#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 11:28:43 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1129 $
#$URL: svn://172.16.1.111/rod/cif/8/10/00/8100051.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_8100051
loop_
_publ_author_name
'Newnham, R. E.'
'de Haan, Y. M.'
_publ_section_title
;
 Refinement of the alpha Al2O3, Ti2O3, V2O3 and Cr2O3 structures Locality:
 synthetic
;
_journal_name_full               'Zeitschrift fur Kristallographie'
_journal_page_first              235
_journal_page_last               237
_journal_volume                  117
_journal_year                    1962
_chemical_compound_source        R110117
_chemical_formula_sum            'Al2 O3'
_chemical_name_mineral           Corundum
_space_group_IT_number           167
_symmetry_space_group_name_Hall  '-R 3 2"c'
_symmetry_space_group_name_H-M   'R -3 c :H'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_length_a                   4.7589
_cell_length_b                   4.7589
_cell_length_c                   12.991
_cell_volume                     254.792
_exptl_crystal_density_diffrn    3.987
_cod_original_sg_symbol_H-M      'R -3 c'
_cod_database_code               9008081
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R110117.rod
_rod_data_source.block           3500000
_rod_database.code               8100051
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9008081 COD http://www.crystallography.net/cod/9008081.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
151.3860 0.0000000E+00
151.8681 3.297424
152.3502 3.655487
152.8323 0.4234310
153.3145 0.8286130
153.7966 1.475616
154.2787 1.129700
154.7608 0.1290280
155.2429 0.7742310
155.7250 1.283325
156.2072 1.459595
156.6893 1.294373
157.1714 1.015015
157.6535 0.2847900
158.1356 0.8856200
158.6177 2.563843
159.0999 5.035950
159.5820 8.661499
160.0641 13.66510
160.5462 18.36346
161.0283 22.58075
161.5104 26.58173
161.9926 30.34637
162.4747 33.87164
162.9568 37.70728
163.4389 42.48224
163.9210 48.16687
164.4031 53.93707
164.8853 59.54510
165.3674 65.18921
165.8495 70.95648
166.3316 76.79462
166.8137 83.04242
167.2958 90.43048
167.7780 98.65344
168.2601 106.4361
168.7422 112.8787
169.2243 118.3136
169.7064 123.8474
170.1885 129.1608
170.6707 135.2247
171.1528 142.9935
171.6349 152.1130
172.1170 161.1819
172.5991 169.0135
173.0812 175.5462
173.5634 182.1486
174.0455 188.4537
174.5276 195.2792
175.0097 203.2559
175.4918 212.2261
175.9739 221.3721
176.4561 229.8054
176.9382 237.5416
177.4203 244.6447
177.9024 251.0179
178.3845 256.9089
178.8666 262.2706
179.3488 267.1483
179.8309 271.7875
180.3130 276.3969
180.7951 280.7418
181.2772 285.5597
181.7593 292.0590
182.2415 298.2097
182.7236 302.0787
183.2057 303.3539
183.6878 303.6814
184.1699 305.5989
184.6520 310.4659
185.1342 314.2900
185.6163 316.5060
186.0984 317.8630
186.5805 319.3376
187.0626 321.2668
187.5447 322.8271
188.0269 322.3474
188.5090 319.4836
188.9911 316.5262
189.4732 313.8851
189.9553 311.4815
190.4374 309.3767
190.9196 307.7831
191.4017 305.9711
191.8838 302.7454
192.3659 298.1102
192.8480 293.1951
193.3301 288.4544
193.8123 283.8359
194.2944 279.1767
194.7765 274.6563
195.2586 269.7858
195.7407 264.0740
196.2228 257.5228
196.7050 250.7816
197.1871 244.3099
197.6692 238.0977
198.1513 231.8040
198.6334 224.9651
199.1155 218.3926
199.5977 212.8549
200.0798 208.3224
200.5619 203.8607
201.0440 198.4538
201.5261 191.9033
202.0082 185.5165
202.4904 178.3168
202.9725 172.1407
203.4546 168.6086
203.9367 167.6157
