#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 11:27:00 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1100 $
#$URL: svn://172.16.1.111/rod/cif/8/10/00/8100045.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_8100045
loop_
_publ_author_name
'Chevrier, G.'
'Giester, G.'
'Heger, G.'
'Jarosch, D.'
'Wildner, M.'
'Zemann, J.'
_publ_section_title
;
 Neutron single-crystal refinement of cerussite, PbCO3, and comparison
 with other aragonite-type carbonates Locality: Pribram, Czech Republic
;
_journal_name_full               'Zeitschrift fur Kristallographie'
_journal_page_first              67
_journal_page_last               74
_journal_volume                  199
_journal_year                    1992
_chemical_compound_source        R060017
_chemical_formula_sum            'C O3 Pb'
_chemical_name_mineral           Cerussite
_space_group_IT_number           62
_symmetry_space_group_name_Hall  '-P 2n 2a'
_symmetry_space_group_name_H-M   'P m c n'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   5.179
_cell_length_b                   8.492
_cell_length_c                   6.141
_cell_volume                     270.082
_exptl_crystal_density_diffrn    6.572
_cod_original_formula_sum        'Pb C O3'
_cod_database_code               9008411
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060017.rod
_rod_data_source.block           3500000
_rod_database.code               8100045
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9008411 COD http://www.crystallography.net/cod/9008411.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
113.3126 0.0000000E+00
113.7947 7.026733
114.2769 20.96106
114.7590 39.13013
115.2411 59.00842
115.7232 78.68787
116.2053 98.45251
116.6874 119.3682
117.1696 136.8723
117.6517 149.1357
118.1338 157.4030
118.6159 161.8123
119.0980 164.9196
119.5801 174.8807
120.0623 179.9093
120.5444 169.6519
121.0265 150.4227
121.5086 125.1003
121.9907 98.65186
122.4728 72.42444
122.9550 48.02600
123.4371 28.57324
123.9192 15.96313
124.4013 7.838745
124.8834 0.4249270
125.3655 6.458740
125.8476 10.84082
126.3298 11.11145
126.8119 7.158569
127.2940 0.3927000
127.7761 10.05505
128.2582 22.72461
128.7404 37.33948
129.2225 53.85181
129.7046 71.55725
130.1867 89.51135
130.6688 108.2472
131.1509 126.1630
131.6331 143.5240
132.1152 160.0364
132.5973 175.3555
133.0794 189.3260
133.5615 202.3754
134.0436 215.7985
134.5258 229.0717
135.0079 243.0292
135.4900 257.6014
135.9721 272.8545
136.4542 288.8715
136.9363 305.6598
137.4185 323.3025
137.9006 342.5254
138.3827 363.0760
138.8648 385.0665
139.3469 408.9816
139.8290 434.5887
140.3112 460.8810
140.7933 486.8193
141.2754 512.7749
141.7575 540.6550
142.2396 572.4491
142.7217 605.3445
143.2039 635.8322
143.6860 663.3235
144.1681 690.4301
144.6502 719.6084
145.1323 749.9967
145.6144 779.9409
146.0966 809.8033
146.5787 838.7288
147.0608 864.2205
147.5429 885.8005
148.0250 903.6677
148.5071 918.6145
148.9893 930.7119
149.4714 940.4078
149.9535 948.4193
150.4356 954.9910
150.9177 956.3705
151.3998 950.4390
151.8820 940.4895
152.3641 927.9412
152.8462 912.7903
153.3283 894.1603
153.8104 871.0603
154.2925 842.1757
154.7747 811.8925
155.2568 778.5238
155.7389 743.1252
156.2210 706.3849
156.7031 669.2714
157.1852 632.5151
157.6673 597.3049
158.1495 563.7073
158.6316 533.2095
159.1137 505.3339
159.5958 480.6837
160.0779 460.0632
160.5600 443.5868
161.0422 430.4395
161.5243 419.2375
162.0064 409.6288
162.4885 402.2838
162.9706 397.3331
163.4527 394.7722
