#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 10:43:20 +0300 (Thu, 07 Jun 2018) $
#$Revision: 955 $
#$URL: svn://172.16.1.111/rod/cif/8/10/00/8100028.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_8100028
loop_
_publ_author_name
'Newnham, R. E.'
'de Haan, Y. M.'
_publ_section_title
;
 Refinement of the alpha Al2O3, Ti2O3, V2O3 and Cr2O3 structures Locality:
 synthetic
;
_journal_name_full               'Zeitschrift fur Kristallographie'
_journal_page_first              235
_journal_page_last               237
_journal_volume                  117
_journal_year                    1962
_chemical_compound_source        R110099
_chemical_formula_sum            'Al2 O3'
_chemical_name_mineral           Corundum
_space_group_IT_number           167
_symmetry_space_group_name_Hall  '-R 3 2"c'
_symmetry_space_group_name_H-M   'R -3 c :H'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_length_a                   4.7589
_cell_length_b                   4.7589
_cell_length_c                   12.991
_cell_volume                     254.792
_exptl_crystal_density_diffrn    3.987
_cod_original_sg_symbol_H-M      'R -3 c'
_cod_database_code               9008081
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R110099.rod
_rod_data_source.block           3500000
_rod_database.code               8100028
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9008081 COD http://www.crystallography.net/cod/9008081.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
176.3090 0.0000000E+00
176.7911 0.3026960
177.2732 2.4955999E-02
177.7553 0.6587600
178.2374 1.720100
178.7195 2.844322
179.2017 5.307182
179.6838 6.622421
180.1659 5.948250
180.6480 3.156746
181.1301 0.2866210
181.6122 0.5231700
182.0944 0.2555160
182.5765 1.095573
183.0586 1.032249
183.5407 0.6098330
184.0228 1.145874
184.5049 2.762711
184.9871 4.673462
185.4692 6.125626
185.9513 7.126770
186.4334 7.599136
186.9155 7.111679
187.3976 6.029861
187.8798 5.672104
188.3619 6.192429
188.8440 6.995178
189.3261 7.327835
189.8082 7.210266
190.2903 6.811584
190.7725 6.132416
191.2546 5.209114
191.7367 4.208130
192.2188 3.027924
192.7009 2.028229
193.1830 1.987877
193.6652 2.906441
194.1473 3.877052
194.6294 4.366539
195.1115 4.416946
195.5936 4.640579
196.0757 5.209824
196.5579 5.733315
197.0400 5.261078
197.5221 3.693542
198.0042 2.208717
198.4863 1.409874
198.9684 1.302284
199.4506 1.647118
199.9327 2.588326
200.4148 3.763550
200.8969 4.363647
201.3790 4.340149
201.8611 4.054146
202.3433 3.507797
202.8254 2.621628
203.3075 2.507759
203.7896 3.512032
204.2717 5.099159
204.7538 5.792892
205.2360 5.367722
205.7181 4.882660
206.2002 4.987343
206.6823 5.765495
207.1644 6.614601
207.6465 7.620842
208.1287 8.592300
208.6108 8.892952
209.0929 8.324982
209.5750 7.632851
210.0571 7.315880
210.5392 7.486656
211.0214 7.492386
211.5035 7.264610
211.9856 6.842415
212.4677 6.288124
212.9498 5.475601
213.4319 4.814766
213.9140 4.677917
214.3962 5.354980
214.8783 5.464569
215.3604 4.620674
215.8425 3.160500
216.3246 2.541359
216.8067 3.113831
217.2889 3.864212
217.7710 4.145065
218.2531 3.667686
218.7352 3.651459
219.2173 4.453682
219.6994 5.801323
220.1816 6.285629
220.6637 5.459618
221.1458 4.555161
221.6279 4.487717
222.1100 5.867653
222.5921 6.400528
223.0743 5.507011
223.5564 3.612053
224.0385 2.770813
224.5206 3.593460
225.0027 4.529518
225.4848 4.529190
225.9670 2.978477
