#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 11:16:36 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1052 $
#$URL: svn://172.16.1.111/rod/cif/8/10/00/8100037.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_8100037
loop_
_publ_author_name
'Chevrier, G.'
'Giester, G.'
'Heger, G.'
'Jarosch, D.'
'Wildner, M.'
'Zemann, J.'
_publ_section_title
;
 Neutron single-crystal refinement of cerussite, PbCO3, and comparison
 with other aragonite-type carbonates Locality: Pribram, Czech Republic
;
_journal_name_full               'Zeitschrift fur Kristallographie'
_journal_page_first              67
_journal_page_last               74
_journal_volume                  199
_journal_year                    1992
_chemical_compound_source        R060017
_chemical_formula_sum            'C O3 Pb'
_chemical_name_mineral           Cerussite
_space_group_IT_number           62
_symmetry_space_group_name_Hall  '-P 2n 2a'
_symmetry_space_group_name_H-M   'P m c n'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   5.179
_cell_length_b                   8.492
_cell_length_c                   6.141
_cell_volume                     270.082
_exptl_crystal_density_diffrn    6.572
_cod_original_formula_sum        'Pb C O3'
_cod_database_code               9008411
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060017.rod
_rod_data_source.block           3500000
_rod_database.code               8100037
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9008411 COD http://www.crystallography.net/cod/9008411.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
112.6909 0.0000000E+00
113.1730 0.2996830
113.6551 2.291504
114.1373 0.9755860
114.6194 8.961060
115.1015 22.14148
115.5836 45.35474
116.0657 66.72388
116.5478 80.71118
117.0300 86.63416
117.5121 90.96143
117.9942 95.30737
118.4763 99.22339
118.9584 102.1655
119.4405 101.3372
119.9227 101.1157
120.4048 103.8469
120.8869 109.6914
121.3690 118.5713
121.8511 131.8252
122.3332 148.0825
122.8154 164.5422
123.2975 177.0525
123.7796 190.1304
124.2617 208.4092
124.7438 232.2344
125.2259 261.5474
125.7081 298.7610
126.1902 341.1794
126.6723 371.2029
127.1544 386.2642
127.6365 399.0115
128.1186 416.3364
128.6008 441.6172
129.0829 469.3169
129.5650 490.7468
130.0471 506.2654
130.5292 520.6467
131.0113 539.7102
131.4935 561.6218
131.9756 578.4482
132.4577 586.7356
132.9398 589.2617
133.4219 592.8237
133.9040 597.3325
134.3862 602.3296
134.8683 607.7310
135.3504 613.4893
135.8325 617.6697
136.3146 617.6497
136.7967 614.4221
137.2789 618.9539
137.7610 632.5105
138.2431 650.5520
138.7252 667.1602
139.2073 681.8792
139.6894 697.5535
140.1716 714.4897
140.6537 732.2800
141.1358 755.9702
141.6179 787.7397
142.1000 823.6014
142.5821 855.5575
143.0643 882.5824
143.5464 908.6187
144.0285 935.9429
144.5106 966.1191
144.9927 993.0344
145.4748 1015.164
145.9570 1034.192
146.4391 1054.222
146.9212 1077.396
147.4033 1099.192
147.8854 1117.922
148.3675 1134.684
148.8497 1146.589
149.3318 1154.690
149.8139 1158.272
150.2960 1153.109
150.7781 1135.335
151.2602 1112.319
151.7424 1089.840
152.2245 1068.860
152.7066 1044.271
153.1887 1014.241
153.6708 978.4307
154.1529 940.2609
154.6351 897.2190
155.1172 852.6292
155.5993 808.9819
156.0814 762.9927
156.5635 716.1892
157.0456 667.3353
157.5278 616.9722
158.0099 574.2678
158.4920 545.3995
158.9741 522.6521
159.4562 499.0140
159.9383 469.1570
160.4205 441.5544
160.9026 418.6521
161.3847 400.5969
161.8668 386.9946
162.3489 379.7852
162.8310 376.3210
163.3132 373.5101
163.7953 368.1060
