#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 11:26:13 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1088 $
#$URL: svn://172.16.1.111/rod/cif/8/10/00/8100042.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_8100042
loop_
_publ_author_name
'Chevrier, G.'
'Giester, G.'
'Heger, G.'
'Jarosch, D.'
'Wildner, M.'
'Zemann, J.'
_publ_section_title
;
 Neutron single-crystal refinement of cerussite, PbCO3, and comparison
 with other aragonite-type carbonates Locality: Pribram, Czech Republic
;
_journal_name_full               'Zeitschrift fur Kristallographie'
_journal_page_first              67
_journal_page_last               74
_journal_volume                  199
_journal_year                    1992
_chemical_compound_source        R050298
_chemical_formula_sum            'C O3 Pb'
_chemical_name_mineral           Cerussite
_space_group_IT_number           62
_symmetry_space_group_name_Hall  '-P 2n 2a'
_symmetry_space_group_name_H-M   'P m c n'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   5.179
_cell_length_b                   8.492
_cell_length_c                   6.141
_cell_volume                     270.082
_exptl_crystal_density_diffrn    6.572
_cod_original_formula_sum        'Pb C O3'
_cod_database_code               9008411
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R050298.rod
_rod_data_source.block           3500000
_rod_database.code               8100042
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9008411 COD http://www.crystallography.net/cod/9008411.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
114.7008 0.0000000E+00
115.1829 5.344971
115.6650 0.1594240
116.1471 2.640839
116.6293 10.72971
117.1114 16.19739
117.5935 16.73654
118.0756 15.30737
118.5577 18.59949
119.0398 16.93219
119.5220 12.35812
120.0041 11.78317
120.4862 13.06158
120.9683 11.24573
121.4504 4.560272
121.9325 2.211792
122.4147 5.453094
122.8968 5.042847
123.3789 2.688873
123.8610 3.408447
124.3431 10.15109
124.8252 13.88184
125.3074 12.06796
125.7895 8.340057
126.2716 10.84885
126.7537 23.50958
127.2358 35.65189
127.7179 44.06619
128.2001 49.98965
128.6822 54.97876
129.1643 59.74310
129.6464 64.38995
130.1285 70.07339
130.6106 78.06570
131.0928 85.98959
131.5749 92.18848
132.0570 97.68863
132.5391 105.3013
133.0212 118.1382
133.5033 138.0394
133.9855 149.7695
134.4676 150.6342
134.9497 147.4636
135.4318 141.3325
135.9139 133.4120
136.3960 128.0851
136.8782 130.8502
137.3603 143.4448
137.8424 156.9305
138.3245 175.0348
138.8066 192.1592
139.2887 199.3399
139.7709 192.6486
140.2530 183.5909
140.7351 187.3504
141.2172 202.4133
141.6993 219.8817
142.1814 235.3614
142.6636 249.9681
143.1457 268.5734
143.6278 295.1171
144.1099 322.5712
144.5920 345.6427
145.0741 364.1401
145.5563 379.9870
146.0384 393.4464
146.5205 403.8492
147.0026 417.3856
147.4847 436.8905
147.9668 458.8784
148.4490 482.7877
148.9311 508.1107
149.4132 533.1584
149.8953 555.7147
150.3774 577.1021
150.8595 592.6689
151.3417 601.5110
151.8238 606.0153
152.3059 607.4322
152.7880 606.3435
153.2701 603.3450
153.7522 600.0052
154.2344 603.7595
154.7165 597.7734
155.1986 577.4233
155.6807 548.1162
156.1628 514.4808
156.6449 478.1521
157.1271 441.8136
157.6092 417.5470
158.0913 412.5323
158.5734 408.6570
159.0555 400.9134
159.5376 390.4747
160.0198 380.4760
160.5019 372.6907
160.9840 366.6895
161.4661 360.4676
161.9482 352.8844
162.4303 346.2287
162.9125 341.4749