226.4491 2.004715
226.9312 1.949890
227.4133 2.610909
227.8954 2.984955
228.3775 2.865578
228.8597 2.754875
229.3418 2.925598
229.8239 3.338348
230.3060 4.172943
230.7881 5.818581
231.2702 7.942635
231.7524 8.808815
232.2345 7.789818
232.7166 6.392197
233.1987 5.489578
233.6808 5.290497
234.1629 5.121643
234.6451 5.010948
235.1272 4.909332
235.6093 4.563736
236.0914 3.715042
236.5735 2.971573
237.0556 2.677444
237.5378 2.980759
238.0199 3.449799
238.5020 4.216148
238.9841 5.138962
239.4662 5.580299
239.9483 5.487305
240.4305 5.145432
240.9126 4.709732
241.3947 4.158035
241.8768 3.552948
242.3589 2.810715
242.8410 2.024109
243.3232 1.524315
243.8053 1.429146
244.2874 1.462044
244.7695 1.499336
245.2516 1.574265
245.7337 1.574097
246.2159 1.481903
246.6980 1.310493
247.1801 1.073128
247.6622 0.6065830
248.1443 0.3130490
248.6264 0.4030840
249.1086 1.014610
249.5907 1.704208
250.0728 2.616989
250.5549 3.562401
251.0370 3.966362
251.5191 3.458817
252.0013 3.000961
252.4834 3.075470
252.9655 4.022263
253.4476 4.627121
253.9297 4.900597
254.4118 4.829742
254.8940 4.337387
255.3761 3.220184
255.8582 2.033333
256.3403 0.9169620
256.8224 0.3134310
257.3046 0.8267750
257.7867 0.4004670
258.2688 0.5995410
258.7509 1.505676
259.2330 2.330811
259.7151 3.017662
260.1973 3.608360
260.6794 4.194458
261.1615 4.134155
261.6436 3.033371
262.1257 1.629005
262.6078 1.290962
263.0900 2.502731
263.5721 3.641167
264.0542 4.166275
264.5363 4.032692
265.0184 3.538094
265.5005 2.408020
265.9827 1.229729
266.4648 0.9099960
266.9469 1.720360
267.4290 2.626297
267.9111 3.447128
268.3932 4.209610
268.8754 4.236298
269.3575 3.266396
269.8396 2.064217
270.3217 1.537849
270.8038 1.803947
271.2859 2.076302
271.7681 2.060333
272.2502 1.776207
272.7323 1.878326
273.2144 2.562759
273.6965 3.297600
274.1786 3.373924
274.6608 2.602676
275.1429 2.316498
275.6250 3.037308
276.1071 4.574585
276.5892 5.499321
277.0714 5.718475
277.5535 5.547935
278.0356 5.169861
278.5177 4.549042
278.9998 4.066650
279.4819 3.756180
279.9641 3.707031
280.4462 4.112091
280.9283 4.999382
281.4104 6.020897
281.8925 6.995621
282.3746 7.920685
282.8568 8.475868
283.3389 8.525070
283.8210 8.292595
284.3031 8.478630
284.7852 9.142738
285.2673 9.746773
285.7495 9.841255
286.2316 9.470940
286.7137 9.183937
287.1958 9.030197
287.6779 9.023094
288.1600 9.355354
288.6422 10.03694
289.1243 10.44507
289.6064 9.983948
290.0885 8.833794
290.5706 7.938492
291.0527 7.393173
291.5349 7.097191
292.0170 6.835838
292.4991 6.632156
292.9812 6.737709
293.4633 7.363556
293.9454 8.411278
294.4276 9.775063
294.9097 11.57960
295.3918 13.06018
295.8739 12.80759
296.3560 11.19003
296.8381 9.935226
297.3203 10.10826
297.8024 11.16867
298.2845 12.06174
298.7666 12.76562
299.2487 13.35630
299.7308 14.17497
300.2130 14.99245
300.6951 15.12923
301.1772 13.76259
301.6593 11.83725
302.1414 10.78501
302.6235 10.59626
303.1057 10.48140
303.5878 9.594910
304.0699 8.339600
304.5520 7.491127
305.0341 7.518585
305.5162 7.859756
305.9984 8.102219
306.4805 8.210670
306.9626 7.955269
307.4447 6.559746
307.9268 4.896278
308.4089 4.219925
308.8911 5.416588
309.3732 6.808121
309.8553 7.104095
310.3374 6.484192
310.8195 5.548584
311.3016 4.090378
311.7838 2.759552
312.2659 2.236061
312.7480 2.979027
313.2301 3.761864
313.7122 3.895332
314.1943 3.541367
314.6765 3.032753
315.1586 2.080200
315.6407 1.337585
316.1228 1.396431
316.6049 2.605972