164.2774 364.7430
164.7595 366.0752
165.2416 372.6237
165.7237 381.2996
166.2059 391.7407
166.6880 403.1382
167.1701 414.2729
167.6522 423.5312
168.1343 432.9934
168.6164 444.3984
169.0986 458.3086
169.5807 472.5210
170.0628 485.8734
170.5449 496.9264
171.0270 507.6243
171.5091 518.8018
171.9913 529.4360
172.4734 538.4054
172.9555 545.3743
173.4376 551.4097
173.9197 560.0825
174.4018 569.1161
174.8840 572.1091
175.3661 560.8496
175.8482 542.9016
176.3303 528.6045
176.8124 520.8069
177.2945 513.6497
177.7767 501.2910
178.2588 484.1093
178.7409 464.3931
179.2230 442.4703
179.7051 418.8464
180.1872 395.0798
180.6694 371.6908
181.1515 347.2496
181.6336 318.7478
182.1157 286.8254
182.5978 256.1853
183.0799 230.0107
183.5621 207.3025
184.0442 186.1124
184.5263 166.2314
185.0084 147.0819
185.4905 126.5880
185.9726 104.9420
186.4547 84.42773
186.9369 67.00012
187.4190 52.14209
187.9011 38.71729
188.3832 26.62122
188.8653 15.47131
189.3474 3.783203
189.8296 8.638916
190.3117 19.54883
190.7938 26.60071
191.2759 30.17114
191.7580 33.27747
192.2401 36.92786
192.7223 40.43469
193.2044 41.62952
193.6865 40.39429
194.1686 38.18567
194.6507 36.49365
195.1328 35.27563
195.6150 32.86182
196.0971 28.03064
196.5792 21.92212
197.0613 20.11670
197.5434 23.64343
198.0255 26.66699
198.5077 22.26624
198.9898 10.10327
199.4719 0.7021480
199.9540 7.401245
200.4361 10.89282
200.9182 17.02612
201.4004 26.63354
201.8825 36.65564
202.3646 43.74829
202.8467 47.53491
203.3288 50.98779
203.8109 54.17041
204.2931 57.47644
204.7752 64.43555
205.2573 75.84644
205.7394 88.43774
206.2215 98.82764
206.7036 106.5242
207.1858 115.8330
207.6679 127.8860
208.1500 142.0050
208.6321 154.3325
209.1142 165.0544
209.5963 174.8634
210.0785 184.0444
210.5606 192.1559
211.0427 199.9161
211.5248 207.3906
212.0069 214.7101
212.4890 223.5344
212.9712 234.5792
213.4533 245.8934
213.9354 255.6288
214.4175 264.2418
214.8996 270.0006
215.3817 271.8578
215.8639 269.8730
216.3460 269.2135
216.8281 270.5958
217.3102 272.1677
217.7923 271.4855
218.2744 266.9003
218.7566 264.5311
219.2387 266.3124
219.7208 272.2019
220.2029 277.3790
220.6850 282.3235
221.1671 286.0437
221.6493 286.8071
222.1314 282.3871
222.6135 280.3113
223.0956 283.0891
223.5777 290.9380
224.0598 296.7830
224.5420 300.7698
225.0241 302.6399
225.5062 301.7765
225.9883 296.8243
226.4704 292.2080
226.9525 289.4878
227.4347 288.7510
227.9168 285.3827
228.3989 277.7162
228.8810 269.2109
229.3631 263.8947
229.8452 263.7721
230.3274 262.7067
230.8095 259.5027
231.2916 254.1235
231.7737 247.3002
232.2558 237.5109
232.7379 227.9252
233.2201 222.0963
233.7022 221.9803
234.1843 221.7601
234.6664 220.2966
235.1485 217.6138
235.6306 214.9703
236.1128 211.9869
236.5949 209.3580
237.0770 207.8574
237.5591 208.3444
238.0412 208.2899
238.5233 206.9886
239.0055 204.4320
239.4876 202.9658
239.9697 203.5836
240.4518 204.1172
240.9339 202.4904
241.4160 197.3418
241.8982 192.8085
242.3803 189.7288
242.8624 188.0426
243.3445 186.3381
243.8266 184.4595
244.3087 182.6552
244.7909 181.3308
245.2730 181.4607
245.7551 180.0929
246.2372 176.5712
246.7193 171.0002
247.2014 164.8914
247.6836 157.6295
248.1657 149.5813
248.6478 141.2308
249.1299 132.1952
249.6120 124.1641
250.0941 117.9292
250.5762 113.0956
251.0584 106.5061
251.5405 97.75439
252.0226 88.25098
252.5047 78.86377
252.9868 69.06543
253.4689 60.56763
253.9511 53.79846
254.4332 48.64673
254.9153 44.37488
255.3974 41.79382
255.8795 38.29614
256.3617 32.07617
256.8438 21.14941
257.3259 14.12463
257.8080 12.72253
258.2901 15.19727