204.4188 167.1374
204.9009 164.4487
205.3831 158.4688
205.8652 153.6185
206.3473 150.6141
206.8294 148.2395
207.3115 146.1140
207.7936 144.0429
208.2758 141.7343
208.7579 138.5932
209.2400 132.6687
209.7221 128.8044
210.2042 127.7366
210.6863 127.8065
211.1685 128.3449
211.6506 129.0156
212.1327 129.4547
212.6148 129.0497
213.0969 126.8150
213.5790 125.8971
214.0612 127.0005
214.5433 128.8791
215.0254 130.4439
215.5075 131.4662
215.9896 132.6398
216.4717 134.9263
216.9539 138.6535
217.4360 143.0265
217.9181 148.3644
218.4002 154.1821
218.8823 160.2001
219.3644 166.3389
219.8466 172.3063
220.3287 177.5075
220.8108 181.7140
221.2929 186.6300
221.7750 193.0842
222.2571 200.1422
222.7393 206.4742
223.2214 211.6821
223.7035 216.8566
224.1856 223.9026
224.6677 232.6616
225.1498 240.1174
225.6320 244.4596
226.1141 247.2720
226.5962 251.1388
227.0783 256.5945
227.5604 262.7811
228.0425 269.3772
228.5247 276.1747
229.0068 282.2297
229.4889 287.0735
229.9710 290.8840
230.4531 293.8566
230.9352 295.5229
231.4174 297.3519
231.8995 300.5685
232.3816 304.8152
232.8637 309.2006
233.3458 312.9630
233.8279 316.4963
234.3101 321.2414
234.7922 327.6752
235.2743 334.6426
235.7564 341.5136
236.2385 348.3746
236.7206 355.5075
237.2028 363.5516
237.6849 372.0687
238.1670 379.1531
238.6491 384.0049
239.1312 388.3679
239.6133 393.0410
240.0955 397.7056
240.5776 401.8762
241.0597 405.0545
241.5418 407.5587
242.0239 411.1028
242.5060 417.7892
242.9882 422.6427
243.4703 424.0689
243.9524 422.9119
244.4345 420.2607
244.9166 416.5084
245.3987 411.8695
245.8809 407.6688
246.3630 404.8855
246.8451 401.3846
247.3272 396.0847
247.8093 389.9853
248.2914 384.5393
248.7736 380.5843
249.2557 377.5956
249.7378 373.4857
250.2199 367.1366
250.7020 360.9339
251.1841 355.3820
251.6663 350.4229
252.1484 346.0826
252.6305 342.2917
253.1126 338.5541
253.5947 333.2471
254.0768 324.8029
254.5590 316.6982
255.0411 309.5002
255.5232 302.7058
256.0053 295.5235
256.4874 287.6400
256.9695 279.4644
257.4517 271.9906
257.9338 265.4447
258.4159 259.4632
258.8980 254.2737
259.3801 249.5748
259.8622 245.0442
260.3444 240.5631
260.8265 236.1017
261.3086 231.6078
261.7907 226.8643
262.2728 222.3941
262.7549 218.1684
263.2371 214.2323
263.7192 210.7801
264.2013 207.8293
264.6834 204.9915
265.1655 201.7454
265.6476 198.2631
266.1298 193.7665
266.6119 187.2632
267.0940 180.2632
267.5761 174.2015
268.0582 169.3260
268.5403 164.9972
269.0225 160.3837
269.5046 155.2773
269.9867 151.2065
270.4688 149.3338
270.9509 147.8312
271.4330 144.7563
271.9152 139.9813
272.3973 135.3897
272.8794 132.8852
273.3615 132.6790
273.8436 132.2585
274.3257 131.6258
274.8079 130.7262
275.2900 129.1400
275.7721 126.9483
276.2542 125.4163
276.7363 125.7683
277.2184 127.7833
277.7006 128.9154
278.1827 128.2747
278.6648 127.4467
279.1469 127.9429
279.6290 129.5421
280.1111 130.3557
280.5933 129.0606
281.0754 126.1037
281.5575 123.4955
282.0396 121.8928
282.5217 119.8606
283.0038 116.2963
283.4860 111.4280
283.9681 106.4882
284.4502 102.2876
284.9323 98.07861
285.4144 92.33359
285.8965 84.52948
286.3787 76.56512
286.8608 69.27722
287.3429 62.65308
287.8250 56.51682
288.3071 50.79211
288.7892 45.61813
289.2714 41.36026
289.7535 38.18707
290.2356 34.59909
290.7177 29.38089
291.1998 23.19589
291.6819 17.73572
292.1641 13.41345
292.6462 9.827972
293.1283 6.678558
293.6104 3.916809
294.0925 1.141022
294.5746 1.995483
295.0568 5.212830
295.5389 8.035004
296.0210 10.49164
296.5031 12.29355
296.9852 12.87747
297.4673 12.58063
297.9495 12.19312