163.3946 338.6431
163.8767 338.7855
164.3588 344.0444
164.8409 352.4724
165.3230 360.8551
165.8052 368.9771
166.2873 376.5485
166.7694 381.5721
167.2515 381.9781
167.7336 387.2161
168.2157 408.3826
168.6979 435.0668
169.1800 454.2860
169.6621 457.6173
170.1442 452.0807
170.6263 458.1721
171.1084 483.3946
171.5906 509.0179
172.0727 532.5364
172.5548 551.7495
173.0369 563.7376
173.5190 565.5193
174.0011 558.6622
174.4833 555.6079
174.9654 563.1183
175.4475 567.7549
175.9296 567.3281
176.4117 561.8839
176.8938 552.1053
177.3760 538.4121
177.8581 520.7810
178.3402 499.7592
178.8223 468.7347
179.3044 441.1326
179.7865 424.9290
180.2687 417.0793
180.7508 407.9377
181.2329 388.6830
181.7150 357.8376
182.1971 333.2100
182.6792 320.2515
183.1614 308.0717
183.6435 288.9884
184.1256 263.3332
184.6077 238.4401
185.0898 221.3267
185.5719 212.7283
186.0540 202.2301
186.5362 188.2329
187.0183 173.0787
187.5004 158.6315
187.9825 145.0114
188.4646 132.5363
188.9467 121.7008
189.4289 112.3346
189.9110 103.7540
190.3931 96.01624
190.8752 88.93994
191.3573 81.85553
191.8394 74.23166
192.3216 68.04807
192.8037 65.77319
193.2858 66.10266
193.7679 66.21448
194.2500 63.92270
194.7321 60.35217
195.2143 59.57596
195.6964 64.12778
196.1785 67.59750
196.6606 65.53793
197.1427 59.88437
197.6248 54.93250
198.1070 53.98688
198.5891 56.55212
199.0712 57.48093
199.5533 54.43127
200.0354 52.31815
200.5175 53.89529
200.9997 57.95782
201.4818 61.51425
201.9639 61.60269
202.4460 58.02887
202.9281 58.06415
203.4102 66.61322
203.8924 74.54556
204.3745 78.65765
204.8566 79.72473
205.3387 80.24231
205.8208 82.35025
206.3029 86.19720
206.7851 90.57199
207.2672 95.80643
207.7493 100.9484
208.2314 105.7823
208.7135 110.3173
209.1956 115.0114
209.6778 119.7341
210.1599 124.0421
210.6420 128.4269
211.1241 134.4669
211.6062 139.6935
212.0883 141.6016
212.5705 140.7197
213.0526 140.5770
213.5347 145.0183
214.0168 154.9558
214.4989 160.6713
214.9810 161.5313
215.4632 158.8910
215.9453 151.8748
216.4274 141.2283
216.9095 131.7327
217.3916 127.7593
217.8737 128.9999
218.3559 127.5720
218.8380 122.5952
219.3201 116.2396
219.8022 109.0563
220.2843 100.9534
220.7664 94.85327
221.2486 94.52660
221.7307 98.55505
222.2128 100.8973
222.6949 100.2920
223.1770 97.88226
223.6591 94.00186
224.1413 88.18889
224.6234 83.82907
225.1055 85.63947
225.5876 90.64725
226.0697 93.30006
226.5518 90.87206
227.0340 85.82297
227.5161 81.68683
227.9982 78.60876
228.4803 76.05017
228.9624 74.10043
229.4445 72.38062
229.9267 70.20062
230.4088 66.66521
230.8909 63.14552
231.3730 62.86305
231.8551 67.48077
232.3372 71.02170
232.8194 69.79852
233.3015 66.60532
233.7836 64.43033
234.2657 64.26793
234.7478 66.10428
235.2299 70.37029
235.7121 78.66656
236.1942 86.28714
236.6763 92.32880
237.1584 96.89218
237.6405 99.73782
238.1227 100.5563
238.6048 100.3836
239.0869 102.1730
239.5690 108.2610
240.0511 112.1435
240.5332 111.2742
241.0154 108.5446
241.4975 106.9034
241.9796 107.6311
242.4617 109.6809
242.9438 110.3599
243.4259 108.3663
243.9081 106.9586
244.3902 107.7893
244.8723 108.7222
245.3544 107.5305
245.8365 103.3641
246.3186 97.37289
246.8007 91.93521
247.2829 85.54341
247.7650 82.34790
248.2471 86.42120
248.7292 91.57425
249.2113 91.49203
249.6934 84.17410
250.1756 73.14238
250.6577 65.27702
251.1398 63.60808
251.6219 61.01744
252.1040 56.68071
252.5861 51.93260
253.0683 48.29016
253.5504 46.13660
254.0325 44.16133
254.5146 40.01596
