#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 11:29:34 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1142 $
#$URL: svn://172.16.1.111/rod/cif/8/10/00/8100055.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_8100055
loop_
_publ_author_name
'Newnham, R. E.'
'de Haan, Y. M.'
_publ_section_title
;
 Refinement of the alpha Al2O3, Ti2O3, V2O3 and Cr2O3 structures Locality:
 synthetic
;
_journal_name_full               'Zeitschrift fur Kristallographie'
_journal_page_first              235
_journal_page_last               237
_journal_volume                  117
_journal_year                    1962
_chemical_compound_source        X080005
_chemical_formula_sum            'Al2 O3'
_chemical_name_mineral           Corundum
_space_group_IT_number           167
_symmetry_space_group_name_Hall  '-R 3 2"c'
_symmetry_space_group_name_H-M   'R -3 c :H'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_length_a                   4.7589
_cell_length_b                   4.7589
_cell_length_c                   12.991
_cell_volume                     254.792
_exptl_crystal_density_diffrn    3.987
_cod_original_sg_symbol_H-M      'R -3 c'
_cod_database_code               9008081
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            X080005.rod
_rod_data_source.block           3500000
_rod_database.code               8100055
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9008081 COD http://www.crystallography.net/cod/9008081.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
124.1566 0.0000000E+00
124.6387 0.6124730
125.1208 1.028996
125.6029 0.3146670
126.0850 1.8066000E-02
126.5672 0.3972510
127.0493 1.039078
127.5314 1.494652
128.0135 1.609192
128.4956 1.469406
128.9777 1.267807
129.4599 0.7582660
129.9420 0.4964870
130.4241 0.7962650
130.9062 1.329918
131.3883 1.617161
131.8704 1.386864
132.3526 0.7701840
132.8347 0.4851610
133.3168 0.7035290
133.7989 0.9788590
134.2810 1.228508
134.7632 1.435787
135.2453 1.468304
135.7274 1.158764
136.2095 0.7166370
136.6916 0.4359250
137.1737 0.4753110
137.6559 0.6685940
138.1380 0.7873000
138.6201 0.8226470
139.1022 0.8395080
139.5843 0.9411700
140.0664 1.072742
140.5486 1.113667
141.0307 0.9889110
141.5128 0.7676430
141.9949 0.6744960
142.4770 0.7543790
142.9591 0.8811720
143.4413 1.070831
143.9234 1.273685
144.4055 1.406227
144.8876 1.504005
145.3697 1.322445
145.8518 1.125854
146.3340 0.9247740
146.8161 0.7191010
147.2982 0.4164770
147.7803 6.6405997E-02
148.2624 0.1566540
148.7445 4.1412000E-02
149.2267 0.5325470
149.7088 0.9862020
150.1909 1.400021
150.6730 1.630508
151.1551 1.642101
151.6372 1.456337
152.1194 1.258228
152.6015 1.382870
153.0836 1.847412
153.5657 1.952473
154.0478 1.397762
154.5299 0.6505890
155.0121 0.1861310
155.4942 0.1206470
155.9763 0.2329180
156.4584 0.3492240
156.9405 0.4681780
157.4226 0.6130330
157.9048 0.8785210
158.3869 1.172642
158.8690 1.268169
159.3511 1.019508
159.8332 0.6979980
160.3153 0.6373210
160.7975 0.8379670
161.2796 1.070045
161.7617 1.183434
162.2438 1.188736
162.7259 1.224686
163.2081 1.471977
163.6902 1.622253
164.1723 1.318180
164.6544 0.5332830
165.1365 0.2012790
165.6186 0.2068060
166.1008 0.7324750
166.5829 1.442074
167.0650 1.673229
167.5471 1.663933
168.0292 1.470055
168.5113 1.114399
168.9935 0.6998600
169.4756 0.3866810
169.9577 0.1759800
170.4398 7.6964997E-02
170.9219 0.1215630
171.4040 0.2381400
171.8862 0.3886030
172.3683 0.5555310
172.8504 0.7156520
173.3325 0.8158000
173.8146 0.8989940
174.2967 0.8490030
174.7789 0.5062980
175.2610 7.9975002E-02
175.7431 0.1750560
176.2252 0.1426730
176.7073 9.7607002E-02
177.1894 0.2879180
177.6716 0.3837360
178.1537 0.4909440
178.6358 0.7388880
179.1179 1.008762
179.6000 1.017101
180.0821 0.5454290
180.5643 0.1718830
181.0464 0.4016950
181.5285 9.2518002E-02
182.0106 0.6468580
182.4927 0.9513970
182.9748 1.030777
183.4570 0.9882240
183.9391 0.8331450
184.4212 0.6047130
184.9033 0.3668060
185.3854 8.1119999E-02
185.8675 0.1541710