163.9349 394.7611
164.4170 397.6420
164.8991 402.8734
165.3812 409.1376
165.8633 416.3128
166.3454 424.5458
166.8276 433.8907
167.3097 444.3462
167.7918 456.1581
168.2739 470.3694
168.7560 485.3713
169.2381 499.2264
169.7203 511.5887
170.2024 523.2618
170.6845 535.2594
171.1666 550.0038
171.6487 563.8835
172.1308 577.6205
172.6130 589.5947
173.0951 598.1833
173.5772 602.7950
174.0593 604.4057
174.5414 604.8651
175.0235 605.1599
175.5057 601.8428
175.9878 594.3724
176.4699 583.6813
176.9520 570.2518
177.4341 554.2550
177.9162 535.9852
178.3984 516.0193
178.8805 493.6163
179.3626 470.2957
179.8447 446.0667
180.3268 420.9454
180.8089 394.6068
181.2911 366.9167
181.7732 338.1798
182.2553 309.6000
182.7374 279.7230
183.2195 251.0970
183.7016 224.5353
184.1838 200.0138
184.6659 177.3937
185.1480 156.6020
185.6301 137.3494
186.1122 118.7621
186.5943 99.50397
187.0765 82.09717
187.5586 67.79382
188.0407 56.28088
188.5228 46.39618
189.0049 37.67847
189.4870 30.03790
189.9692 22.10297
190.4513 12.60004
190.9334 3.837891
191.4155 2.652832
191.8976 6.879822
192.3797 9.896301
192.8619 11.95117
193.3440 13.23468
193.8261 14.37122
194.3082 15.50409
194.7903 16.39935
195.2724 16.97235
195.7546 17.31403
196.2367 16.69299
196.7188 13.91217
197.2009 9.957092
197.6830 5.987915
198.1651 2.295593
198.6473 1.181091
199.1294 4.314148
199.6115 6.634338
200.0936 9.888245
200.5757 14.96930
201.0578 21.31262
201.5400 28.40131
202.0221 36.19147
202.5042 44.41644
202.9863 52.29736
203.4684 59.39520
203.9505 66.85431
204.4327 75.42902
204.9148 84.44446
205.3969 92.84119
205.8790 99.82257
206.3611 105.8761
206.8432 113.6368
207.3254 124.8719
207.8075 135.8585
208.2896 145.8663
208.7717 155.0750
209.2538 163.8591
209.7359 172.4250
210.2181 180.7490
210.7002 188.5262
211.1823 195.1346
211.6644 201.8248
212.1465 208.7696
212.6286 215.9653
213.1108 223.5826
213.5929 231.8961
214.0750 240.7429
214.5571 247.3691
215.0392 250.0157
215.5213 252.5623
216.0035 256.2439
216.4856 260.6764
216.9677 264.8408
217.4498 268.0089
217.9319 270.2605
218.4140 272.8914
218.8962 276.0049
219.3783 279.3171
219.8604 282.8396
220.3425 286.4832
220.8246 289.9803
221.3067 293.0683
221.7889 295.9055
222.2710 299.4268
222.7531 304.5047
223.2352 309.3202
223.7173 312.8781
224.1994 315.3286
224.6816 317.4815
225.1637 319.8727
225.6458 322.2827
226.1279 324.0423
226.6100 325.4373
227.0921 325.9373
227.5743 325.2393
228.0564 323.3620
228.5385 320.2121
229.0206 315.1881
229.5027 309.0020
229.9848 303.5036
230.4670 298.9765
230.9491 294.8557
231.4312 290.5353
231.9133 285.9919
232.3954 282.0189
232.8775 279.6026
233.3597 277.7263
233.8418 275.0338
234.3239 271.0553
234.8060 266.7103
235.2881 262.8720
235.7702 259.5689
236.2524 256.5380
236.7345 253.7753
237.2166 251.2367
237.6987 248.9623
238.1808 246.9722
238.6629 245.2112
239.1451 243.5450
239.6272 241.8783
240.1093 240.7638
240.5914 241.5293
241.0735 242.3063
241.5556 241.6907
242.0378 239.3112
242.5199 236.0076
243.0020 232.8600
243.4841 230.1173
243.9662 226.7149
244.4483 221.7589
244.9305 216.5172
245.4126 211.9543
245.8947 208.2389
246.3768 204.4343
246.8589 199.1579
247.3410 191.9354
247.8232 184.6346
248.3053 176.8262
248.7874 169.1291
249.2695 162.2200
249.7516 156.2032
250.2337 150.1940
250.7159 142.8724
251.1980 133.6932
251.6801 124.8696
252.1622 116.3177
252.6443 108.1766
253.1264 100.6761
253.6086 93.76636
254.0907 87.09637
254.5728 80.26602
255.0549 72.98041
255.5370 66.69547
256.0191 62.10144
256.5013 57.74704
256.9834 52.63565