254.9967 30.60240
255.4788 25.04610
255.9610 27.44493
256.4431 31.33583
256.9252 30.55881
257.4073 23.81279
257.8894 14.88727
258.3716 8.705353
258.8537 6.144897
259.3358 4.835335
259.8179 6.239876
260.3000 7.994568
260.7821 7.695450
261.2643 5.014435
261.7464 1.971558
262.2285 0.9125370
262.7106 2.468208
263.1927 2.886734
263.6748 0.6556320
264.1570 1.810501
264.6391 1.740150
265.1212 0.9778060
265.6033 3.040497
266.0854 0.6948850
266.5675 6.255180
267.0497 10.13910
267.5318 8.023994
268.0139 4.680984
268.4960 4.134529
268.9781 6.511238
269.4602 9.036110
269.9424 9.496094
270.4245 8.171074
270.9066 7.681084
271.3887 9.050156
271.8708 10.53406
272.3529 10.41426
272.8351 8.844292
273.3172 7.976135
273.7993 10.09191
274.2814 13.56158
274.7635 13.40650
275.2456 6.223602
275.7278 0.9300460
276.2099 2.448929
276.6920 1.047943
277.1741 4.509270
277.6562 5.722443
278.1383 5.203896
278.6204 4.411728
279.1025 3.194054
279.5847 1.982300
280.0668 1.226349
280.5489 0.8176570
281.0310 1.8821999E-02
281.5131 2.024170
281.9952 4.078102
282.4774 4.481628
282.9595 2.947273
283.4416 1.484276
283.9237 1.419296
284.4058 2.472336
284.8879 3.408066
285.3701 3.769081
285.8522 4.166794
286.3343 5.502228
286.8164 7.714470
287.2985 9.391525
287.7806 9.020515
288.2628 7.431095
288.7449 7.702370
289.2270 11.37936
289.7091 14.88328
290.1912 14.63940
290.6733 11.61455
291.1555 9.214191
291.6376 9.812599
292.1197 12.09271
292.6018 12.60642
293.0839 10.32054
293.5660 8.388901
294.0482 9.025082
294.5303 11.42506
295.0124 14.41029
295.4945 18.50235
295.9766 22.37684
296.4587 23.22884
296.9409 20.23356
297.4230 17.07619
297.9051 15.89878
298.3872 15.57694
298.8693 14.75336
299.3514 12.78002
299.8336 10.61573
300.3157 9.538898
300.7978 9.673164
301.2799 10.15883
301.7620 10.39193
302.2441 10.99704
302.7263 12.80487
303.2084 16.15112
303.6905 19.70855
304.1726 22.36023
304.6547 24.09394
305.1368 24.75842
305.6190 23.46225
306.1011 21.71483
306.5832 20.53088
307.0653 19.99414
307.5474 19.99220
308.0295 20.56320
308.5117 21.67695
308.9938 23.07654
309.4759 25.95964
309.9580 27.49892
310.4401 24.88214
310.9222 19.16602
311.4044 14.36881
311.8865 13.43061
312.3686 15.61780
312.8507 17.79961
313.3328 20.13879
313.8149 22.07029
314.2971 23.46464
314.7792 24.30275
315.2613 24.42183
315.7434 23.18308
316.2255 21.52152
316.7076 21.80797
317.1898 24.84932
317.6719 27.62850
318.1540 28.87528
318.6361 29.13411
319.1182 28.74891
319.6003 27.62733
320.0825 26.41519
320.5646 26.09826
321.0467 26.81797
321.5288 27.49178
322.0109 27.56329
322.4930 27.53395
322.9752 28.05815
323.4573 29.16191
323.9394 29.78392
324.4215 28.05713
324.9036 24.20424
325.3857 21.53774
325.8679 20.91497
326.3500 21.37919
326.8321 22.49976
327.3142 24.08353
327.7963 25.35508
328.2784 25.93438
328.7606 25.81051
329.2427 24.84291
329.7248 22.32304
330.2069 20.28016
330.6890 20.34337
331.1711 21.71875
331.6533 22.70442
332.1354 22.89791
332.6175 22.23652
333.0996 19.69862
333.5817 13.85352
334.0638 10.38182
334.5460 15.73282
335.0281 23.61577
335.5102 26.71780
335.9923 22.08352
336.4744 15.02308
336.9565 11.64288
337.4387 12.14054
337.9208 13.15752
338.4029 14.09204
338.8850 14.71494
339.3671 14.62465
339.8492 13.67694
340.3314 12.99298
340.8135 13.92616
341.2956 16.02193
341.7777 16.73052
342.2598 14.86682
342.7419 12.66331
343.2241 12.03270
343.7062 12.74132
344.1883 13.76067
344.6704 15.23441
345.1525 16.56037
345.6346 16.00712
346.1168 12.80459