186.3497 0.2343520
186.8318 0.1549610
187.3139 6.2550001E-02
187.7960 2.6455000E-02
188.2781 9.0939999E-03
188.7602 2.7184000E-02
189.2424 8.9954004E-02
189.7245 0.1729810
190.2066 0.2717860
190.6887 0.3895720
191.1708 0.5094870
191.6530 0.5841290
192.1351 0.6744610
192.6172 0.8816110
193.0993 1.270218
193.5814 1.673344
194.0635 1.705975
194.5457 1.106934
195.0278 0.6556820
195.5099 0.4915470
195.9920 0.5380360
196.4741 0.7762220
196.9562 1.209473
197.4384 1.729382
197.9205 2.023201
198.4026 1.981911
198.8847 1.826965
199.3668 1.471458
199.8489 1.066498
200.3311 0.7795260
200.8132 0.6963010
201.2953 0.7765960
201.7774 0.8619230
202.2595 1.028931
202.7416 1.111366
203.2238 1.040550
203.7059 0.8866460
204.1880 0.7350500
204.6701 0.6285320
205.1522 0.5692060
205.6343 0.5742450
206.1165 0.6883960
206.5986 0.8094750
207.0807 0.9447980
207.5628 1.062309
208.0449 1.121601
208.5270 1.104820
209.0092 1.013714
209.4913 0.8512690
209.9734 0.5395280
210.4555 0.2642210
210.9376 8.0200002E-02
211.4197 1.7601000E-02
211.9019 3.2223001E-02
212.3840 5.8127999E-02
212.8661 0.2075690
213.3482 0.2839470
213.8303 0.2176170
214.3124 0.2014270
214.7946 0.4208640
215.2767 0.8218150
215.7588 1.095806
216.2409 1.057816
216.7230 0.8368110
217.2052 0.6876600
217.6873 0.6133420
218.1694 0.6127430
218.6515 0.7395900
219.1336 0.9870220
219.6157 1.147152
220.0979 1.052647
220.5800 0.8867610
221.0621 0.8568120
221.5442 1.003914
222.0263 1.209301
222.5084 1.391800
222.9906 1.542431
223.4727 1.578728
223.9548 1.356770
224.4369 1.085476
224.9190 0.9450840
225.4011 0.9728200
225.8833 1.042839
226.3654 0.9708440
226.8475 0.6991000
227.3296 0.5581440
227.8117 0.7345050
228.2938 0.9894450
228.7760 1.202827
229.2581 1.346165
229.7402 1.430111
230.2223 1.474991
230.7044 1.496346
231.1865 1.422516
231.6687 1.048897
232.1508 0.7235260
232.6329 0.7210660
233.1150 1.063778
233.5971 1.506199
234.0792 1.748741
234.5614 1.782204
235.0435 1.662617
235.5256 1.208591
236.0077 0.7584150
236.4898 0.4956400
236.9719 0.4653360
237.4541 0.6288070
237.9362 0.9817090
238.4183 1.705368
238.9004 2.073189
239.3825 2.014080
239.8646 1.771275
240.3468 1.445988
240.8289 1.083355
241.3110 0.7407490
241.7931 0.4764820
242.2752 0.2751010
242.7573 0.2339900
243.2395 0.3728750
243.7216 0.6180040
244.2037 1.028442
244.6858 1.572411
245.1679 2.050186
245.6501 2.226387
246.1322 2.014774
246.6143 1.789406
247.0964 1.429649
247.5785 1.145218
248.0606 1.135998
248.5428 1.387836
249.0249 1.674683
249.5070 1.780659
249.9891 1.673668
250.4712 1.551208
250.9533 1.381424
251.4355 1.220203
251.9176 1.059650
252.3997 0.9174420
252.8818 0.9095610
253.3639 1.193764
253.8460 1.770702
254.3282 2.075249
254.8103 1.954353
255.2924 1.690578
255.7745 1.406166
256.2566 1.124363
256.7387 0.9483870
257.2209 0.9876170
257.7030 1.210335
258.1851 1.344757
258.6672 1.354103
259.1493 1.341129
259.6314 1.338833
260.1136 1.332508
260.5957 1.267117
261.0778 1.036858
261.5599 0.7423630
262.0420 0.6776810
262.5241 1.083538
263.0063 1.437649
263.4884 1.251534
263.9705 0.5970880
264.4526 0.1083640
264.9347 0.1471900
265.4168 0.5049930
265.8990 0.7357830
266.3811 0.7911570
266.8632 0.8167420
267.3453 0.9717330
267.8274 1.223789
268.3095 1.299839
268.7917 0.9720190
269.2738 0.5355530
269.7559 0.3965070
270.2380 0.6054760
270.7201 0.8794630
271.2022 1.055496
271.6844 1.140701
272.1665 1.155041
272.6486 1.035934
273.1307 0.9086420
273.6128 0.9254950
274.0949 1.087112
274.5771 1.231934
275.0592 1.261341
275.5413 1.184914
276.0234 1.048241
276.5055 0.7780570
276.9876 0.5591050
277.4698 0.5423930
277.9519 0.6932790
278.4340 0.8640440
278.9161 0.9460220
279.3982 0.9646870
279.8803 1.060032
280.3625 1.354668
280.8446 1.534878
281.3267 1.255043
281.8088 0.7215390
282.2909 0.4299960
282.7730 0.8386500
283.2552 1.685768
283.7373 2.067738
284.2194 1.759666
284.7015 1.392387
285.1836 1.240780
285.6658 1.232327
286.1479 1.276867
286.6300 1.381546
287.1121 1.470608
287.5942 1.341370
288.0764 0.8893200