317.0870 3.408417
317.5692 2.684235
318.0513 1.229019
318.5334 0.1574940
319.0155 0.1017230
319.4976 0.2712020
319.9797 0.3508990
320.4619 0.3090360
320.9440 0.2921830
321.4261 0.2670360
321.9082 0.3187260
322.3903 0.5286640
322.8724 1.288025
323.3546 1.828438
323.8367 1.810432
324.3188 1.257126
324.8009 0.9020920
325.2830 1.329140
325.7651 1.708359
326.2473 1.502022
326.7294 0.2320480
327.2115 1.518921
327.6936 2.092514
328.1757 2.036652
328.6578 1.807495
329.1400 1.180763
329.6221 0.5726620
330.1042 0.1717990
330.5863 0.2734830
331.0684 7.8025997E-02
331.5505 0.6605450
332.0327 1.648262
332.5148 2.207771
332.9969 2.030251
333.4790 1.832069
333.9611 1.882439
334.4432 2.290230
334.9254 2.518730
335.4075 2.639671
335.8896 2.545433
336.3717 1.950455
336.8538 0.4511260
337.3359 0.8306810
337.8180 1.526031
338.3001 1.640144
338.7823 1.478737
339.2644 0.9856800
339.7465 0.3288040
340.2286 0.4456410
340.7107 1.423607
341.1928 1.949753
341.6750 1.757462
342.1571 1.061089
342.6392 0.7083740
343.1213 0.7400130
343.6034 0.8853910
344.0855 0.9475860
344.5677 0.9320370
345.0498 1.003349
345.5319 1.221848
346.0140 1.468040
346.4961 1.486412
346.9782 1.285065
347.4604 1.057953
347.9425 0.9106520
348.4246 0.8261570
348.9067 0.7394790
349.3888 0.6396940
349.8709 0.5745540
350.3531 0.6254040
350.8352 0.7667010
351.3173 0.9038700
351.7994 0.8995590
352.2815 0.8975140
352.7636 1.278664
353.2458 2.040977
353.7279 2.619576
354.2100 2.323044
354.6921 1.546783
355.1742 0.9825520
355.6563 0.9382250
356.1385 1.083366
356.6206 0.9330750
357.1027 0.6156010
357.5848 0.7648700
358.0669 2.492508
358.5490 4.501282
359.0312 5.491631
359.5133 4.924110
359.9954 3.987251
360.4775 2.967903
360.9596 2.078224
361.4417 1.778366
361.9239 2.664497
362.4060 3.867279
362.8881 4.907616
363.3702 5.689369
363.8523 6.557762
364.3344 7.542725
364.8166 8.702080
365.2987 10.11366
365.7808 12.39214
366.2629 14.29086
366.7450 15.28838
367.2271 15.38557
367.7093 15.68082
368.1914 16.65232
368.6735 17.63860
369.1556 18.20404
369.6377 17.07564
370.1198 17.09519
370.6020 18.76402
371.0841 21.71080
371.5662 24.61363
372.0483 27.30766
372.5304 30.10631
373.0125 32.97821
373.4947 35.37995
373.9768 39.40955
374.4589 45.45010
374.9410 52.85654
375.4231 60.43532
375.9052 67.95187
376.3874 76.40100
376.8695 85.71215
377.3516 96.05502
377.8337 109.9468
378.3158 129.3835
378.7979 147.4149
379.2801 158.6560
379.7622 163.3707
380.2443 156.6761
380.7264 134.4871
381.2085 102.8038
381.6906 75.95088
382.1728 53.99413
382.6549 36.98145
383.1370 26.78355
383.6191 22.02938
384.1012 17.80282
384.5833 13.50283
385.0655 9.682686
385.5476 7.411903
386.0297 6.439880
386.5118 5.851349
386.9939 5.389656
387.4760 4.989845
387.9582 4.558899
388.4403 4.065361
388.9224 3.520988
389.4045 2.748840
389.8866 1.963814
390.3687 1.506836
390.8509 1.832115
391.3330 2.159729
391.8151 1.893814
392.2972 1.142761
392.7793 0.3459090
393.2614 0.8976820
393.7436 1.711639
394.2257 1.282120
394.7078 1.216072
395.1899 3.215500
395.6720 3.554848
396.1541 2.934631
396.6363 2.442451
397.1184 1.944672
397.6005 2.026222
398.0826 3.108047
398.5647 5.332947
399.0468 7.171227
399.5290 7.673195
400.0111 8.183197
400.4932 9.761162
400.9753 12.45189
401.4574 16.19643
401.9395 21.34278
402.4217 27.60426
402.9038 33.65555
403.3859 40.01878
403.8680 45.40781
404.3501 48.93336
404.8322 49.76903
405.3144 51.55541
405.7965 54.46651
406.2786 58.09218
