#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 10:52:28 +0300 (Thu, 07 Jun 2018) $
#$Revision: 980 $
#$URL: svn://172.16.1.111/rod/cif/8/10/00/8100032.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_8100032
loop_
_publ_author_name
'Chevrier, G.'
'Giester, G.'
'Heger, G.'
'Jarosch, D.'
'Wildner, M.'
'Zemann, J.'
_publ_section_title
;
 Neutron single-crystal refinement of cerussite, PbCO3, and comparison
 with other aragonite-type carbonates Locality: Pribram, Czech Republic
;
_journal_name_full               'Zeitschrift fur Kristallographie'
_journal_page_first              67
_journal_page_last               74
_journal_volume                  199
_journal_year                    1992
_chemical_compound_source        R050174
_chemical_formula_sum            'C O3 Pb'
_chemical_name_mineral           Cerussite
_space_group_IT_number           62
_symmetry_space_group_name_Hall  '-P 2n 2a'
_symmetry_space_group_name_H-M   'P m c n'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   5.179
_cell_length_b                   8.492
_cell_length_c                   6.141
_cell_volume                     270.082
_exptl_crystal_density_diffrn    6.572
_cod_original_formula_sum        'Pb C O3'
_cod_database_code               9008411
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R050174.rod
_rod_data_source.block           3500000
_rod_database.code               8100032
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9008411 COD http://www.crystallography.net/cod/9008411.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
140.5407 0.0000000E+00
141.0228 28.95215
141.5049 9.572266
141.9870 5.152344
142.4692 36.13770
142.9513 110.4775
143.4334 213.9092
143.9155 342.9941
144.3976 495.8164
144.8797 664.1211
145.3619 868.2334
145.8440 1115.023
146.3261 1397.433
146.8082 1665.098
147.2903 1905.722
147.7724 2147.114
148.2546 2409.866
148.7367 2708.578
149.2188 3003.199
149.7009 3294.545
150.1830 3581.366
150.6651 3834.505
151.1473 4051.771
151.6294 4236.455
152.1115 4388.784
152.5936 4541.262
153.0757 4628.824
153.5578 4637.164
154.0400 4567.693
154.5221 4463.682
155.0042 4315.516
155.4863 4133.861
155.9684 3929.081
156.4505 3695.130
156.9327 3441.361
157.4148 3155.611
157.8969 2833.884
158.3790 2541.579
158.8611 2288.557
159.3432 2069.454
159.8254 1876.632
160.3075 1712.908
160.7896 1571.127
161.2717 1445.132
161.7538 1331.271
162.2359 1251.557
162.7181 1221.725
163.2002 1228.848
163.6823 1255.011
164.1644 1297.820
164.6465 1355.058
165.1286 1421.213
165.6108 1492.923
166.0929 1597.852
166.5750 1776.035
167.0571 2028.152
167.5392 2294.317
168.0213 2561.326
168.5035 2830.823
168.9856 3090.457
169.4677 3337.813
169.9498 3569.652
170.4319 3796.084
170.9140 4025.843
171.3962 4245.289
171.8783 4453.281
172.3604 4644.118
172.8425 4811.675
173.3246 4952.412
173.8067 5076.775
174.2889 5203.508
174.7710 5325.069
175.2531 5414.898
175.7352 5455.409
176.2173 5454.886
176.6994 5423.417
177.1816 5361.490
177.6637 5271.189
178.1458 5151.416
178.6279 5002.673
179.1100 4835.563
179.5921 4657.818
180.0743 4463.876
180.5564 4244.370
181.0385 3988.031
181.5206 3714.031
182.0027 3446.979
182.4848 3187.190
182.9670 2939.783
183.4491 2711.901
183.9312 2496.780
184.4133 2279.979
184.8954 2052.185
185.3775 1824.614
185.8597 1607.502
186.3418 1402.101
186.8239 1213.881
187.3060 1053.520
187.7881 915.0850
188.2702 781.3271
188.7523 644.7422
189.2345 510.6191
189.7166 387.8721
190.1987 274.9365
190.6808 177.4102
191.1629 106.9531
191.6451 60.30273