298.4316 11.65198
298.9137 11.28558
299.3958 11.78519
299.8779 13.36169
300.3600 14.85379
300.8422 15.65201
301.3243 15.80383
301.8064 15.21030
302.2885 13.34341
302.7706 11.20264
303.2527 10.00693
303.7349 9.813477
304.2170 9.672729
304.6991 9.199402
305.1812 8.482666
305.6633 7.677185
306.1454 6.851410
306.6276 5.809235
307.1097 3.855530
307.5918 1.108795
308.0739 0.2000730
308.5560 1.729004
309.0381 4.512848
309.5203 5.445038
310.0024 4.347443
310.4845 2.606720
310.9666 0.7649230
311.4487 1.054779
311.9308 2.113892
312.4130 1.861938
312.8951 1.379089
313.3772 1.695679
313.8593 2.704651
314.3414 3.737366
314.8235 4.672516
315.3057 5.380890
315.7878 5.451965
316.2699 4.653778
316.7520 3.682922
317.2341 2.876495
317.7162 2.276703
318.1984 2.053833
318.6805 2.542480
319.1626 3.321716
319.6447 3.628357
320.1268 3.332611
320.6089 3.229340
321.0911 4.050262
321.5732 5.278534
322.0553 6.213898
322.5374 6.701019
323.0195 6.897797
323.5016 6.850616
323.9838 6.559113
324.4659 6.383911
324.9480 6.443878
325.4301 6.720123
325.9122 7.158478
326.3943 7.768616
326.8765 8.517151
327.3586 9.267365
327.8407 10.09265
328.3228 11.45828
328.8049 13.78137
329.2870 16.24561
329.7692 17.85355
330.2513 18.68741
330.7334 19.77228
331.2155 21.55051
331.6976 23.92972
332.1797 26.88126
332.6619 30.67294
333.1440 34.27197
333.6261 36.46579
334.1082 37.77927
334.5903 39.46939
335.0724 41.74564
335.5546 44.65811
336.0367 48.44946
336.5188 53.16980
337.0009 58.07999
337.4830 63.15503
337.9651 68.00015
338.4473 71.84048
338.9294 74.29721
339.4115 76.20267
339.8936 78.23248
340.3757 80.32751
340.8578 81.94769
341.3400 82.87524
341.8221 83.22037
342.3042 83.38434
342.7863 83.51605
343.2684 82.79199
343.7505 80.34311
344.2327 76.75653
344.7148 73.64801
345.1969 71.66742
345.6790 69.38458
346.1611 64.28992
346.6432 56.89478
347.1254 50.80600
347.6075 47.91217
348.0896 46.36740
348.5717 43.53589
349.0538 39.10846
349.5359 35.73318
350.0181 36.08707
350.5002 39.22794
350.9823 40.58954
351.4644 38.13129
351.9465 35.28177
352.4286 34.39249
352.9108 35.11069
353.3929 35.80862
353.8750 35.68628
354.3571 35.14444
354.8392 35.17853
355.3214 36.03705
355.8035 36.97241
356.2856 37.54523
356.7677 38.03790
357.2498 39.08496
357.7319 40.91858
358.2141 42.73352
358.6962 43.47156
359.1783 43.06311
359.6604 42.41327
360.1425 41.00781
360.6246 39.93652
361.1068 40.54950
361.5889 42.78931
362.0710 44.86615
362.5531 45.26550
363.0352 44.00043
363.5173 43.01593
363.9995 42.05438
364.4816 41.61615
364.9637 42.02765
365.4458 43.25507
365.9279 45.15210
366.4100 47.61414
366.8922 50.16266
367.3743 51.41559
367.8564 50.30255
368.3385 49.84723
368.8206 50.81653
369.3027 52.47815
369.7849 53.92743
370.2670 54.85327
370.7491 55.56873
371.2312 56.53925
371.7133 57.78687
372.1954 59.37390
372.6776 61.04242
373.1597 63.19104
373.6418 66.11456
374.1239 69.74341
374.6060 73.78473
375.0881 78.05566
375.5703 82.55713
376.0524 87.73438
376.5345 95.01025
377.0166 101.4489
377.4987 107.2225
377.9808 111.5025
378.4630 113.3315
378.9451 112.2993
379.4272 108.5776
379.9093 102.3897
380.3914 92.08508
380.8735 81.80487
381.3557 70.44275
381.8378 60.01813
382.3199 52.19434
382.8020 47.04370
383.2841 43.30670
383.7662 39.57404
384.2484 35.67645
384.7305 32.87811
385.2126 32.31287
385.6947 31.77979
386.1768 30.41608
386.6589 28.56604
387.1411 27.01697
387.6232 26.26172
388.1053 26.11365
388.5874 25.89587
389.0695 25.46893
389.5516 25.24561
390.0338 25.31647
390.5159 25.60669
390.9980 26.11896
391.4801 26.85242