288.5585 0.4630970
289.0406 0.1653750
289.5227 3.3333000E-02
290.0048 0.1567610
290.4869 0.2171060
290.9691 0.1981890
291.4512 4.3262001E-02
291.9333 0.3088070
292.4154 0.6017760
292.8975 0.8271750
293.3796 0.9366460
293.8618 0.8182600
294.3439 0.4448170
294.8260 4.3007001E-02
295.3081 0.1063650
295.7902 1.7128000E-02
296.2723 0.2953380
296.7545 0.9988100
297.2366 1.649334
297.7187 1.941936
298.2008 1.863205
298.6829 1.635708
299.1650 1.479198
299.6472 1.405224
300.1293 1.281445
300.6114 0.9125290
301.0935 0.6702730
301.5756 0.8734660
302.0577 1.397762
302.5399 1.781727
303.0220 1.592297
303.5041 0.8661040
303.9862 0.4308200
304.4683 0.5054170
304.9504 0.6418650
305.4326 0.7100940
305.9147 0.7167170
306.3968 0.6826250
306.8789 0.6054530
307.3610 0.5064200
307.8431 0.4830630
308.3253 0.5854840
308.8074 0.6893770
309.2895 0.8196030
309.7716 0.9121970
310.2537 0.8359680
310.7358 0.5034100
311.2180 0.1169820
311.7001 0.1987610
312.1822 1.100552
312.6643 1.683735
313.1464 1.553024
313.6285 1.164978
314.1107 0.8828770
314.5928 0.8045880
315.0749 0.7685280
315.5570 0.4811400
316.0391 0.2073520
316.5212 0.5938840
317.0034 0.3742520
317.4855 1.5675001E-02
317.9676 0.2940140
318.4497 0.5103990
318.9318 0.6268040
319.4139 0.5968930
319.8961 0.3976780
320.3782 0.2830700
320.8603 0.3461040
321.3424 0.4125820
321.8245 0.4008410
322.3066 0.3354950
322.7888 0.2901150
323.2709 0.3198320
323.7530 0.4155430
324.2351 0.5173800
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325.1993 0.7442780
325.6815 0.9084590
326.1636 1.050022
326.6457 1.051319
327.1278 0.8373070
327.6099 0.4958880
328.0920 0.2446400
328.5742 6.7893997E-02
329.0563 4.4495001E-02
329.5384 0.1132130
330.0205 0.1210020
330.5026 5.9739999E-03
330.9847 0.2583050
331.4669 0.5389370
331.9490 0.6264840
332.4311 0.4563060
332.9132 0.2547840
333.3953 8.4141001E-02
333.8774 0.3475420
334.3596 0.3786430
334.8417 0.1870650
335.3238 7.2903000E-02
335.8059 0.2713810
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336.7701 0.5348820
337.2523 0.7131840
337.7344 0.8032230
338.2165 0.6754420
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352.6800 0.5906070
353.1621 0.6998060
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358.9475 8.6249998E-03
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381.6070 3.093399
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384.0176 1.256882
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385.4640 0.2143860
385.9461 1.3138000E-02
386.4282 0.3971750
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388.8388 0.6299440
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397.5169 1.272003
397.9990 1.737755
398.4811 2.136120
398.9633 2.584450
399.4454 3.188938
399.9275 3.888401
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400.8917 5.084919
401.3738 5.497314
401.8560 5.709568
402.3381 5.573788
402.8202 5.519783
403.3023 5.683880
403.7844 5.981144
404.2665 6.363739
404.7487 6.826962
405.2308 7.262020
405.7129 7.483402
406.1950 7.474552
406.6771 7.580746
407.1592 7.820477
407.6414 8.252655
408.1235 8.959846
408.6056 9.902622
409.0877 10.87505
409.5698 11.63407
410.0519 12.35246
410.5341 13.37659
411.0162 14.64920
411.4983 16.45534
411.9804 18.78677
412.4625 21.84567
412.9446 26.00804
413.4268 31.31876
413.9089 37.76717
414.3910 45.06033
414.8731 53.36839
415.3552 63.69155
415.8373 76.73321
416.3195 91.29516
416.8016 107.4814
417.2837 126.1312
417.7658 138.1246
418.2479 141.4479
418.7300 136.6311
419.2122 121.3699
419.6943 96.04819
420.1764 69.95752
420.6585 49.75408
421.1406 35.45964
421.6227 24.87766
422.1049 19.20366
422.5870 15.33674
423.0691 12.68080
423.5512 10.91035
424.0333 9.482998
424.5154 8.173203
424.9976 7.081509
425.4797 6.450455
425.9618 6.488705
426.4439 6.629414
426.9260 6.813263
427.4081 7.140125
427.8903 7.792850
428.3724 8.698177
428.8545 9.557697
429.3366 10.12295
429.8187 10.37620
430.3008 10.54223
430.7830 10.85975
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