192.1272 8.638672
192.6093 62.89844
193.0914 141.5479
193.5735 185.1963
194.0556 191.4277
194.5378 184.8418
195.0199 190.2998
195.5020 207.0498
195.9841 214.0498
196.4662 204.2949
196.9483 180.8613
197.4305 156.7969
197.9126 132.5068
198.3947 102.4072
198.8768 63.17578
199.3589 14.25293
199.8410 35.21484
200.3232 81.44141
200.8053 125.2266
201.2874 173.1709
201.7695 225.2578
202.2516 280.9805
202.7337 339.0830
203.2159 398.9517
203.6980 466.0981
204.1801 544.6050
204.6622 632.7954
205.1443 712.8911
205.6264 782.2969
206.1086 850.5068
206.5907 928.6104
207.0728 1018.134
207.5549 1107.035
208.0370 1193.664
208.5191 1278.664
209.0013 1358.434
209.4834 1428.731
209.9655 1499.824
210.4476 1585.521
210.9297 1690.277
211.4118 1791.203
211.8940 1885.950
212.3761 1974.733
212.8582 2048.877
213.3403 2107.659
213.8224 2151.392
214.3045 2180.425
214.7867 2193.509
215.2688 2199.040
215.7509 2197.456
216.2330 2188.336
216.7151 2171.726
217.1972 2148.618
217.6794 2117.549
218.1615 2075.624
218.6436 2017.356
219.1257 1959.978
219.6078 1909.966
220.0899 1866.505
220.5721 1817.591
221.0542 1760.877
221.5363 1702.709
222.0184 1650.962
222.5005 1606.128
222.9826 1564.102
223.4648 1525.899
223.9469 1490.692
224.4290 1457.173
224.9111 1421.493
225.3932 1390.781
225.8753 1372.893
226.3575 1376.256
226.8396 1375.141
227.3217 1363.467
227.8038 1340.596
228.2859 1323.833
228.7680 1313.664
229.2502 1309.298
229.7323 1311.331
230.2144 1322.924
230.6965 1333.579
231.1786 1340.746
231.6607 1344.497
232.1429 1350.776
232.6250 1358.767
233.1071 1370.251
233.5892 1387.444
234.0713 1412.480
234.5534 1438.716
235.0356 1463.780
235.5177 1487.948
235.9998 1520.174
236.4819 1565.622
236.9640 1613.408
237.4461 1653.511
237.9283 1679.564
238.4104 1710.545
238.8925 1751.449
239.3746 1801.618
239.8567 1846.207
240.3388 1884.521
240.8210 1918.079
241.3031 1947.928
241.7852 1973.732
242.2673 1996.657
242.7494 2018.237
243.2315 2037.793
243.7137 2048.243
244.1958 2047.890
244.6779 2040.579
245.1600 2029.317
245.6421 2016.178
246.1242 1994.867
246.6064 1964.503
247.0885 1925.353
247.5706 1878.317
248.0527 1821.382
248.5348 1759.415
249.0169 1696.413
249.4990 1630.827
249.9812 1564.801
250.4633 1498.106
250.9454 1428.562
251.4275 1348.896
251.9096 1258.438
252.3917 1166.577
252.8739 1078.535
253.3560 993.6665
253.8381 910.5552
254.3202 829.1328
254.8023 751.0596
255.2844 681.5566
255.7666 623.9102
256.2487 569.8145
256.7308 515.3848
257.2129 457.2446
257.6950 408.8140
258.1772 370.9658
258.6593 340.2627
259.1414 307.5259
259.6235 270.7930
260.1056 235.0176
260.5877 200.7324
261.0699 167.4004
261.5520 139.4272
262.0341 118.2305
262.5162 101.2915
262.9983 81.23975
263.4804 55.19629
263.9626 33.05078
264.4447 20.86621
264.9268 22.15234
265.4089 15.70703
265.8910 2.375488
266.3731 24.68066
266.8553 39.22852
267.3374 44.23193
267.8195 45.49976
268.3016 43.40942
268.7837 37.46509
269.2658 35.11035
269.7480 38.29150
270.2301 42.40137
270.7122 38.98877
271.1943 25.04053
271.6764 14.97778
272.1585 15.67944
272.6407 27.21216
273.1228 29.22119
273.6049 18.65942
274.0870 4.114014
274.5691 3.975586
275.0512 4.385254
275.5334 4.381104
276.0155 5.696045
276.4976 8.240234
276.9797 11.77563
277.4618 16.87769
277.9439 21.28345
278.4261 21.61401
278.9081 17.30200
279.3903 15.97192
279.8724 20.75024
280.3545 29.95557
280.8366 34.31592
281.3187 32.75171
281.8008 31.30420
282.2830 35.32007
282.7651 44.90283
283.2472 55.96411
283.7293 68.68433
284.2114 81.81396
284.6935 92.10156
285.1757 99.54858