258.7722 15.02393
259.2544 10.75427
259.7365 6.147095
260.2186 3.228149
260.7007 2.606812
261.1828 1.877319
261.6649 0.5450440
262.1471 0.8840330
262.6292 0.4788820
263.1113 3.189819
263.5934 5.692383
264.0755 3.846924
264.5576 4.782715
265.0398 8.658569
265.5219 5.538208
266.0040 1.208496
266.4861 3.368530
266.9682 0.8703610
267.4503 5.242432
267.9325 6.499268
268.4146 3.765015
268.8967 2.115845
269.3788 1.944092
269.8609 2.450684
270.3430 2.150146
270.8252 0.9255370
271.3073 0.7514650
271.7894 3.027954
272.2715 6.088257
272.7536 7.596558
273.2357 7.031738
273.7179 5.646973
274.2000 5.567993
274.6821 7.235474
275.1642 8.132446
275.6463 6.743286
276.1284 3.050293
276.6106 1.850464
277.0927 3.709961
277.5748 6.859253
278.0569 9.372559
278.5390 11.29138
279.0211 12.16895
279.5032 11.24915
279.9854 8.933472
280.4675 8.754883
280.9496 10.95630
281.4317 14.45911
281.9138 18.95801
282.3959 24.58826
282.8781 27.98096
283.3602 27.65320
283.8423 24.49817
284.3244 22.27563
284.8065 21.02588
285.2886 20.31909
285.7708 19.72119
286.2529 19.24670
286.7350 19.31299
287.2171 19.98779
287.6992 21.25000
288.1813 23.53992
288.6635 26.95520
289.1456 29.62817
289.6277 29.29700
290.1098 26.50427
290.5919 25.04053
291.0740 25.67432
291.5562 27.61865
292.0383 29.64636
292.5204 31.74878
293.0025 33.49426
293.4846 34.93274
293.9667 35.86523
294.4489 35.43079
294.9310 33.36316
295.4131 30.44568
295.8952 27.02075
296.3773 23.38611
296.8594 21.24841
297.3416 22.66028
297.8237 26.15466
298.3058 28.33618
298.7879 28.88086
299.2700 28.63586
299.7521 27.86597
300.2343 26.96118
300.7164 27.22070
301.1985 30.68689
301.6806 35.23694
302.1627 37.28357
302.6448 36.60413
303.1270 35.06641
303.6091 33.66443
304.0912 32.68872
304.5733 32.65991
305.0554 34.77307
305.5375 37.41248
306.0197 38.65344
306.5018 38.55640
306.9839 38.23206
307.4660 38.23279
307.9481 38.59631
308.4302 39.44983
308.9124 41.98486
309.3945 43.93835
309.8766 42.32129
310.3587 37.91882
310.8408 34.94556
311.3229 37.43347
311.8051 41.96362
312.2872 44.95081
312.7693 45.00488
313.2514 44.40198
313.7335 44.69495
314.2156 45.42639
314.6978 45.26184
315.1799 41.19849
315.6620 37.48022
316.1441 37.80542
316.6262 44.42749
317.1083 50.24036
317.5905 52.14771
318.0726 51.22998
318.5547 49.41980
319.0368 45.43799
319.5189 42.16968
320.0010 41.52441
320.4832 44.40735
320.9653 46.89771
321.4474 48.58960
321.9295 48.74524
322.4116 46.26941
322.8937 36.38159
323.3759 29.28455
323.8580 29.86157
324.3401 38.39526
324.8222 43.49036
325.3043 40.97803
325.7864 35.95374
326.2686 32.44629
326.7507 31.66638
327.2328 31.24219
327.7149 31.01672
328.1970 30.98792
328.6791 30.84082
329.1613 30.73560
329.6434 30.41504
330.1255 29.72119
330.6076 27.95618
331.0897 26.56128
331.5718 25.53223
332.0540 24.91309
332.5361 24.86353
333.0182 26.24133
333.5003 26.94031
333.9824 25.63037
334.4645 20.83386
334.9467 19.25781
335.4288 22.80579
335.9109 28.25330
336.3930 29.82825
336.8751 25.39185
337.3572 22.10608
337.8394 22.81177
338.3215 27.83398
338.8036 29.91235
339.2857 28.15222
339.7678 25.05872
340.2499 23.27100
340.7321 22.95044
341.2142 22.83472
341.6963 22.69141
342.1784 22.51428
342.6605 22.16687
343.1426 21.58325
343.6248 21.14185
344.1069 21.27454
344.5890 21.93713
345.0711 22.44421
345.5532 22.89563
346.0353 23.06799
346.5175 21.91479
346.9996 19.40076
347.4817 17.77454
347.9638 19.43152
348.4459 23.36243
348.9280 25.71143
349.4102 26.02222
349.8923 25.52673
350.3744 26.11670
350.8565 27.34216
351.3386 27.47522
351.8207 24.42700
352.3029 20.19031
