.0000000E+00