285.6578 103.8813
286.1399 101.8467
286.6220 94.34546
287.1041 94.47998
287.5862 105.5999
288.0684 122.6072
288.5505 136.1018
289.0326 146.0754
289.5147 152.9363
289.9968 154.8064
290.4789 152.8818
290.9611 154.9028
291.4432 162.1375
291.9253 171.5232
292.4074 178.8560
292.8895 184.1763
293.3716 188.2629
293.8538 189.8191
294.3359 190.2817
294.8180 195.6445
295.3001 207.2727
295.7822 218.5378
296.2643 219.1714
296.7465 211.5129
297.2286 206.0686
297.7107 208.1641
298.1928 215.4043
298.6749 223.3516
299.1570 232.0249
299.6392 240.8345
300.1213 250.8433
300.6034 260.7275
301.0855 266.8933
301.5676 266.2778
302.0497 262.3110
302.5319 258.8379
303.0140 255.8687
303.4961 255.4553
303.9782 261.2532
304.4603 270.3218
304.9424 277.2778
305.4246 279.3379
305.9067 280.1387
306.3888 283.8113
306.8709 289.8381
307.3530 295.6587
307.8351 300.1416
308.3173 303.2771
308.7994 304.2766
309.2815 300.8452
309.7636 299.6921
310.2457 309.5964
310.7278 326.5320
311.2100 339.5540
311.6921 340.8352
312.1742 336.8845
312.6563 332.3596
313.1384 326.9453
313.6205 324.1104
314.1027 327.4641
314.5848 334.5649
315.0669 341.1133
315.5490 345.0496
316.0311 348.1157
316.5132 351.8376
316.9954 356.6047
317.4775 359.3647
317.9596 357.6145
318.4417 353.4358
318.9238 349.1453
319.4059 342.1189
319.8881 338.2754
320.3702 342.6204
320.8523 354.6504
321.3344 362.0916
321.8165 356.9741
322.2986 348.2820
322.7808 343.1482
323.2629 344.7339
323.7450 346.6650
324.2271 350.4658
324.7092 354.9622
325.1913 352.5034
325.6735 335.9106
326.1556 317.1536
326.6377 302.3264
327.1198 292.5559
327.6019 284.9426
328.0840 279.9006
328.5662 277.4282
329.0483 276.9351
329.5304 280.2852
330.0125 282.6387
330.4946 281.6406
330.9767 276.3389
331.4589 273.6118
331.9410 277.6079
332.4231 282.1589
332.9052 278.0381
333.3873 256.5483
333.8694 239.5029
334.3516 233.7170
334.8337 240.2253
335.3158 243.1191
335.7979 240.9705
336.2800 236.4236
336.7621 231.5991
337.2443 225.8713
337.7264 222.0437
338.2085 221.0583
338.6906 222.3416
339.1727 223.4343
339.6548 225.0039
340.1370 224.9326
340.6191 220.3342
341.1012 210.0962
341.5833 205.1807
342.0654 208.0398
342.5475 215.1133
343.0297 219.2034
343.5118 220.3210
343.9939 217.9155
344.4760 209.1489
344.9581 194.9880
345.4402 187.5515
345.9224 188.6304
346.4045 192.1047
346.8866 187.9685
347.3687 176.9141
347.8508 168.7395
348.3329 168.9834
348.8151 174.6882
349.2972 177.4788
349.7793 177.2661
350.2614 175.9971
350.7435 174.4702
351.2256 173.2480
351.7078 174.5056
352.1899 181.2456
352.6720 188.0002
353.1541 186.2634
353.6362 177.0657
354.1183 166.5906
354.6005 156.6868
355.0826 148.8713
355.5647 145.8970
356.0468 149.5425
356.5289 154.7317
357.0110 158.2861
357.4932 159.9683
357.9753 159.3938
358.4574 154.2686
358.9395 148.0969
359.4216 143.4214
359.9037 140.4502
360.3859 139.0510
360.8680 140.4497
361.3501 142.9268
361.8322 144.4944
362.3143 144.4258
362.7964 143.3171
363.2786 142.0334
363.7607 140.3418
364.2428 135.8877
364.7249 124.2312
365.2070 111.7712
365.6891 102.9746
366.1713 102.2688
366.6534 101.2651
367.1355 96.16724
367.6176 88.44336
368.0997 84.69531
368.5818 89.74805
369.0640 95.94897
369.5461 100.8733
370.0282 105.4209
370.5103 106.3975
370.9924 102.3657
371.4745 95.40430
371.9567 87.83960
372.4388 75.63452
372.9209 69.26270
373.4030 73.42627
373.8851 88.50220
374.3672 95.93726
374.8494 92.88110
375.3315 86.16602
375.8136 81.14111
376.2957 78.11353
376.7778 75.46606
377.2599 73.14331
377.7421 70.88696
378.2242 67.85938
378.7063 63.92139