352.7850 18.43115
353.2671 19.24719
353.7492 20.13110
354.2313 18.12207
354.7134 14.67749
355.1956 12.53027
355.6777 13.18604
356.1598 14.97803
356.6419 17.13782
357.1240 19.40247
357.6061 20.34937
358.0883 17.74390
358.5704 14.07544
359.0525 11.82861
359.5346 11.83447
360.0167 12.72595
360.4988 14.19617
360.9810 16.00330
361.4631 17.48413
361.9452 18.36255
362.4273 18.77417
362.9094 18.84729
363.3915 18.67896
363.8737 17.67346
364.3558 13.84521
364.8379 9.643311
365.3200 7.959961
365.8021 12.62683
366.2842 16.76880
366.7664 18.34033
367.2485 17.28650
367.7306 15.64465
368.2127 12.30652
368.6948 9.314575
369.1769 8.031494
369.6591 11.31494
370.1412 12.88562
370.6233 11.58569
371.1054 8.233154
371.5875 5.887695
372.0696 4.419678
372.5518 4.126343
373.0339 5.493042
373.5160 9.833252
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374.4802 10.92126
374.9623 8.435425
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375.9266 6.910400
376.4087 7.410889
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377.3729 10.66003
377.8550 11.25330
378.3372 9.995483
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380.2656 13.12988
380.7477 12.70203
381.2299 11.21606
381.7120 11.54871
382.1941 13.81580
382.6762 15.72583
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383.6404 12.72961
384.1226 11.67371
384.6047 12.43164
385.0868 13.33728
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386.0510 8.717407
386.5331 5.526733
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387.4974 0.2576900
387.9795 0.6818850
388.4616 3.742065
388.9437 6.409790
389.4258 5.328613
389.9080 2.660767
390.3901 1.628174
390.8722 4.879395
391.3543 8.129150
391.8364 7.644897
392.3185 4.329590
392.8007 1.580811
393.2828 1.084717
393.7649 1.740723
394.2470 3.041016
394.7291 5.423340
395.2112 6.818970
395.6934 5.316040
396.1755 2.629517
396.6576 1.288208
397.1397 3.911011
397.6218 6.023560
398.1039 5.741455
398.5861 2.718506
399.0682 0.6544190
399.5503 0.3035890
400.0324 2.2826999E-02
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402.9251 4.762939
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404.3714 4.853027
404.8535 1.083008
405.3357 1.453735
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406.7820 2.933472
407.2641 3.505981
407.7462 3.912231
408.2284 4.134033
408.7105 4.091675
409.1926 3.277100
409.6747 1.611206
410.1568 0.1864010
410.6389 2.037476
411.1211 3.663452
411.6032 3.229004
412.0853 4.603480
412.5674 4.545166
413.0495 4.875610
413.5316 2.073242
414.0138 0.3494870
414.4959 0.5449220
414.9780 0.8626710
415.4601 3.799438
415.9422 8.466797
416.4243 11.54041
416.9065 8.765625
417.3886 3.016357
417.8707 1.432617
418.3528 3.495605
418.8349 3.439697
419.3170 5.446015
419.7992 5.167725
420.2813 9.767090
420.7634 12.19458
421.2455 13.19812
421.7276 13.07568
422.2097 11.26892
422.6919 9.798584
423.1740 10.08459
423.6561 10.84924
424.1382 10.09143
424.6203 4.507690
425.1024 0.3940430
425.5846 5.6519002E-02
426.0667 3.782104
426.5488 5.977417
427.0309 6.222656
427.5130 5.359985
427.9951 3.797485
428.4773 3.592166
428.9594 2.989241
429.4415 2.438721
429.9236 2.784302
430.4057 3.043823
430.8878 3.452515
431.3700 2.936035
431.8521 0.3972170
432.3342 4.172485
432.8163 6.460327
433.2984 6.155640
433.7805 4.683472
434.2627 2.932739
434.7448 1.074829
435.2269 1.183105
435.7090 5.020630
436.1911 9.847168
436.6732 9.230591
437.1554 3.801147
437.6375 1.292480
438.1196 2.738037
438.6017 1.606079
439.0838 1.151611
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