257.4655 46.76346
257.9476 40.98355
258.4297 36.22903
258.9118 32.60602
259.3940 29.57831
259.8761 27.52280
260.3582 25.59940
260.8403 23.28851
261.3224 20.65659
261.8045 18.12656
262.2867 16.04703
262.7688 14.41760
263.2509 13.28421
263.7330 13.21680
264.2151 13.02042
264.6972 12.09598
265.1794 10.53891
265.6615 8.718719
266.1436 6.893219
266.6257 5.030121
267.1078 3.729919
267.5899 3.421967
268.0721 3.103455
268.5542 2.077209
269.0363 0.5943910
269.5184 0.4771120
270.0005 0.4379270
270.4826 0.6004640
270.9648 1.032013
271.4469 0.3358150
271.9290 0.2838130
272.4111 0.2022400
272.8932 0.3211670
273.3753 0.5625920
273.8575 3.7108999E-02
274.3396 1.034821
274.8217 1.485809
275.3038 0.8280940
275.7859 0.2565610
276.2680 0.2969210
276.7502 0.6816860
277.2323 0.8047490
277.7144 0.3180080
278.1965 0.4870300
278.6786 0.6454930
279.1607 0.4241640
279.6429 0.9730380
280.1250 0.1555630
280.6071 1.451767
281.0892 2.843658
281.5713 3.668304
282.0534 4.089813
282.5356 4.347977
283.0177 4.376617
283.4998 4.494751
283.9819 4.780396
284.4640 5.206161
284.9461 5.776596
285.4283 6.518753
285.9104 7.278839
286.3925 7.864670
286.8746 8.299759
287.3567 8.489090
287.8388 8.073227
288.3210 7.528366
288.8031 7.529694
289.2852 8.219009
289.7673 9.166946
290.2494 9.907166
290.7315 10.45769
291.2137 11.21156
291.6958 12.51631
292.1779 13.90085
292.6600 14.76791
293.1421 15.04956
293.6242 15.30678
294.1064 16.10851
294.5885 17.30891
295.0706 18.12419
295.5527 17.87233
296.0348 17.62253
296.5169 18.66180
296.9991 20.93901
297.4812 22.70416
297.9633 22.52997
298.4454 21.06142
298.9275 20.46028
299.4096 21.26978
299.8918 22.41840
300.3739 23.18950
300.8560 23.63341
301.3381 24.11172
301.8202 24.84311
302.3023 25.65802
302.7845 26.27635
303.2666 26.78828
303.7487 26.91829
304.2308 26.07100
304.7129 24.61877
305.1950 23.97289
305.6772 24.87816
306.1593 26.37767
306.6414 26.98349
307.1235 26.60558
307.6056 26.41765
308.0877 27.16476
308.5699 28.45518
309.0520 29.33452
309.5341 29.49051
310.0162 29.41592
310.4983 29.69208
310.9804 30.26009
311.4626 30.75150
311.9447 30.94832
312.4268 31.02992
312.9089 31.28741
313.3910 31.77827
313.8731 32.33452
314.3553 32.76518
314.8374 33.10703
315.3195 33.53943
315.8016 34.19406
316.2837 34.92413
316.7658 35.56711
317.2480 36.12860
317.7301 36.69226
318.2122 37.24091
318.6943 37.83099
319.1764 38.62003
319.6585 39.86215
320.1407 41.02763
320.6228 41.59967
321.1049 41.65927
321.5870 41.82309
322.0691 42.45273
322.5512 43.20297
323.0334 43.40869
323.5155 42.87137
323.9976 42.59740
324.4797 43.28346
324.9618 44.59723
325.4439 45.64629
325.9261 46.16673
326.4082 46.41527
326.8903 46.67271
327.3724 46.92157
327.8545 47.24808
328.3366 47.89813
328.8188 48.64667
329.3009 48.97885
329.7830 48.69856
330.2651 48.23184
330.7472 48.10278
331.2293 48.24390
331.7115 48.14040
332.1936 47.34883
332.6757 46.46629
333.1578 46.40947
333.6399 47.21095
334.1220 47.50237
334.6042 46.09373
335.0863 43.45058
335.5684 41.52875
336.0505 40.76384
336.5326 40.33934
337.0147 39.92297
337.4969 39.45671
337.9790 38.63516
338.4611 37.18333
338.9432 35.41248
339.4253 34.01576
339.9074 33.10751
340.3896 32.22597
340.8717 31.19281
341.3538 30.06053
341.8359 28.95282
342.3180 27.91815
342.8001 26.84471
343.2823 25.39725
343.7644 23.46947
344.2465 22.16571
344.7286 22.23473
345.2107 22.75302
345.6928 22.73174
346.1750 22.03104
346.6571 20.96669
347.1392 19.76982
347.6213 18.42758
348.1034 17.09113
348.5855 15.44312
349.0677 14.05814
349.5498 13.47627