379.1884 59.72461
379.6705 54.34229
380.1526 47.68726
380.6348 47.04150
381.1169 53.98560
381.5990 63.37939
382.0811 68.74927
382.5632 70.10791
383.0453 67.80103
383.5275 59.66431
384.0096 48.40942
384.4917 42.41553
384.9738 41.92944
385.4559 42.95435
385.9380 42.26660
386.4202 40.20557
386.9023 37.87915
387.3844 36.04297
387.8665 33.61890
388.3486 27.86694
388.8307 19.67700
389.3129 12.92432
389.7950 7.307373
390.2771 5.048828
390.7592 10.76489
391.2413 27.31299
391.7234 40.95874
392.2056 37.02124
392.6877 24.01929
393.1698 15.48804
393.6519 22.33594
394.1340 30.14307
394.6161 30.97974
395.0983 24.90552
395.5804 18.52686
396.0625 12.92627
396.5446 8.606934
397.0267 6.050293
397.5089 7.939697
397.9910 8.506592
398.4731 4.647705
398.9552 1.601807
399.4373 4.038086
399.9194 0.9184570
400.4016 7.907227
400.8837 15.46167
401.3658 25.51636
401.8479 29.44214
402.3300 24.05566
402.8121 14.80811
403.2942 7.617188
403.7763 1.640381
404.2585 0.4223630
404.7406 4.004883
405.2227 13.85034
405.7048 16.91602
406.1869 10.77393
406.6690 3.411377
407.1512 0.6506350
407.6333 3.031738
408.1154 5.508301
408.5975 7.828369
409.0796 9.812500
409.5617 10.87793
410.0439 11.08594
410.5260 10.97021
411.0081 10.73291
411.4902 10.25830
411.9723 9.338623
412.4544 7.942871
412.9366 6.026123
413.4187 1.278564
413.9008 4.267822
414.3829 4.071533
414.8650 7.307861
415.3471 21.01953
415.8293 25.80737
416.3114 22.77368
416.7935 16.86719
417.2756 7.097656
417.7577 1.852539
418.2398 3.540771
418.7220 4.837891
419.2041 12.41992
419.6862 11.31250
420.1683 5.500488
420.6504 1.118164
421.1325 0.9438480
421.6147 2.166016
422.0968 5.639160
422.5789 11.01514
423.0610 10.90918
423.5431 5.150635
424.0252 21.81909
424.5074 29.16138
424.9895 15.86548
425.4716 6.159180
425.9537 3.220947
426.4358 4.785889
426.9179 5.910645
427.4001 7.141846
427.8822 7.368164
428.3643 5.880371
428.8464 2.257324
429.3285 0.3930660
429.8106 1.257080
430.2928 2.628906
430.7749 2.597656
431.2570 1.355225
431.7391 3.028320
432.2212 12.68237
432.7033 24.60449
433.1855 28.36743
433.6676 23.16846
434.1497 16.86279
434.6318 14.28540
435.1139 14.81177
435.5960 14.88550
436.0782 14.45239
436.5603 13.04712
437.0424 8.435059
437.5245 2.005615
438.0066 1.222900
438.4887 3.025635
438.9709 9.607422
439.4530 11.68604
439.9351 9.653076
440.4172 6.267578
440.8993 2.752441
441.3814 0.8735350
441.8636 5.012695
442.3457 10.46533
442.8278 14.05103
443.3099 15.05762
443.7920 12.80225
444.2741 6.155273
444.7563 16.14600
445.2384 32.79028
445.7205 30.72021
446.2026 9.602051
446.6847 4.018311
447.1668 4.710693
447.6490 16.31689
448.1311 18.56055
448.6132 1.473145
449.0953 14.60303
449.5774 18.41724
450.0595 15.82178
450.5417 12.40088
451.0238 6.946289
451.5059 2.826904
451.9880 1.781494
452.4701 4.072266
452.9522 3.597656
453.4344 0.5788570
453.9165 5.336914
454.3986 7.643311
454.8807 7.379150
455.3628 7.787598
455.8449 10.21313
456.3271 12.29980
456.8092 7.303223
457.2913 4.132813
457.7734 12.79980
458.2555 11.13330
458.7376 3.744629
459.2198 1.627441
459.7019 5.451416
460.1840 8.845947
460.6661 4.755859
461.1482 3.255371
461.6303 9.237305
462.1125 10.29956
462.5946 10.42334
463.0767 12.63745
463.5588 16.24121
464.0409 19.22363
464.5230 21.79224
465.0052 22.57349
465.4873 19.42749
465.9694 10.91187
466.4515 5.961670
466.9336 10.54590
467.4157 17.87915
467.8979 21.56299
468.3800 14.89258
468.8621 11.66235
469.3442 14.92749
469.8263 22.84497
470.3084 28.09253
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1305.334 0.0000000E+00