406.7607 61.69908
407.2428 65.17613
407.7249 69.23192
408.2071 73.89990
408.6892 79.38378
409.1713 86.12708
409.6534 94.09664
410.1355 103.3979
410.6176 113.2518
411.0998 124.1291
411.5819 138.7860
412.0640 158.2108
412.5461 180.9397
413.0282 204.8560
413.5103 230.1206
413.9925 258.0828
414.4746 287.0601
414.9567 320.3824
415.4388 362.9871
415.9209 415.8852
416.4030 475.6703
416.8852 562.1897
417.3673 650.4702
417.8494 700.4061
418.3315 693.3015
418.8136 646.3331
419.2957 550.5430
419.7779 415.1944
420.2600 293.8365
420.7421 210.7861
421.2242 151.7050
421.7063 109.3795
422.1884 86.63034
422.6706 70.47806
423.1527 59.38725
423.6348 52.43802
424.1169 47.78996
424.5990 46.12875
425.0811 45.74123
425.5633 46.23630
426.0454 47.62073
426.5275 49.67363
427.0096 52.49359
427.4917 55.92570
427.9738 59.90251
428.4560 64.64966
428.9381 69.56561
429.4202 75.23540
429.9023 80.86170
430.3844 84.01511
430.8665 84.78207
431.3487 82.70157
431.8308 76.87914
432.3129 67.16821
432.7950 57.22740
433.2771 46.76031
433.7592 37.05608
434.2414 29.73584
434.7235 24.69447
435.2056 20.71687
435.6877 17.59346
436.1698 15.18623
436.6519 13.22114
437.1341 11.69695
437.6162 10.52666
438.0983 9.804344
438.5804 9.369370
439.0625 8.821281
439.5446 7.967506
440.0268 7.287521
440.5089 7.423645
440.9910 8.087433
441.4731 8.678505
441.9552 8.776108
442.4373 8.837090
442.9195 9.099182
443.4016 9.576439
443.8837 10.29512
444.3658 11.54132
444.8479 12.88319
445.3300 14.04989
445.8122 13.90740
446.2943 14.82478
446.7764 17.71856
447.2585 21.93382
447.7406 25.84582
448.2227 30.00138
448.7049 33.21223
449.1870 35.41976
449.6691 36.85007
450.1512 35.68230
450.6333 30.81812
451.1154 24.56726
451.5976 18.91194
452.0797 13.85481
452.5618 9.938148
453.0439 7.348595
453.5260 5.843987
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454.4903 3.404182
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457.3830 0.7095490
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459.3114 1.298393
459.7935 1.993408
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460.7578 1.203697
461.2399 0.6807560
461.7220 1.076202
462.2041 1.761780
462.6862 2.116089
463.1684 1.986671
463.6505 1.855705
464.1326 2.293419
464.6147 2.727470
465.0968 2.475845
465.5789 6.9159999E-02
466.0611 1.602280
466.5432 1.281204
467.0253 0.8484730
467.5074 2.552948
467.9895 3.850113
468.4716 4.447601
468.9538 4.064423
469.4359 1.826248
469.9180 0.5681380
470.4001 0.6840290
470.8822 1.495369
471.3643 2.069221
471.8465 2.477524
472.3286 2.392265
472.8107 1.446869
473.2928 8.2999997E-02
473.7749 0.4514620
474.2570 0.5532000
474.7392 1.619286
475.2213 1.517174
475.7034 0.4795070
476.1855 0.2352520
476.6676 1.119560
477.1497 2.293427
477.6319 2.486633
478.1140 1.992218
478.5961 1.762886
479.0782 2.638863
479.5603 3.733963
480.0424 3.916443
480.5246 3.282478
481.0067 2.616341
481.4888 2.416023
481.9709 2.399857
482.4530 2.314034
482.9352 2.056671
483.4173 1.848244
483.8994 1.782654
484.3815 1.818207
484.8636 1.892624
485.3457 2.336731
485.8279 2.464348
486.3100 1.845947
486.7921 0.4819950
487.2742 0.2790680
487.7563 0.1679530
488.2384 0.2668530
488.7206 0.7837830
489.2027 1.550606
489.6848 1.958969
490.1669 1.854988
490.6490 1.469940
491.1311 1.105453
491.6133 0.7242430
492.0954 0.6694720
492.5775 1.204330
493.0596 2.104851
493.5417 2.580750
494.0238 2.629921
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