350.0319 13.55896
350.5140 13.63272
350.9961 13.29718
351.4782 12.63130
351.9604 12.02615
352.4425 11.35959
352.9246 10.88293
353.4067 10.81517
353.8888 10.96214
354.3709 10.99257
354.8531 10.78455
355.3352 10.40239
355.8173 9.931610
356.2994 9.224503
356.7815 8.758667
357.2636 8.817474
357.7458 9.012909
358.2279 8.914154
358.7100 8.465469
359.1921 7.992844
359.6742 7.885864
360.1563 8.247177
360.6385 8.334869
361.1206 8.086075
361.6027 7.652313
362.0848 6.952347
362.5669 6.105560
363.0490 5.458755
363.5312 5.299637
364.0133 5.533554
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364.9775 4.368088
365.4596 3.471176
365.9417 2.746246
366.4239 2.259384
366.9060 2.169510
367.3881 2.534454
367.8702 3.097153
368.3523 3.336044
368.8344 3.106277
369.3166 2.750687
369.7987 2.263168
370.2808 1.662308
370.7629 0.8319850
371.2450 0.1654360
371.7271 1.012802
372.2093 1.325974
372.6914 1.001999
373.1735 0.8289030
373.6556 0.8242030
374.1377 0.9423980
374.6198 1.279556
375.1020 1.724838
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376.0662 2.105942
376.5483 1.951782
377.0304 1.906693
377.5125 2.087387
377.9947 2.210388
378.4768 2.284790
378.9589 2.258713
379.4410 1.975220
379.9231 1.403564
380.4052 0.8703000
380.8874 1.002548
381.3695 2.152664
381.8516 2.802917
382.3337 2.435425
382.8158 1.876450
383.2979 1.493057
383.7801 1.309860
384.2622 1.187912
384.7443 0.9624180
385.2264 0.6619570
385.7085 0.7137450
386.1906 1.638504
386.6728 2.138779
387.1549 1.476501
387.6370 0.1714940
388.1191 0.9969940
388.6012 1.693115
389.0833 2.108368
389.5655 2.592072
390.0476 3.189575
390.5297 3.645172
391.0118 3.702377
391.4939 3.687210
391.9760 3.836105
392.4582 4.181030
392.9403 4.674057
393.4224 5.327682
393.9045 6.115891
394.3866 6.872879
394.8687 7.541885
395.3509 8.233688
395.8330 9.066925
396.3151 10.00055
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397.2793 11.60362
397.7614 12.30046
398.2436 13.47008
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400.1720 15.90352
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403.0647 19.00093
403.5468 19.46072
404.0290 19.74431
404.5111 20.26239
404.9932 21.01669
405.4753 21.83929
405.9574 22.70242
406.4395 23.61287
406.9217 24.66063
407.4038 25.82672
407.8859 26.84471
408.3680 27.50406
408.8501 27.81226
409.3322 27.97421
409.8144 27.61786
410.2965 27.54546
410.7786 28.33253
411.2607 29.54570
411.7428 30.32182
412.2249 30.28271
412.7071 29.97701
413.1892 30.51433
413.6713 32.71643
414.1534 34.30183
414.6355 34.90683
415.1176 35.19695
415.5998 35.45280
416.0819 35.81548
416.5640 36.54767
417.0461 37.97932
417.5282 40.12799
418.0103 41.64531
418.4925 41.86562
418.9746 42.13553
419.4567 42.98837
419.9388 43.99557
420.4209 44.35782
420.9030 43.69560
421.3852 42.79468
421.8673 43.47046
422.3494 46.68839
422.8315 48.99663
423.3136 49.16589
423.7957 49.09470
424.2779 50.03632
424.7600 51.96814
425.2421 53.95197
425.7242 55.18710
426.2063 55.75188
426.6884 56.32164
427.1706 56.88234
427.6527 57.40636
428.1348 57.98921
428.6169 58.52420
429.0990 58.80788
429.5811 58.72845
430.0633 58.48950
430.5454 58.19592
431.0275 57.83093
431.5096 58.05791
431.9917 59.51089
432.4738 61.10907
432.9560 61.92963
433.4381 62.00380
433.9202 61.35799
434.4023 59.48158
434.8844 57.03249
435.3665 55.20778
435.8487 54.15515
436.3308 53.46320
436.8129 52.94351
437.2950 52.53966
437.7771 52.06895
438.2592 51.63367
438.7414 51.00102
439.2235 50.04367
439.7056 48.78491
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