391.9622 27.60193
392.4443 28.20111
392.9265 28.67743
393.4086 28.71149
393.8907 27.51038
394.3728 26.58929
394.8549 27.00232
395.3370 28.51129
395.8192 30.07837
396.3013 30.87836
396.7834 31.23920
397.2655 32.36469
397.7476 34.62683
398.2297 36.67468
398.7119 37.27344
399.1940 37.39276
399.6761 38.40405
400.1582 41.00049
400.6403 43.78754
401.1224 45.06122
401.6046 44.94983
402.0867 45.40894
402.5688 47.09204
403.0509 49.55164
403.5330 52.30957
404.0151 55.37201
404.4973 58.34113
404.9794 60.70221
405.4615 62.95300
405.9436 66.11542
406.4257 70.37378
406.9078 74.79266
407.3900 78.47192
407.8721 81.60638
408.3542 85.29834
408.8363 89.23755
409.3184 94.09106
409.8005 99.80743
410.2827 106.6854
410.7648 115.5193
411.2469 126.5103
411.7290 139.8874
412.2111 156.2274
412.6932 174.4626
413.1754 197.3563
413.6575 224.9649
414.1396 257.6216
414.6217 298.3485
415.1038 346.6910
415.5859 396.3107
416.0681 443.5132
416.5502 489.9816
417.0323 509.0567
417.5144 500.8145
417.9965 470.4678
418.4786 407.5547
418.9608 325.5196
419.4429 245.7363
419.9250 178.8568
420.4071 124.8430
420.8892 83.85675
421.3713 61.79675
421.8535 45.54004
422.3356 36.63745
422.8177 31.38971
423.2998 27.34790
423.7819 24.00012
424.2640 22.03192
424.7462 22.34009
425.2283 25.08069
425.7104 27.80487
426.1925 30.12427
426.6746 32.87256
427.1567 36.50879
427.6389 40.67505
428.1210 45.10492
428.6031 49.89520
429.0852 54.00092
429.5673 55.11957
430.0494 52.70642
430.5316 49.32233
431.0137 45.04578
431.4958 40.29108
431.9779 34.94696
432.4600 29.13885
432.9421 23.86871
433.4243 20.01129
433.9064 17.36584
434.3885 15.04608
434.8706 13.09814
435.3527 11.34406
435.8348 9.285950
436.3170 7.293701
436.7991 6.123840
437.2812 6.066772
437.7633 6.769409
438.2454 8.276062
438.7275 10.45142
439.2097 12.18140
439.6918 12.93604
440.1739 13.28473
440.6560 14.03613
441.1381 15.18115
441.6202 16.52405
442.1024 18.30780
442.5845 20.09802
443.0666 21.24420
443.5487 21.73914
444.0308 22.24292
444.5129 23.15631
444.9951 24.51575
445.4772 26.59143
445.9593 29.39844
446.4414 32.76508
446.9235 37.76849
447.4056 42.97656
447.8878 46.37494
448.3699 47.27026
448.8520 46.11774
449.3341 43.48297
449.8162 38.88171
450.2983 34.07654
450.7805 28.06592
451.2626 22.80597
451.7447 19.39813
452.2268 17.61115
452.7089 16.60565
453.1910 15.85303
453.6732 15.40173
454.1553 15.51752
454.6374 16.60632
455.1195 17.58392
455.6016 18.59839
456.0837 19.28253
456.5659 18.90192
457.0480 17.45172
457.5301 16.24860
458.0122 16.71490
458.4943 18.82306
458.9764 21.16949
459.4586 24.15845
459.9407 26.68243
460.4228 27.65570
460.9049 27.90552
461.3870 29.04852
461.8691 32.16663
462.3513 35.58746
462.8334 36.73578
463.3155 35.67542
463.7976 35.57715
464.2797 38.03210
464.7618 41.15363
465.2440 42.26910
465.7261 41.33636
466.2082 41.01062
466.6903 42.46313
467.1724 44.85266
467.6545 47.27216
468.1367 49.63098
468.6188 52.03247
469.1009 54.57458
469.5830 57.18823
470.0651 59.58392
470.5472 61.83801
471.0294 63.80188
471.5115 65.69214
471.9936 67.16351
472.4757 67.51984
472.9578 66.66211
473.4399 65.61456
473.9221 65.82050
474.4042 67.89185
474.8863 67.55756
475.3684 63.29071
475.8505 58.53925
476.3326 53.95624
476.8148 49.89197
477.2969 46.89624
477.7790 45.28900
478.2611 44.35986
478.7432 42.44513
479.2253 38.79218
479.7075 36.33984
480.1896 37.14276
480.6717 37.80951
481.1538 35.88885
481.6359 31.90411
482.1180 28.57343
482.6002 28.27393
483.0823 29.79456
483.5644 29.61731
484.0465 27.41553
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