346.5989 9.905964
347.0810 10.23825
347.5631 12.31020
348.0452 13.58009
348.5273 12.97410
349.0095 11.65840
349.4916 10.90355
349.9737 10.73369
350.4558 10.77582
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351.4200 11.24262
351.9022 11.10516
352.3843 10.29705
352.8664 9.940510
353.3485 11.24194
353.8306 13.73732
354.3127 15.50212
354.7949 15.77078
355.2770 15.47704
355.7591 16.15864
356.2412 17.83406
356.7233 18.39459
357.2054 16.23717
357.6876 12.74899
358.1697 9.904982
358.6518 7.904572
359.1339 7.062355
359.6160 8.538330
360.0981 11.70868
360.5803 13.12071
361.0624 10.52351
361.5445 7.397655
362.0266 6.471714
362.5087 7.648180
362.9908 10.03229
363.4730 13.96815
363.9551 18.21198
364.4372 19.11679
364.9193 14.87074
365.4014 10.70271
365.8835 8.471294
366.3657 7.834070
366.8478 8.372061
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368.7762 11.45943
369.2584 10.17111
369.7405 8.656939
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370.7047 8.048218
371.1868 9.777521
371.6689 11.41309
372.1511 11.50552
372.6332 9.958515
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373.5974 8.612923
374.0795 8.507389
374.5616 8.549301
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376.9722 5.436192
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382.2755 8.932995
382.7576 10.48000
383.2397 8.516975
383.7219 3.968784
384.2040 8.7674998E-02
384.6861 0.4441410
385.1682 2.124981
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387.0967 5.405577
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388.0609 9.523449
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389.5073 6.202194
389.9894 4.363571
390.4715 2.776493
390.9536 0.7745610
391.4357 0.5294380
391.9178 9.1091000E-02
392.4000 2.010464
392.8821 4.671986
393.3642 7.189474
393.8463 9.616726
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394.8105 5.650864
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395.7748 1.380203
396.2569 2.439606
396.7390 2.970245
397.2211 1.710024
397.7032 0.4118100
398.1854 1.175192
398.6675 5.5500001E-02
399.1496 0.8593350
399.6317 0.5069120
400.1138 6.2999999E-05
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408.7919 1.063879
409.2740 1.122036
409.7561 2.578344
410.2383 3.717175
410.7204 2.890879
411.2025 0.8956170
411.6846 0.2223320
412.1667 1.768589
412.6488 3.959770
413.1310 4.745613
413.6131 4.180901
414.0952 3.980700
414.5773 5.103798
415.0594 6.268654
415.5415 6.130371
416.0237 4.731707
416.5058 3.091740
416.9879 1.696999
417.4700 0.6859470
417.9521 0.7452160
418.4342 3.222719
418.9164 4.944008
419.3985 4.608082
419.8806 3.119917
420.3627 1.737522
420.8448 0.8670330
421.3269 0.2394330
421.8091 0.6064320
422.2912 2.079008
422.7733 2.452148
423.2554 0.9101430
423.7375 0.9022220
424.2196 2.293436
424.7018 3.196684
425.1839 3.858002
425.6660 4.526966
426.1481 5.026703
426.6302 4.109451
427.1123 1.222836
427.5945 4.201843
428.0766 2.293047
428.5587 1.445311
429.0408 4.007526
429.5229 4.464878
430.0050 3.841545
430.4872 3.391560
430.9693 3.006491
431.4514 3.251936
431.9335 5.748207
432.4156 7.432121
432.8977 6.221895
433.3799 3.127644
433.8620 0.8622300
434.3441 1.491587
434.8262 3.805405
435.3083 4.020058
435.7904 1.122442
436.2726 1.092583
436.7547 0.6455230
437.2368 0.7588100
437.7189 1.722553
438.2010 1.978176
438.6831 1.996035
439.1653 2.145317
439.6474 2.394064
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